2,2'-Bipyridine-3,3'-dicarboxylic acid dimethyl ester

Product Name: 2,2'-Bipyridine-3,3'-dicarboxylic acid dimethyl ester
CAS No.: 39775-31-0
Chemical Name: 2,2'-Bipyridine-3,3'-dicarboxylic acid dimethyl ester
Synonyms: 3,3'-bis(methoxycarbonyl)-2,2'-bipyridine;diMethyl 2,2'-bipyridine-3,3'-dicarboxylate;Dimethyl [2,2'-bipyridine]-3,3'-dicarboxylate;2,2'-Bipyridine-3,3'-dicarboxylic acid dimethyl ester;2,2'-Bipyridinyl-3,3'-dicarboxylic acid diMethyl ester;2, 2'-Bipyridine-3, 3'-dicarboxylic acid dimethyl ester;(2,2')BIPYRIDINYL-3,3'-DICARBOXYLIC ACID DIMETHYL ESTER;[2,2'-Bipyridine]-3,3'-dicarboxylicacid, 3,3'-dimethyl ester;[2,2'-Bipyridine]-3,3'-dicarboxylic acid, 3,3'-dimethyl ester;methyl2-(3-methoxycarbonylpyridin-2-yl)pyridine-3-carboxylate
CBNumber: CB62135454
Molecular Formula: C14H12N2O4
Formula Weight: 272.26
MOL File: 39775-31-0.mol

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2,2'-Bipyridine-3,3'-dicarboxylic acid dimethyl ester Property

Melting point:: 155-156 °C
Boiling point:: 424.6±45.0 °C(Predicted)
Density: 1.254±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 1.84±0.32(Predicted)
Appearance: Light yellow to yellow Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B399323
Product name: 2,2-Bipyridine-3,3-dicarboxylicAcidDimethylEster
Packaging: 500mg
Price: $175
Updated: 2021/12/16

AK Scientific

Product number: 2145CC
Product name: Dimethyl[2,2'-bipyridine]-3,3'-dicarboxylate
Packaging: 5g
Price: $392
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0309474
Product name: (2,2')BIPYRIDINYL-3,3'-DICARBOXYLIC ACID DIMETHYL ESTER
Purity: 95.00%
Packaging: 5MG
Price: $497.08
Updated: 2021/12/16

Alichem

Product number: 39775310
Product name: Dimethyl[2,2'-bipyridine]-3,3'-dicarboxylate
Packaging: 10g
Price: $520
Updated: 2021/12/16

Arctom

Product number: AS446049
Product name: Dimethyl[2,2'-bipyridine]-3,3'-dicarboxylate
Purity: 97%
Packaging: 10g
Price: $394
Updated: 2021/12/16

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2,2'-Bipyridine-3,3'-dicarboxylic acid dimethyl ester Chemical Properties,Usage,Production

Synthesis

67-56-1

4479-74-7

39775-31-0

2,2'-Bipyridine-3,3'-dicarboxylic acid (3 g, 12.3 mmol) was dissolved in methanol (300 mL) at 0 °C, followed by addition of N,N'-dicyclohexylcarbodiimide (DCC, 12 g, 58.2 mmol). The reaction mixture was stirred at 0 °C for 3 h. The solid by-products were removed by filtration. The filtrate was concentrated and the resulting residue was washed several times with pentane to remove impurities. Finally, the product was purified by gel chromatography (eluent: dichloromethane mixed with methanol in a ratio of 99:1) to afford the target compound dimethyl [2,2'-bipyridyl]-3,3'-dicarboxylate (2.87 g, 85% yield).

References

[1] Tetrahedron Letters, 2013, vol. 54, # 8, p. 840 - 842

2,2'-Bipyridine-3,3'-dicarboxylic acid dimethyl ester Preparation Products And Raw materials

Raw materials

Preparation Products

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2,2'-Bipyridine-3,3'-dicarboxylic acid dimethyl ester Suppliers

China 55 India 1 United States 3 Global 59

ZhengZhou HuaWen Chemical Co.Ltd

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View Lastest Price from 2,2'-Bipyridine-3,3'-dicarboxylic acid dimethyl ester manufacturers

Shanghai UCHEM Inc.

Product: 2,2'-Bipyridine-3,3'-dicarboxylic acid dimethyl ester 39775-31-0
Price: US $68.00-415.00/g
Min. Order: 5g
Purity: 0.98
Supply Ability: 10kg
Release date: 2023-11-27

Career Henan Chemical Co

Product: 2,2'-Bipyridine-3,3'-dicarboxylic acid dimethyl ester 39775-31-0
Price: US $1.00/KG
Min. Order: 1KG
Purity: Min98% HPLC
Supply Ability: g/kg/ton
Release date: 2019-12-25

39775-31-0, 2,2'-Bipyridine-3,3'-dicarboxylic acid dimethyl esterRelated Search:

diethyl 2,2'-bipyridine-5,5'-dicarboxylate 2,2'-Bipyridine-5,5'-dicarboxylic acid DIMETHYL 2,2'-BIPYRIDINE-6,6'-DICARBOXYLATE 4,4'-Bis(methoxycarbonly)-2,2'-bipyridine diethyl [2,2'-bipyridine]-3,3'-dicarboxylate 3,3'-DIMETHYL-2,2'-BIPYRIDINE 2,2'-Bipyridine-4,4'-dicarboxylic acid 5,5'-DIMETHYL-2,2'-DIPYRIDYL 4,4'-Bis(hydroxymethyl)-2,2'-bipyridine 6,6'-Dimethyl-2,2'-dipyridyl [2,2'-Bipyridine]-5,5'-diMethanol 4,4'-Dimethyl-2,2'-bipyridyl 2,2'-Bipyridyl-5,5'-dialdehyde DIETHYL 2,2'-BIPYRIDINE-6,6'-DICARBOXYLATE 5,5'-diMethoxycarbonyl-2,2'-bipyridine 6,6′-bis(hydroxymethyl)-2,2′-bipyridine 2,2'-BIPYRIDINE-6,6'-DICARBOXYLIC ACID 2,2'-Bipyridine-3,3'-dicarboxylic acid

2,2'-Bipyridine-3,3'-dicarboxylic acid dimethyl ester

2,2'-Bipyridinyl-3,3'-dicarboxylic acid diMethyl ester

3,3'-bis(methoxycarbonyl)-2,2'-bipyridine

diMethyl 2,2'-bipyridine-3,3'-dicarboxylate

[2,2'-Bipyridine]-3,3'-dicarboxylic acid, 3,3'-dimethyl ester

2,2'-Bipyridine-3,3'-dicarboxylic acid dimethyl ester3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester

methyl2-(3-methoxycarbonylpyridin-2-yl)pyridine-3-carboxylate

Dimethyl [2,2'-bipyridine]-3,3'-dicarboxylate

2, 2'-Bipyridine-3, 3'-dicarboxylic acid dimethyl ester

[2,2'-Bipyridine]-3,3'-dicarboxylicacid, 3,3'-dimethyl ester

(2,2')BIPYRIDINYL-3,3'-DICARBOXYLIC ACID DIMETHYL ESTER

39775-31-0