ChemicalBook > CAS DataBase List > 1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE

1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE

Product Name: 1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE
CAS No.: 67938-76-5
Chemical Name: 1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE
Synonyms: (5-Chloropyridin-2-yl);5-Chloro-2-pyridinemethanamine;2-Aminomethyl-5-chloropyridine;(5-chloro-2-pyridyl)methanamine;2-Pyridinemethanamine, 5-chloro-;1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE;C-(5-Chloro-pyridin-2-yl)-MethylaMine;2-Aminomethyl-5-chloropyridine hydrochloride;1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE ISO 9001：2015 REACH
CBNumber: CB62454490
Molecular Formula: C6H7ClN2
Formula Weight: 142.59
MOL File: 67938-76-5.mol

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1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE Property

Boiling point:: 216.2±25.0 °C(Predicted)
Density: 1.244±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
solubility: Chloroform (Slightly), Methanol (Slightly)
pka: 8.31±0.39(Predicted)
form: Low-Melting Solid
color: Pale Yellow to Light Yellow

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Safety

Hazard Codes: T
Risk Statements: 25
Safety Statements: 45
HS Code: 2933399090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H301Toxic if swalloed

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.

P321Specific treatment (see … on this label).

P330Rinse mouth.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: C596263
Product name: (5-Chloropyridin-2-yl)methanamine
Packaging: 25mg
Price: $45
Updated: 2021/12/16

TRC

Product number: C596263
Product name: (5-Chloropyridin-2-yl)methanamine
Packaging: 50mg
Price: $60
Updated: 2021/12/16

TRC

Product number: C596263
Product name: (5-Chloropyridin-2-yl)methanamine
Packaging: 250mg
Price: $75
Updated: 2021/12/16

AK Scientific

Product number: 7855BB
Product name: (5-Chloropyridin-2-YL)methanamine
Packaging: 1g
Price: $208
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0064047
Product name: (5-CHLOROPYRIDIN-2-YL)METHANAMINE
Purity: 95.00%
Packaging: 5G
Price: $2752.94
Updated: 2021/12/16

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1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE Chemical Properties,Usage,Production

Synthesis

89809-64-3

67938-76-5

The general procedure for the synthesis of 2-aminomethyl-5-chloropyridine from 5-chloro-2-cyanopyridine was as follows: 5-chloropyridinecarbonitrile (3.8 g, 27.43 mmol) was dissolved in ethanol (100 mL), and concentrated HCl (3 mL) and 10% Pd-C catalyst (1.0 g) were added. The reaction mixture was shaken under hydrogen atmosphere (40 psi) for 2 hours. After completion of the reaction, the catalyst was removed by filtration and the filtrate was concentrated. The obtained residue was dissolved in saturated NaHCO3 solution (50 mL) and extracted with dichloromethane (4 x 25 mL). The organic phases were combined, dried with anhydrous Na2SO4, filtered and concentrated to afford 2-aminomethyl-5-chloropyridine as a yellow oil (2.0 g, 51% yield). The product was analyzed by LCMS showing a (M + H)+ peak of 143.07 (calculated value: 143.04, C6H8ClN2).1HNMR (500 MHz, CDCl3) δ ppm: 8.56-8.51 (1H, br d), 7.66-7.60 (1H, m), 7.28-7.14 (1H, m), 3.97 (2H. s), 1.72 (2H, s).

References

[1] Patent: US2005/267105, 2005, A1. Location in patent: Page/Page column 63
[2] Patent: US2007/111984, 2007, A1. Location in patent: Page/Page column 29
[3] Patent: US2007/129379, 2007, A1. Location in patent: Page/Page column 21-22
[4] Patent: WO2007/64316, 2007, A1. Location in patent: Page/Page column 140 - 141

1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE Suppliers

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View Lastest Price from 1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE manufacturers

Dideu Industries Group Limited

Product: 1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE 67938-76-5
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons min
Release date: 2021-09-03

Career Henan Chemical Co

Product: 1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE 67938-76-5
Price: US $7.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100kg
Release date: 2020-02-18

67938-76-5, 1-(5-CHLOROPYRIDIN-2-YL)METHANAMINERelated Search:

LAZABEMIDE 3-AMINO-5-CHLOROPYRIDINE-2-CARBOXAMIDE N-(2-Aminoethyl)-5-chlor-2-pyridincarboxamid-hydrochlorid 5-CHLORO-3-NITROPYRIDINE-2-CARBOXAMIDE SALOR-INT L120766-1EA 4-AMINO-3,5,6-TRICHLOROPYRIDINE-2-CARBOHYDRAZIDE C-(5-CHLORO-4-METHYL-PYRIDIN-2-YL)-METHYLAMINE 4-AMINO-3,5,6-TRICHLOROPYRIDINE-2-CARBOXAMIDE RARECHEM AL BW 1601 4-AMINO-3,5-DICHLORO-6-HYDRAZINO-PYRIDINE-2-CARBOXYLIC ACID HYDRAZIDE RARECHEM AL BW 1815 RARECHEM AL BW 1664 RARECHEM AL BW 1502 4-AMINO-3,5-DICHLOROPYRIDINE-2-CARBOXAMIDE 5-CHLORO-3-(HYDROXYMETHYL)-6-METHOXYPYRIDINE-2-CARBOXAMIDE RARECHEM AL BW 2483 3,5-dichloropyridine-2-carboxamidine 3,4,5-TRICHLOROPYRIDINE-2-CARBOXAMIDE

1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE

2-Aminomethyl-5-chloropyridine

2-Aminomethyl-5-chloropyridine hydrochloride

C-(5-Chloro-pyridin-2-yl)-MethylaMine

5-Chloro-2-pyridinemethanamine

(5-Chloropyridin-2-yl)

(5-chloro-2-pyridyl)methanamine

2-Pyridinemethanamine, 5-chloro-

1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE ISO 9001：2015 REACH

67938-76-5

C6H72N2HCl

Building Blocks

Pyridine