ChemicalBook > CAS DataBase List > 5-CHLORO-2-METHOXYBENZALDEHYDE

5-CHLORO-2-METHOXYBENZALDEHYDE

Product Name: 5-CHLORO-2-METHOXYBENZALDEHYDE
CAS No.: 7035-09-8
Chemical Name: 5-CHLORO-2-METHOXYBENZALDEHYDE
Synonyms: AKOS B014153;ASISCHEM R42152;ART-CHEM-BB B014153;CHEMBRDG-BB 3014153;5-Chloro-2-Anisaldehyde;5-CHLORO-2-METHOXYBENZALDEHYDE;Benzaldehyde, 5-chloro-2-methoxy-;2-Bromo-5-(trifluoromethyl)acetophenone;JR-13439, 5-Chloro-2-methoxybenzaldehyde, 97%;5-chloro-2-methoxybenzaldehyde(SALTDATA: FREE)
CBNumber: CB6214511
Molecular Formula: C8H7ClO2
Formula Weight: 170.59
MOL File: 7035-09-8.mol

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5-CHLORO-2-METHOXYBENZALDEHYDE Property

Melting point:: 75-79℃
Boiling point:: 152 °C(Press: 15 Torr)
Density: 1.244±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
form: solid
Appearance: White to light yellow Solid
Sensitive: Air Sensitive
InChI: InChI=1S/C8H7ClO2/c1-11-8-3-2-7(9)4-6(8)5-10/h2-5H,1H3
InChIKey: HXTWDGGMXZXOIV-UHFFFAOYSA-N
SMILES: C(=O)C1=CC(Cl)=CC=C1OC
CAS DataBase Reference: 7035-09-8(CAS DataBase Reference)

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Safety

Hazard Codes: Xi,Xn
Risk Statements: 22-36-51
Safety Statements: 26
WGK Germany: 3
HazardClass: IRRITANT
HS Code: 2913000090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: CDS005116
Product name: 5-Chloro-2-methoxybenzaldehyde
Purity: AldrichCPR
Packaging: 100mg
Price: $70.9
Updated: 2024/03/01

TRC

Product number: C596573
Product name: 5-Chloro-2-methoxybenzaldehyde
Packaging: 2.5g
Price: $90
Updated: 2021/12/16

Matrix Scientific

Product number: 015723
Product name: 5-Chloro-2-methoxybenzaldehyde
Purity: 95%
Packaging: 1g
Price: $25
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC70984
Product name: 5-Chloro-2-methoxybenzaldehyde
Packaging: 10g
Price: $50
Updated: 2021/12/16

Matrix Scientific

Product number: 015723
Product name: 5-Chloro-2-methoxybenzaldehyde
Purity: 95%
Packaging: 5g
Price: $60
Updated: 2021/12/16

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5-CHLORO-2-METHOXYBENZALDEHYDE Chemical Properties,Usage,Production

Synthesis Reference(s)

Synthetic Communications, 19, p. 799, 1989 DOI: 10.1080/00397918908050996

Synthesis

635-93-8

74-88-4

7035-09-8

Step 1: Preparation of 5-chloro-2-methoxybenzaldehyde 5-Chloro-2-hydroxybenzaldehyde (20 g, 128 mmol) was dissolved in N,N-dimethylformamide (DMF, 70 mL) and the solution was cooled to 5-10 °C. Sodium hydride (7.69 g, 192 mmol) was added to the solution in small portions over 20 min. Subsequently, iodomethane (23.8 mL, 384 mmol) was added dropwise while keeping the temperature of the reaction mixture below 15 °C. After addition, the reaction mixture was stirred at room temperature for 2 hours. Upon completion of the reaction, the mixture was poured into pre-cooled saturated ammonium chloride solution (250 mL) and a white precipitate precipitated. The precipitate was collected by filtration and dried under vacuum. The resulting solid was ground with a solvent mixture of pentane and ether (4:1, 100 mL) to afford 18 g (82.58% yield) of the target product, 5-chloro-2-methoxybenzaldehyde, as a white solid.LC-MS analysis showed m/z = 170.1 ([M+H]+).

References

[1] Chemical Communications, 2011, vol. 47, # 9, p. 2679 - 2681
[2] Journal of Medicinal Chemistry, 2013, vol. 56, # 12, p. 5019 - 5032
[3] Bioorganic and Medicinal Chemistry, 2016, vol. 24, # 12, p. 2768 - 2776
[4] Patent: WO2014/151472, 2014, A1. Location in patent: Paragraph 00392-00393
[5] Patent: WO2016/40315, 2016, A1. Location in patent: Paragraph 00435; 00436

5-CHLORO-2-METHOXYBENZALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

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5-CHLORO-2-METHOXYBENZALDEHYDE Suppliers

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View Lastest Price from 5-CHLORO-2-METHOXYBENZALDEHYDE manufacturers

PUSHAN INDUSTRIAL (SHAANXI) CO.,LTD

Product: 5-Chloro-2-methoxybenzaldehyde 7035-09-8
Price: US $0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 2 MTs
Release date: 2024-08-06

Shaanxi Dideu New Materials Co. Ltd

Product: 5-CHLORO-2-METHOXYBENZALDEHYDE 7035-09-8
Price: US $0.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 10000KGS
Release date: 2025-02-22

7035-09-8, 5-CHLORO-2-METHOXYBENZALDEHYDERelated Search:

3-BROMO-5-CHLORO-2,6-DIMETHOXYBENZAMIDE 5-CHLORO-BENZOFURAN-3-ONE 5-Chloro-2-methoxybenzoic acid 2-Ethoxy-4-amino-5-chlorobenzoic acid Clebopride maleate METHYL 5-CHLORO-2-METHOXYBENZOATE (+)-Griseofulvin 6-CHLOROCHROMAN-4-ONE 6,8-DICHLORO-3-FORMYLCHROMONE 5-CHLORO-2-METHOXYBENZALDEHYDE Glibenclamide 3-BROMO-5-CHLORO-2,6-DIMETHOXYBENZOIC ACID Methyl 4-acetamido-5-chloro-2-methoxybenzoate 3-CHLORO-4-METHOXYBENZALDEHYDE 3-CHLORO-2-METHOXYBENZALDEHYDE 2-CHLORO-6-METHOXY-BENZALDEHYDE 2-CHLORO-3-METHOXYBENZALDEHYDE,98.0+%(GC) Metoclopramide monohydrochloride monohydrate

CHEMBRDG-BB 3014153

ART-CHEM-BB B014153

ASISCHEM R42152

JR-13439, 5-Chloro-2-methoxybenzaldehyde, 97%

5-CHLORO-2-METHOXYBENZALDEHYDE

AKOS B014153

5-chloro-2-methoxybenzaldehyde(SALTDATA: FREE)

Benzaldehyde, 5-chloro-2-methoxy-

5-Chloro-2-Anisaldehyde

2-Bromo-5-(trifluoromethyl)acetophenone

7035-09-8

7039-09-8

1875772

7035-9-8

Aromatic Aldehydes & Derivatives (substituted)

Benzaldehyde

Adehydes, Acetals & Ketones

Anisoles, Alkyloxy Compounds & Phenylacetates

Chlorine Compounds