ChemicalBook > CAS DataBase List > 4-(4-AMINOPHENYL)-PIPERIDINE

4-(4-AMINOPHENYL)-PIPERIDINE

Product Name: 4-(4-AMINOPHENYL)-PIPERIDINE
CAS No.: 113310-52-4
Chemical Name: 4-(4-AMINOPHENYL)-PIPERIDINE
Synonyms: 4-(4-Piperidyl)aniline;4-(4-piperidinyl)aniline;4-(Piperidin-4-yl)benzenamine;Benzenamine, 4-(4-piperidinyl)-;4-(4-Aminophenyl)-piperidine HCl
CBNumber: CB61118898
Molecular Formula: C11H16N2
Formula Weight: 176.26
MOL File: 113310-52-4.mol

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4-(4-AMINOPHENYL)-PIPERIDINE Property

Boiling point:: 328.3±42.0 °C(Predicted)
Density: 1.043±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: 10.34±0.10(Predicted)
Appearance: Off-white to pink Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: P992350
Product name: 4-(Piperidin-4-yl)aniline
Packaging: 500mg
Price: $310
Updated: 2021/12/16

AK Scientific

Product number: 0097DA
Product name: 4-(Piperidin-4-yl)aniline
Packaging: 250mg
Price: $123
Updated: 2021/12/16

AK Scientific

Product number: 0097DA
Product name: 4-(Piperidin-4-yl)aniline
Packaging: 1g
Price: $232
Updated: 2021/12/16

Ambeed

Product number: A293511
Product name: 4-(Piperidin-4-yl)aniline
Purity: 97%
Packaging: 250mg
Price: $47
Updated: 2021/12/16

Ambeed

Product number: A293511
Product name: 4-(Piperidin-4-yl)aniline
Purity: 97%
Packaging: 1g
Price: $47
Updated: 2021/12/16

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4-(4-AMINOPHENYL)-PIPERIDINE Chemical Properties,Usage,Production

Synthesis

26905-03-3

113310-52-4

Under argon protection, 4-(4-nitrophenyl)piperidine (400 mg, 1.942 mmol) was dissolved in methanol (30 mL) and palladium catalyst (144 mg) was added. Argon was replaced with hydrogen and the reaction was stirred at room temperature for 3.5 hours. Upon completion of the reaction, the palladium catalyst was removed by filtration and the solvent was removed by concentration under reduced pressure. The residue was purified by dichloromethane milling to give 4-(piperidin-4-yl)aniline (340 mg, 99% yield) as a white solid.HPLC analysis showed a purity of 95.0% [retention time R = 6.74 min, mobile phase 30% methanol/0.1% trifluoroacetic acid aqueous solution, run time 20 min].1H NMR (400 MHz, methanol-d4) δ 6.99 (d, J = 8.4 Hz, 2H), 6.69 (d, J = 8.4 Hz, 2H), 3.46-3.22 (m, 2H), 2.95 (td, J = 12.8, 3.0 Hz, 2H), 2.70-2.62 (m, 1H), 1.96-1.84 (m, 2H), 1.82-1.70 (m, 2H).LC -MS (ESI+) m/z 177.13808 [M + H]+. HRMS (ESI+) m/z Calculated C11H16N2 [M + H]+ 177.1386, measured 177.1382.

References

[1] Patent: WO2015/21149, 2015, A1. Location in patent: Page/Page column 99
[2] Journal of Medicinal Chemistry, 2015, vol. 58, # 6, p. 2746 - 2763

4-(4-AMINOPHENYL)-PIPERIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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113310-52-4, 4-(4-AMINOPHENYL)-PIPERIDINE Related Search:

4-(8-azabicyclo[3.2.1]oct-3-yl)aniline 4-P-AMINOPHENYL-1-BOC-PIPERIDINE 1-[4-(4-Amino-phenyl)-piperidin-1-yl]-3,3-dimethyl-butan-1-one N,N-Dimethyl-4-(4-piperidinyl)anilinedihydrochloride (1R,2S,3S,5S)-8-METHYL-3-(4-NITRO-PHENYL)-8-AZA-BICYCLO[3.2.1]OCTANE-2-CARBOXYLIC ACID METHYL ESTER 4-AMINOPHENYL-1-PHENETHYLPIPERIDINE 4-(4-NITRO-PHENYL)-PIPERIDINE HYDROCHLORIDE (1R,2S,3S,5S)-3-(4-AMINO-PHENYL)-8-METHYL-8-AZA-BICYCLO[3.2.1]OCTANE-2-CARBOXYLIC ACID METHYL ESTER 4-(1-METHYL-PIPERIDIN-4-YL)-ANILINE 4-(PIPERIDIN-4-YL)ANILINE HYDROCHLORIDE 4-(4-NITRO-PHENYL)-PIPERIDINE 4-(4-NITROPHENYL)PIPERIDINE HYDROGEN SULFATE (4-PIPERIDIN-4-YL-PHENYL)-CARBAMIC ACID TERT-BUTYL ESTER 4-(4-AMINOPHENYL)-PIPERIDINE

4-(Piperidin-4-yl)benzenamine

4-(4-Aminophenyl)-piperidine HCl

4-(4-piperidinyl)aniline

Benzenamine, 4-(4-piperidinyl)-

4-(4-Piperidyl)aniline

113310-52-4