ChemicalBook > CAS DataBase List > 2,6-DICHLORO-4-METHOXY-PYRIDINE

2,6-DICHLORO-4-METHOXY-PYRIDINE

Product Name
2,6-DICHLORO-4-METHOXY-PYRIDINE
CAS No.
17228-75-0
Chemical Name
2,6-DICHLORO-4-METHOXY-PYRIDINE
Synonyms
4-Methoxy-2,6-dichloropyridine;2,6-DICHLORO-4-METHOXY-PYRIDINE;Pyridine, 2,6-dichloro-4-methoxy-;2,6-Dichloro-4-methoxypyridine 99%
CBNumber
CB62446547
Molecular Formula
C6H5Cl2NO
Formula Weight
178.02
MOL File
17228-75-0.mol
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2,6-DICHLORO-4-METHOXY-PYRIDINE Property

Boiling point:
255.0±35.0 °C(Predicted)
Density 
1.363±0.06 g/cm3(Predicted)
storage temp. 
Inert atmosphere,Room Temperature
pka
-0.91±0.10(Predicted)
form 
solid
color 
White to off-white
InChI
InChI=1S/C6H5Cl2NO/c1-10-4-2-5(7)9-6(8)3-4/h2-3H,1H3
InChIKey
MMQWWYZZOZBFHY-UHFFFAOYSA-N
SMILES
C1(Cl)=NC(Cl)=CC(OC)=C1
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Safety

HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
D437270
Product name
2,6-Dichloro-4-methoxypyridine
Packaging
100mg
Price
$60
Updated
2021/12/16
AK Scientific
Product number
Y7807
Product name
2,6-Dichloro-4-methoxypyridine
Packaging
100mg
Price
$74
Updated
2021/12/16
AK Scientific
Product number
Y7807
Product name
2,6-Dichloro-4-methoxypyridine
Packaging
250mg
Price
$82
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD144045
Product name
2,6-Dichloro-4-methoxypyridine
Packaging
500mg
Price
$90
Updated
2021/12/16
ChemScene
Product number
CS-W021523
Product name
2,6-Dichloro-4-methoxypyridine
Purity
99.37%
Packaging
1g
Price
$42
Updated
2021/12/16
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2,6-DICHLORO-4-METHOXY-PYRIDINE Chemical Properties,Usage,Production

Synthesis

67-56-1

16063-69-7

17228-75-0

To a solution of 2,4,6-trichloropyridine (3.64 g, 20.0 mmol) in DMF (20 mL) was slowly added NaH (60% dispersed in mineral oil, 840 mg, 21 mmol) and methanol (673 mg, 21 mmol) at 0 °C. The reaction mixture was stirred at room temperature for 16 hours. Upon completion of the reaction, the mixture was concentrated and partitioned between ethyl acetate (30 mL) and water (15 mL). The organic layer was dried over anhydrous sodium sulfate, filtered and concentrated. The residue was purified by silica gel column chromatography to afford 2,6-dichloro-4-methoxypyridine (3.0 g, yield: 94%) using ethyl acetate (0-5%) in hexane as eluent.

References

[1] Patent: WO2018/106459, 2018, A1. Location in patent: Paragraph 00110
[2] Bioorganic and Medicinal Chemistry, 2017, vol. 25, # 15, p. 3947 - 3963

2,6-DICHLORO-4-METHOXY-PYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2,6-DICHLORO-4-METHOXY-PYRIDINE manufacturers

Career Henan Chemical Co
Product
2,6-DICHLORO-4-METHOXY-PYRIDINE 17228-75-0
Price
US $9.80/KG
Min. Order
1g
Purity
≥99%
Supply Ability
100kg
Release date
2020-01-08

17228-75-0, 2,6-DICHLORO-4-METHOXY-PYRIDINERelated Search:

2,6-Dichloro-4-ethoxypyridine 2-chloro-4-pyridone 2,6-DICHLORO-4-HYDROXYPYRIDINE 2-Chloro-4-methoxypyridine 2,6-DICHLORO-4-METHOXY-PYRIDINE

  • 2,6-DICHLORO-4-METHOXY-PYRIDINE
  • 4-Methoxy-2,6-dichloropyridine
  • 2,6-Dichloro-4-methoxypyridine 99%
  • Pyridine, 2,6-dichloro-4-methoxy-
  • 17228-75-0