4-BROMO-3-FLUOROPHENYLACETIC ACID

Product Name: 4-BROMO-3-FLUOROPHENYLACETIC ACID
CAS No.: 942282-40-8
Chemical Name: 4-BROMO-3-FLUOROPHENYLACETIC ACID
Synonyms: 2-(4-broMo-3-fluorophenyl)acetic acid;4-BROMO-3-FLUOROPHENYLACETIC ACID;4-Bromo-3-fluorophenylacetic acid 98%;benzeneacetic acid, 4-bromo-3-fluoro-;4-BROMO-3-FLUOROPHENYLACETIC ACID ISO 9001：2015 REACH
CBNumber: CB61483068
Molecular Formula: C8H6BrFO2
Formula Weight: 233.03
MOL File: 942282-40-8.mol

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4-BROMO-3-FLUOROPHENYLACETIC ACID Property

Boiling point:: 317.9±27.0 °C(Predicted)
Density: 1.697±0.06 g/cm3 (20 ºC 760 Torr)
storage temp.: Sealed in dry,Room Temperature
pka: 3.97±0.10(Predicted)
form: powder
color: White to off white

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Safety

HS Code: 2916399090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B692893
Product name: 4-Bromo-3-fluorophenylaceticacid
Packaging: 500mg
Price: $65
Updated: 2021/12/16

TRC

Product number: B692893
Product name: 4-Bromo-3-fluorophenylaceticacid
Packaging: 1g
Price: $75
Updated: 2021/12/16

Matrix Scientific

Product number: 066943
Product name: 4-Bromo-3-fluorophenylacetic acid
Purity: 98%
Packaging: 1g
Price: $19
Updated: 2021/12/16

AK Scientific

Product number: W9665
Product name: 4-Bromo-3-fluorophenylaceticacid
Packaging: 1g
Price: $27
Updated: 2021/12/16

Matrix Scientific

Product number: 066943
Product name: 4-Bromo-3-fluorophenylacetic acid
Purity: 98%
Packaging: 5g
Price: $59
Updated: 2021/12/16

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4-BROMO-3-FLUOROPHENYLACETIC ACID Chemical Properties,Usage,Production

Chemical Properties

off-white solid

Synthesis

499983-13-0

942282-40-8

General procedure for the synthesis of 2-(4-bromo-3-fluorophenyl)acetic acid from 3-fluoro-4-bromophenylacetonitrile: 3-fluoro-4-bromophenylacetonitrile (0.78 g, 3.64 mmol) was dissolved in a mixture of sulphuric acid (5 mL) and water (5 mL), and the reaction was stirred for 16 hours at 100 °C. The progress of the reaction was monitored by LCMS and after confirming complete consumption of the raw materials, the reaction mixture was dissolved in water (20 mL) and extracted with ethyl acetate (20 mL). The organic layers were combined, dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure to afford 2-(4-bromo-3-fluorophenyl)acetic acid (0.7 g, 2.046 mmol, 56.1% yield) as a white solid. The product was characterized by 1H NMR (400 MHz, CD3OD): δ 7.53 (t, J = 7.8 Hz, 1H), 7.16 (dd, J = 9.8, 1.9 Hz, 1H), 7.02 (d, J = 8.0 Hz, 1H), 3.61 (s, 2H).

References

[1] Patent: WO2018/39386, 2018, A1. Location in patent: Page/Page column 302
[2] Patent: US2014/275111, 2014, A1. Location in patent: Paragraph 0349; 0350
[3] Patent: WO2014/141187, 2014, A1. Location in patent: Page/Page column 76
[4] Patent: WO2007/69986, 2007, A1. Location in patent: Page/Page column 92-93
[5] Patent: WO2017/98440, 2017, A1. Location in patent: Page/Page column 184

4-BROMO-3-FLUOROPHENYLACETIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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4-BROMO-3-FLUOROPHENYLACETIC ACID Suppliers

China 96 India 1 United Kingdom 4 United States 10 Global 111

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View Lastest Price from 4-BROMO-3-FLUOROPHENYLACETIC ACID manufacturers

Career Henan Chemical Co

Product: 4-BROMO-3-FLUOROPHENYLACETIC ACID 942282-40-8
Price: US $1.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: 1000KGS
Release date: 2020-01-14

942282-40-8, 4-BROMO-3-FLUOROPHENYLACETIC ACIDRelated Search:

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4-BROMO-3-FLUOROPHENYLACETIC ACID

2-(4-broMo-3-fluorophenyl)acetic acid

benzeneacetic acid, 4-bromo-3-fluoro-

4-Bromo-3-fluorophenylacetic acid 98%

4-BROMO-3-FLUOROPHENYLACETIC ACID ISO 9001：2015 REACH

942282-40-8