ChemicalBook > CAS DataBase List > 4-Methoxycyclohexanon

4-Methoxycyclohexanon

Product Name
4-Methoxycyclohexanon
CAS No.
13482-23-0
Chemical Name
4-Methoxycyclohexanon
Synonyms
4-Methoxycyclohexano;4-Methoxycyclohexanon;p-Methoxycyclohexanone;4-Metho×ycyclohe×anone;Cyclohexanone, 4-methoxy-;4-Methoxycyclohexan-1-one;4-methoxycyclohexanone, 98%min;4-methoxycyclohexan-1-one - [M82414]
CBNumber
CB61448450
Molecular Formula
C7H12O2
Formula Weight
128.17
MOL File
13482-23-0.mol
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4-Methoxycyclohexanon Property

Boiling point:
189 ºC
Density 
0.98
refractive index 
1.4560
Flash point:
69 ºC
storage temp. 
2-8°C
solubility 
soluble in Chloroform, Ethyl Acetate, Methanol
form 
liquid
color 
Clear, pale yellow
InChI
InChI=1S/C7H12O2/c1-9-7-4-2-6(8)3-5-7/h7H,2-5H2,1H3
InChIKey
XADCKKKOYZJNAR-UHFFFAOYSA-N
SMILES
C1(=O)CCC(OC)CC1
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Safety

HS Code 
2914500090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
M262380
Product name
4-Methoxycyclohexanone
Packaging
1g
Price
$80
Updated
2021/12/16
Frontier Specialty Chemicals
Product number
M15675
Product name
4-Methoxycyclohexanone
Purity
97%
Packaging
5g
Price
$98
Updated
2021/12/16
Frontier Specialty Chemicals
Product number
M15675
Product name
4-Methoxycyclohexanone
Purity
97%
Packaging
1g
Price
$24
Updated
2021/12/16
Matrix Scientific
Product number
075943
Product name
4-Methoxycyclohexanone
Purity
95+%
Packaging
1g
Price
$138
Updated
2021/12/16
Apolloscientific
Product number
OR480813
Product name
4-Methoxycyclohexanone
Purity
95%
Packaging
1g
Price
$151
Updated
2021/12/16
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4-Methoxycyclohexanon Chemical Properties,Usage,Production

Uses

4-Methoxycyclohexanone is a substituted cyclohexanone used in the preparation of various organic compounds such as antitumor agents.

Synthesis

150-76-5

13482-23-0

The general procedure for the synthesis of p-methoxycyclohexanone from p-hydroxyanisole is as follows: 7 g of palladium-carbon catalyst and 1 g of borax were added to an autoclave, followed by 150 g of methylcyclohexane and 100 g of p-hydroxyanisole. The reaction was slowly heated to 100 °C and hydrogen was introduced into the system until the pressure reached 1.0 MPa, and stirring was started. When the pressure dropped to 0.5 MPa, hydrogen was supplemented to 1.0 MPa, keeping the reaction pressure in the range of 0.7-1.0 MPa. Continuously monitor the hydrogen consumption, and after the hydrogen consumption stops for a period of time, take samples for reaction process monitoring. When the remaining amount of raw material is less than 1%, the reaction is judged to be complete. The reaction mixture was cooled to 30°C and filtered to remove the catalyst. The filtrate was evaporated to remove the solvent and subsequently distilled under reduced pressure to give 92 g of p-methoxycyclohexanone in 90% yield.

References

[1] Patent: CN107827881, 2018, A. Location in patent: Paragraph 0034; 0035
[2] Patent: US5886232, 1999, A
[3] Tetrahedron Letters, 1994, vol. 35, # 39, p. 7151 - 7154
[4] Journal of Organic Chemistry, 1961, vol. 26, p. 2633 - 2640
[5] Tetrahedron, 1976, vol. 32, p. 2589 - 2594

4-Methoxycyclohexanon Preparation Products And Raw materials

Raw materials

Preparation Products

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4-Methoxycyclohexanon Suppliers

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View Lastest Price from 4-Methoxycyclohexanon manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD
Product
4-Methoxycyclohexanone 13482-23-0
Price
US $3.00-9.00/KG
Min. Order
0.1KG
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2025-06-24
Shanghai Yongzeng Technology Co.,Ltd
Product
4-Methoxycyclohexanone 13482-23-0
Price
US $0.00/kg
Min. Order
100kg
Purity
96%min
Supply Ability
1 tons
Release date
2024-09-10
Anhui Ruihan Technology Co., Ltd
Product
4-Methoxycyclohexanon 13482-23-0
Price
US $50.00/kg
Min. Order
1kg
Purity
99.9%
Supply Ability
10000tons
Release date
2023-08-23

13482-23-0, 4-MethoxycyclohexanonRelated Search:

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  • 4-Methoxycyclohexan-1-one
  • 4-Metho×ycyclohe×anone
  • 4-Methoxycyclohexanon
  • p-Methoxycyclohexanone
  • Cyclohexanone, 4-methoxy-
  • 4-Methoxycyclohexano
  • 4-methoxycyclohexanone, 98%min
  • 4-methoxycyclohexan-1-one - [M82414]
  • 13482-23-0
  • 13842-23-0
  • Intermediates
  • Miscellaneous reagents