ChemicalBook > CAS DataBase List > 2-ISOPROPYL-4-NITROPHENOL

2-ISOPROPYL-4-NITROPHENOL

Product Name
2-ISOPROPYL-4-NITROPHENOL
CAS No.
60515-72-2
Chemical Name
2-ISOPROPYL-4-NITROPHENOL
Synonyms
4-nitro-2-isopropylphenol;2-ISOPROPYL-4-NITROPHENOL;4-nitro-2-propan-2-ylphenol;Phenol, 2-(1-methylethyl)-4-nitro-
CBNumber
CB61507980
Molecular Formula
C9H11NO3
Formula Weight
181.19
MOL File
60515-72-2.mol
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2-ISOPROPYL-4-NITROPHENOL Property

Melting point:
86 °C
Boiling point:
294.3±33.0 °C(Predicted)
Density 
1.209±0.06 g/cm3(Predicted)
storage temp. 
Inert atmosphere,Room Temperature
pka
7.62±0.22(Predicted)
Appearance
Brown to black Solid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
I872808
Product name
2-Isopropyl-4-nitrophenol
Packaging
2mg
Price
$60
Updated
2021/12/16
AK Scientific
Product number
9023AB
Product name
2-Isopropyl-4-nitrophenol
Packaging
5g
Price
$300
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0098205
Product name
2-ISOPROPYL-4-NITROPHENOL
Purity
95.00%
Packaging
5MG
Price
$503.11
Updated
2021/12/16
Crysdot
Product number
CD12056519
Product name
2-Isopropyl-4-nitrophenol
Purity
95+%
Packaging
25g
Price
$534
Updated
2021/12/16
Alichem
Product number
60515722
Product name
2-Isopropyl-4-nitrophenol
Packaging
25g
Price
$555.36
Updated
2021/12/16
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2-ISOPROPYL-4-NITROPHENOL Chemical Properties,Usage,Production

Synthesis

88-69-7

141-78-6

60515-72-2

To a solution of acetic acid (30 mL) containing 2-isopropylphenol (4.1 mL), 69% nitric acid (4 mL) was slowly added under ice bath conditions, keeping the reaction temperature constant with constant stirring for 30 minutes. Upon completion of the reaction, the reaction was quenched by the addition of ice water and subsequently extracted with tert-butyl methyl ether. The organic phase was washed sequentially with water and saturated saline, dried over anhydrous sodium sulfate and filtered. The filtrate was concentrated under reduced pressure to obtain the crude product. The crude product was purified by silica gel column chromatography, and the eluent was a mixed solvent of hexane/ethyl acetate in the ratio of 4:1, v/v. The target compound 2-isopropyl-4-nitrophenol (2.66 g, 49% yield) was finally obtained as a yellow solid. The structure of the product was confirmed by 1H NMR (400 MHz, CDCl3): δ 1.3 (6H, d, J = 7.0 Hz), 3.25 (1H, m), 6.82 (1H, d, J = 9.0 Hz), 8.01 (1H, dd, J = 9.0, 2.5 Hz), 8.13 (1H, d, J = 2.5 Hz).

References

[1] Patent: US6555556, 2003, B1

2-ISOPROPYL-4-NITROPHENOL Preparation Products And Raw materials

Raw materials

Preparation Products

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2-ISOPROPYL-4-NITROPHENOL Suppliers

China 32 India 1 United States 3 Global 36
Cool Pharm, Ltd
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021-60455363 18019463053
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China
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Quzhou AMK BioTech Co., Ltd
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China
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Shanghai YuanYe Biotechnology Co., Ltd.
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021-61312847; 18021002903
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QQ:3008007432
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China
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71826
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Nanijing m&m biotechnology Co. ,Ltd.
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025-87782433 18021532344
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Aikon International Limited
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China
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Suzhou Nuoouman Biological Technology Co., Ltd.
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SHANGHAI FDC-CHEMICAL CO.,LTD
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Suzhou Xiya Pharmaceutical Co., Ltd.
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Henan's chemical products co., LTD
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Fuxin Crest Biotechnology Co. Ltd.
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60515-72-2, 2-ISOPROPYL-4-NITROPHENOLRelated Search:

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  • 2-ISOPROPYL-4-NITROPHENOL
  • 4-nitro-2-isopropylphenol
  • 4-nitro-2-propan-2-ylphenol
  • Phenol, 2-(1-methylethyl)-4-nitro-
  • 60515-72-2