6-CHLORO-2,2'-BIPYRIDINE

Product Name: 6-CHLORO-2,2'-BIPYRIDINE
CAS No.: 13040-77-2
Chemical Name: 6-CHLORO-2,2'-BIPYRIDINE
Synonyms: 6-Chloro-2,2'-bipyridyl;2-CHLORO-2,2'-BIPYRIDINE;6-Chloro-2, 2'-bipyridyl;6-chloro-2,2'-bipyridine;2,2'-Bipyridine, 6-chloro-;2-chloro-6-(pyridin-2-yl)pyridine
CBNumber: CB62456555
Molecular Formula: C10H7ClN2
Formula Weight: 190.63
MOL File: 13040-77-2.mol

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6-CHLORO-2,2'-BIPYRIDINE Property

Melting point:: 62℃
Boiling point:: 320.6±27.0 °C(Predicted)
Density: 1.245±0.06 g/cm3 (20 ºC 760 Torr)
storage temp.: Inert atmosphere,Room Temperature
pka: 3.72±0.22(Predicted)
Appearance: Off-white to light yellow Solid
InChI: InChI=1S/C10H7ClN2/c11-10-6-3-5-9(13-10)8-4-1-2-7-12-8/h1-7H
InChIKey: XRCUTZKABNKOEY-UHFFFAOYSA-N
SMILES: C1(C2=NC=CC=C2)=NC(Cl)=CC=C1

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P330Rinse mouth.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: C365358
Product name: 6-Chloro-2,2''-bipyridine
Packaging: 50mg
Price: $200
Updated: 2021/12/16

AK Scientific

Product number: 4440BB
Product name: 6-Chloro-2,2'-bipyridine
Packaging: 1g
Price: $404
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0367895
Product name: 6-CHLORO-2,2'-BIPYRIDINE
Purity: 95.00%
Packaging: 1G
Price: $853.65
Updated: 2021/12/16

Ambeed

Product number: A260267
Product name: 6-Chloro-2,2'-bipyridine
Purity: 95+%
Packaging: 100mg
Price: $23
Updated: 2021/12/16

Ambeed

Product number: A260267
Product name: 6-Chloro-2,2'-bipyridine
Purity: 95+%
Packaging: 250mg
Price: $44
Updated: 2021/12/16

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6-CHLORO-2,2'-BIPYRIDINE Chemical Properties,Usage,Production

Synthesis

2402-78-0

17997-47-6

13040-77-2

Step 1: 2,6-Dichloropyridine (11) (8.88 g, 60.0 mmol) and 2-(tributylmethylstannyl)pyridine (7.36 g, 20.0 mmol) were dissolved in anhydrous toluene (74 mL) under nitrogen protection. To this solution was added tetrakis(triphenylphosphine)palladium (2.31 g, 2.0 mmol), followed by heating the reaction mixture to reflux and stirring for 11 hours. Upon completion of the reaction, the mixture was concentrated under reduced pressure and the residue was purified by silica gel column chromatography to afford the target product 6-chloro-2,2'-bipyridine (12) (3.9 g, quantitative yield). The structure of the product was confirmed by 1H-NMR (DMSO-d6): δ 7.50-7.53 (m, 1H), 7.59 (d, 1H, J = 8.0 Hz), 7.93-8.05 (m, 2H), 8.30 (d, 1H, J = 8.0 Hz), 8.38 (d, 1H, J = 8.0 Hz), 8.72 (d, 1H, J = 4.4 Hz ).

References

[1] Patent: EP2280000, 2011, A1. Location in patent: Page/Page column 34-35
[2] Patent: US2011/28468, 2011, A1. Location in patent: Page/Page column 22
[3] Organic and Biomolecular Chemistry, 2007, vol. 5, # 9, p. 1397 - 1404

6-CHLORO-2,2'-BIPYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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6-CHLORO-2,2'-BIPYRIDINE Suppliers

China 65 India 1 Switzerland 3 United Kingdom 1 United States 2 Global 72

Shenzhen Gre-syn Chemical Technology Co., Ltd.

Tel: 0755-0755-89366401 18617066401
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Tel: 0757-82582588
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Tel: 0371-0371-13526885213 15637198702
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Shanghai Kangman Biological Technology Co., Ltd.

Tel: 18800375331
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Zhengzhou JACS Chemical Co., Ltd.

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View Lastest Price from 6-CHLORO-2,2'-BIPYRIDINE manufacturers

Shanghai UCHEM Inc.

Product: 2-Chloro-2,2'-bipyridine 13040-77-2
Price: US $55.00-189.00/g
Min. Order: 1g
Purity: 0.98
Supply Ability: 25kg
Release date: 2024-04-12

Career Henan Chemical Co

Product: 6-CHLORO-2,2'-BIPYRIDINE 13040-77-2
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200kg
Release date: 2020-01-09

13040-77-2, 6-CHLORO-2,2'-BIPYRIDINERelated Search:

3,5,6-Trichloropyrid 4,6'-DICHLORO-2,2'-BIPYRIDINE 6,6'-Dichloro-2,2'-bipyridine 6-CHLORO-2,2'-BIPYRIDINE 6-CHLORO-[2,2']BIPYRIDINYL-5-CARBONITRILE 6-CHLORO-2,2'-BIPYRIDINE N'-OXIDE

2-CHLORO-2,2'-BIPYRIDINE

6-Chloro-2,2'-bipyridyl

2-chloro-6-(pyridin-2-yl)pyridine

2,2'-Bipyridine, 6-chloro-

6-chloro-2,2'-bipyridine

6-Chloro-2, 2'-bipyridyl

13040-77-2