ChemicalBook > CAS DataBase List > 6-iodoquinazoline

6-iodoquinazoline

Product Name: 6-iodoquinazoline
CAS No.: 848841-54-3
Chemical Name: 6-iodoquinazoline
Synonyms: 6-iodoquinazoline;Quinazoline, 6-iodo-
CBNumber: CB61518728
Molecular Formula: C8H5IN2
Formula Weight: 256.04
MOL File: 848841-54-3.mol

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6-iodoquinazoline Property

Boiling point:: 329.1±15.0 °C(Predicted)
Density: 1.938±0.06 g/cm3(Predicted)
storage temp.: 2-8°C(protect from light)
pka: 3.65±0.26(Predicted)
Appearance: Light yellow to yellow Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

AK Scientific

Product number: W8756
Product name: 6-Iodoquinazoline
Packaging: 1g
Price: $253
Updated: 2021/12/16

Matrix Scientific

Product number: 072240
Product name: 6-Iodoquinazoline
Purity: 95+%
Packaging: 250mg
Price: $370
Updated: 2021/12/16

Matrix Scientific

Product number: 072240
Product name: 6-Iodoquinazoline
Purity: 95+%
Packaging: 1g
Price: $798
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0143424
Product name: 6-IODOQUINAZOLINE
Purity: 95.00%
Packaging: 250MG
Price: $984.06
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0143424
Product name: 6-IODOQUINAZOLINE
Purity: 95.00%
Packaging: 1G
Price: $1455.3
Updated: 2021/12/16

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6-iodoquinazoline Chemical Properties,Usage,Production

Synthesis

253-82-7

848841-54-3

General procedure for the synthesis of 6-iodoquinazoline from quinazoline: N-iodosuccinimide (NIS, 5.4 g, 24 mmol) was slowly added to a solution of quinazoline (2.1 g, 16.13 mmol) in concentrated sulfuric acid (16 mL) at 0 °C. The reaction mixture was stirred at 0 °C for 10 min before gradually warming to room temperature and continued stirring for 15 h. The reaction mixture was then mixed with NIS (2.4 g, 16.13 mmol). Subsequently, NIS (2.0 g, 8.9 mmol) was added supplementally and the mixture was continued to stir for 5 hours. After completion of the reaction, the mixture was slowly poured into crushed ice (80 g) and stirred for 1 hour. The resulting solution was filtered, the pH was adjusted to 7 with concentrated ammonia and stirred for another 1 hour at 0°C. It was filtered again and the solids were washed with ice-cold water. Finally, the solid was air dried to give 6-iodoquinazoline (3.4 g, 87% yield). The product was confirmed by 1H NMR (400 MHz, DMSO) and mass spectrometry (MS ESI m/z 256 [M+H]+, C6H3IN4).

References

[1] Patent: WO2005/28444, 2005, A1. Location in patent: Page/Page column 56

6-iodoquinazoline Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 6-iodoquinazoline manufacturers

Career Henan Chemical Co

Product: 6-iodoquinazoline 848841-54-3
Price: US $9.80/KG
Min. Order: 1g
Purity: ≥99%
Supply Ability: 100kg
Release date: 2020-01-12

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6-iodoquinazoline

Quinazoline, 6-iodo-

848841-54-3

848541-54-3