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1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE

Product Name
1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE
CAS No.
67938-76-5
Chemical Name
1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE
Synonyms
(5-Chloropyridin-2-yl);5-Chloro-2-pyridinemethanamine;2-Aminomethyl-5-chloropyridine;(5-chloro-2-pyridyl)methanamine;2-Pyridinemethanamine, 5-chloro-;1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE;C-(5-Chloro-pyridin-2-yl)-MethylaMine;2-Aminomethyl-5-chloropyridine hydrochloride;1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE ISO 9001：2015 REACH
CBNumber
CB62454490
Molecular Formula
C6H7ClN2
Formula Weight
142.59
MOL File
67938-76-5.mol
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1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE Property

Boiling point:
216.2±25.0 °C(Predicted)
Density 
1.244±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
solubility 
Chloroform (Slightly), Methanol (Slightly)
pka
8.31±0.39(Predicted)
form 
Low-Melting Solid
color 
Pale Yellow to Light Yellow
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Safety

Hazard Codes 
T
Risk Statements 
25
Safety Statements 
45
HS Code 
2933399090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H301Toxic if swalloed

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.

P321Specific treatment (see … on this label).

P330Rinse mouth.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC
Product number
C596263
Product name
(5-Chloropyridin-2-yl)methanamine
Packaging
25mg
Price
$45
Updated
2021/12/16
TRC
Product number
C596263
Product name
(5-Chloropyridin-2-yl)methanamine
Packaging
50mg
Price
$60
Updated
2021/12/16
TRC
Product number
C596263
Product name
(5-Chloropyridin-2-yl)methanamine
Packaging
250mg
Price
$75
Updated
2021/12/16
AK Scientific
Product number
7855BB
Product name
(5-Chloropyridin-2-YL)methanamine
Packaging
1g
Price
$208
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0064047
Product name
(5-CHLOROPYRIDIN-2-YL)METHANAMINE
Purity
95.00%
Packaging
5G
Price
$2752.94
Updated
2021/12/16
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1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE Chemical Properties,Usage,Production

Synthesis

89809-64-3

67938-76-5

The general procedure for the synthesis of 2-aminomethyl-5-chloropyridine from 5-chloro-2-cyanopyridine was as follows: 5-chloropyridinecarbonitrile (3.8 g, 27.43 mmol) was dissolved in ethanol (100 mL), and concentrated HCl (3 mL) and 10% Pd-C catalyst (1.0 g) were added. The reaction mixture was shaken under hydrogen atmosphere (40 psi) for 2 hours. After completion of the reaction, the catalyst was removed by filtration and the filtrate was concentrated. The obtained residue was dissolved in saturated NaHCO3 solution (50 mL) and extracted with dichloromethane (4 x 25 mL). The organic phases were combined, dried with anhydrous Na2SO4, filtered and concentrated to afford 2-aminomethyl-5-chloropyridine as a yellow oil (2.0 g, 51% yield). The product was analyzed by LCMS showing a (M + H)+ peak of 143.07 (calculated value: 143.04, C6H8ClN2).1HNMR (500 MHz, CDCl3) δ ppm: 8.56-8.51 (1H, br d), 7.66-7.60 (1H, m), 7.28-7.14 (1H, m), 3.97 (2H. s), 1.72 (2H, s).

References

[1] Patent: US2005/267105, 2005, A1. Location in patent: Page/Page column 63
[2] Patent: US2007/111984, 2007, A1. Location in patent: Page/Page column 29
[3] Patent: US2007/129379, 2007, A1. Location in patent: Page/Page column 21-22
[4] Patent: WO2007/64316, 2007, A1. Location in patent: Page/Page column 140 - 141

1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE Suppliers

China 63 India 1 Ukraine 2 United States 10 Global 76
A.J Chemicals
Tel
--
Fax
--
Email
sales@ajchem.in
Country
India
ProdList
6100
Advantage
58
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View Lastest Price from 1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE manufacturers

Dideu Industries Group Limited
Product
1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE 67938-76-5
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons min
Release date
2021-09-03
Career Henan Chemical Co
Product
1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE 67938-76-5
Price
US $7.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
100kg
Release date
2020-02-18

67938-76-5, 1-(5-CHLOROPYRIDIN-2-YL)METHANAMINERelated Search:

LAZABEMIDE 3-AMINO-5-CHLOROPYRIDINE-2-CARBOXAMIDE N-(2-Aminoethyl)-5-chlor-2-pyridincarboxamid-hydrochlorid 5-CHLORO-3-NITROPYRIDINE-2-CARBOXAMIDE SALOR-INT L120766-1EA 4-AMINO-3,5,6-TRICHLOROPYRIDINE-2-CARBOHYDRAZIDE C-(5-CHLORO-4-METHYL-PYRIDIN-2-YL)-METHYLAMINE 4-AMINO-3,5,6-TRICHLOROPYRIDINE-2-CARBOXAMIDE RARECHEM AL BW 1601 4-AMINO-3,5-DICHLORO-6-HYDRAZINO-PYRIDINE-2-CARBOXYLIC ACID HYDRAZIDE RARECHEM AL BW 1815 RARECHEM AL BW 1664 RARECHEM AL BW 1502 4-AMINO-3,5-DICHLOROPYRIDINE-2-CARBOXAMIDE 5-CHLORO-3-(HYDROXYMETHYL)-6-METHOXYPYRIDINE-2-CARBOXAMIDE RARECHEM AL BW 2483 3,5-dichloropyridine-2-carboxamidine 3,4,5-TRICHLOROPYRIDINE-2-CARBOXAMIDE

  • 1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE
  • 2-Aminomethyl-5-chloropyridine
  • 2-Aminomethyl-5-chloropyridine hydrochloride
  • C-(5-Chloro-pyridin-2-yl)-MethylaMine
  • 5-Chloro-2-pyridinemethanamine
  • (5-Chloropyridin-2-yl)
  • (5-chloro-2-pyridyl)methanamine
  • 2-Pyridinemethanamine, 5-chloro-
  • 1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE ISO 9001：2015 REACH
  • 67938-76-5
  • C6H72N2HCl
  • Building Blocks
  • Pyridine