2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE
- Product Name
- 2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE
- CAS No.
- 28004-63-9
- Chemical Name
- 2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE
- Synonyms
- AKOS B014677;TIMTEC-BB SBB007063;ART-CHEM-BB B014677;IFLAB-BB F1386-0069;CHEMBRDG-BB 5313490;5-(2,4-Dichlorophenyl);5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOL-2-AMINE;2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE;1,3,4-Thiadiazol-2-aMine, 5-(2,4-dichlorophenyl)-;5-(2,4-DICHLOROPHENYL)-[1,3,4]THIADIAZOL-2-YL-AMINE
- CBNumber
- CB6101543
- Molecular Formula
- C8H5Cl2N3S
- Formula Weight
- 246.12
- MOL File
- 28004-63-9.mol
2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE Property
- Melting point:
- 240-242℃ (ethanol water )
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
Safety
- Hazard Codes
- Xi
- HazardClass
- IRRITANT
N-Bromosuccinimide Price
- Product number
- D435313
- Product name
- 5-(2,4-Dichlorophenyl)-1,3,4-thiadiazol-2-amine
- Packaging
- 500mg
- Price
- $130
- Updated
- 2021/12/16
- Product number
- 007785
- Product name
- 5-(2,4-Dichlorophenyl)-[1,3,4]thiadiazol-2-yl-amine
- Packaging
- 500mg
- Price
- $168
- Updated
- 2021/12/16
- Product number
- 2698AB
- Product name
- 5-(2,4-Dichlorophenyl)-1,3,4-thiadiazol-2-amine
- Packaging
- 1g
- Price
- $172
- Updated
- 2021/12/16
- Product number
- FD113695
- Product name
- 5-(2,4-Dichlorophenyl)-1,3,4-thiadiazol-2-amine
- Packaging
- 2g
- Price
- $218
- Updated
- 2021/12/16
- Product number
- FD113695
- Product name
- 5-(2,4-Dichlorophenyl)-1,3,4-thiadiazol-2-amine
- Packaging
- 500mg
- Price
- $75
- Updated
- 2021/12/16
2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE Chemical Properties,Usage,Production
Synthesis
6957-92-2
28004-63-9
General method: In step 2, the Schiff base intermediate was dissolved in 1,4-dioxane, iodine and potassium carbonate were added, and the cyclization reaction was carried out at 80 °C. The reaction mixture was refluxed for 4 hours and the progress of the reaction was monitored by thin layer chromatography (TLC). After completion of the reaction, the mixture was cooled to room temperature and the reaction was quenched by the addition of 5% sodium thiosulfate solution (20 ml). The target organic compounds in the reaction mixture were extracted with ethyl acetate. The organic phase was separated and collected and the solvent was removed by evaporation to give a solid product of 2-amino-5-(2,4-dichlorophenyl)-1,3,4-thiadiazole.
References
[1] Monatshefte fur Chemie, 2013, vol. 144, # 5, p. 681 - 686
[2] Bioorganic Chemistry, 2018, vol. 78, p. 201 - 209
[3] Archiv der Pharmazie, 2015, vol. 348, # 1, p. 10 - 22
[4] Turkish Journal of Chemistry, 2018, vol. 42, # 3, p. 839 - 858
[5] Indian Journal of Chemistry, 1970, vol. 8, p. 509 - 513
2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE Preparation Products And Raw materials
Raw materials
Preparation Products
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