3-Hydroxy-2-iodo-6-methylpyridine
- Product Name
- 3-Hydroxy-2-iodo-6-methylpyridine
- CAS No.
- 23003-30-7
- Chemical Name
- 3-Hydroxy-2-iodo-6-methylpyridine
- Synonyms
- 3-Hydroxy-2-iodo-6-;6-IODO-2-PICOLIN-5-OL;6-Iodo-2-picolin-5-ol,97%;6-IODO-2-PICOLIN-5-OL 97%;2-IODO-3-HYDROXY-6-PICOLINE;2-IODO-6-METHYL-3-PYRIDINOL;3-Pyridinol, 2-iodo-6-methyl-;2-IODO-6-METHYL-3-HYDROXYPYRIDINE;3-HYDROXY-2-IODO-6-METHYLPYRIDINE;2-Iodo-3-hydroxy-6-methylpyridine
- CBNumber
- CB6108522
- Molecular Formula
- C6H6INO
- Formula Weight
- 235.02
- MOL File
- 23003-30-7.mol
3-Hydroxy-2-iodo-6-methylpyridine Property
- Melting point:
- 197-199 °C (lit.)
- Boiling point:
- 292.0±35.0 °C(Predicted)
- Density
- 1.8615 (estimate)
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- pka
- 5.46±0.10(Predicted)
- Appearance
- White to light brown Solid
- InChI
- InChI=1S/C6H6INO/c1-4-2-3-5(9)6(7)8-4/h2-3,9H,1H3
- InChIKey
- HRZOWBGCOJWHDY-UHFFFAOYSA-N
- SMILES
- C1(I)=NC(C)=CC=C1O
- CAS DataBase Reference
- 23003-30-7(CAS DataBase Reference)
Safety
- Hazard Codes
- Xi
- Risk Statements
- 36/37/38
- Safety Statements
- 26-37/39-24/25
- WGK Germany
- 3
- HS Code
- 29333999
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 119024
- Product name
- 3-Hydroxy-2-iodo-6-methylpyridine
- Purity
- 97%
- Packaging
- 1g
- Price
- $79.5
- Updated
- 2023/06/20
- Product number
- 279707
- Product name
- 3-Hydroxy-2-iodo-6-methylpyridine
- Packaging
- 1g
- Price
- $345
- Updated
- 2021/12/16
- Product number
- H943618
- Product name
- 3-Hydroxy-2-iodo-6-methylpyridine
- Packaging
- 500mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- H943618
- Product name
- 3-Hydroxy-2-iodo-6-methylpyridine
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 076967
- Product name
- 3-Hydroxy-2-iodo-6-methylpyridine
- Purity
- 97%
- Packaging
- 250mg
- Price
- $14
- Updated
- 2021/12/16
3-Hydroxy-2-iodo-6-methylpyridine Chemical Properties,Usage,Production
Chemical Properties
Light yellow to yellow powder
Synthesis
1121-78-4
23003-30-7
Step A: 6-Methylpyridin-3-ol (0.5 g, 4.58 mmol) was dissolved in aqueous sodium hydroxide solution (4.5 mL, 1 M, 4.5 mmol). Iodine (1.28 g, 5.2 mmol) was added to this solution and the reaction mixture was stirred overnight at room temperature. After completion of the reaction, it was neutralized with aqueous hydrochloric acid (2 M) to pH ≈ 7. A white precipitate precipitated from the reaction system and the product was collected by filtration. The solid product was washed with deionized water and dried to give 2-iodo-6-methylpyridin-3-ol (0.8 g, 50% yield). Mass spectral analysis showed m/z 236.0 [M + H]+.
References
[1] Bioorganic and Medicinal Chemistry Letters, 1998, vol. 8, # 16, p. 2117 - 2122
[2] Patent: US9617268, 2017, B2. Location in patent: Page/Page column 400; 401
[3] Patent: EP1477186, 2004, A1. Location in patent: Page/Page column 35; 36
[4] Patent: EP1357111, 2003, A1. Location in patent: Page/Page column 54
[5] Tetrahedron, 2007, vol. 63, # 13, p. 2787 - 2797
3-Hydroxy-2-iodo-6-methylpyridine Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-Hydroxy-2-iodo-6-methylpyridine manufacturers
- Product
- 3-Hydroxy-2-iodo-6-methylpyridine 23003-30-7
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-09-24
- Product
- 3-Hydroxy-2-iodo-6-methylpyridine 23003-30-7
- Price
- US $3.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100kg
- Release date
- 2019-07-04