ChemicalBook > CAS DataBase List > 6-CHLORO-2,2'-BIPYRIDINE
6-CHLORO-2,2'-BIPYRIDINE
- Product Name
- 6-CHLORO-2,2'-BIPYRIDINE
- CAS No.
- 13040-77-2
- Chemical Name
- 6-CHLORO-2,2'-BIPYRIDINE
- Synonyms
- 6-Chloro-2,2'-bipyridyl;2-CHLORO-2,2'-BIPYRIDINE;6-Chloro-2, 2'-bipyridyl;6-chloro-2,2'-bipyridine;2,2'-Bipyridine, 6-chloro-;2-chloro-6-(pyridin-2-yl)pyridine
- CBNumber
- CB62456555
- Molecular Formula
- C10H7ClN2
- Formula Weight
- 190.63
- MOL File
- 13040-77-2.mol
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6-CHLORO-2,2'-BIPYRIDINE Property
- Melting point:
- 62℃
- Boiling point:
- 320.6±27.0 °C(Predicted)
- Density
- 1.245±0.06 g/cm3 (20 ºC 760 Torr)
- storage temp.
- Inert atmosphere,Room Temperature
- pka
- 3.72±0.22(Predicted)
- Appearance
- Off-white to light yellow Solid
- InChI
- InChI=1S/C10H7ClN2/c11-10-6-3-5-9(13-10)8-4-1-2-7-12-8/h1-7H
- InChIKey
- XRCUTZKABNKOEY-UHFFFAOYSA-N
- SMILES
- C1(C2=NC=CC=C2)=NC(Cl)=CC=C1
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P501Dispose of contents/container to..…
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N-Bromosuccinimide Price
TRC
- Product number
- C365358
- Product name
- 6-Chloro-2,2''-bipyridine
- Packaging
- 50mg
- Price
- $200
- Updated
- 2021/12/16
AK Scientific
- Product number
- 4440BB
- Product name
- 6-Chloro-2,2'-bipyridine
- Packaging
- 1g
- Price
- $404
- Updated
- 2021/12/16
American Custom Chemicals Corporation
- Product number
- HCH0367895
- Product name
- 6-CHLORO-2,2'-BIPYRIDINE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $853.65
- Updated
- 2021/12/16
Chemenu
- Product number
- CM174267
- Product name
- 6-chloro-2,2''-bipyridine
- Purity
- 95%
- Packaging
- 5g
- Price
- $1477
- Updated
- 2021/12/16
Crysdot
- Product number
- CD11297932
- Product name
- 6-Chloro-2,2'-bipyridine
- Purity
- 95+%
- Packaging
- 5g
- Price
- $1565
- Updated
- 2021/12/16
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6-CHLORO-2,2'-BIPYRIDINE Chemical Properties,Usage,Production
Synthesis
2402-78-0
17997-47-6
13040-77-2
Step 1: 2,6-Dichloropyridine (11) (8.88 g, 60.0 mmol) and 2-(tributylmethylstannyl)pyridine (7.36 g, 20.0 mmol) were dissolved in anhydrous toluene (74 mL) under nitrogen protection. To this solution was added tetrakis(triphenylphosphine)palladium (2.31 g, 2.0 mmol), followed by heating the reaction mixture to reflux and stirring for 11 hours. Upon completion of the reaction, the mixture was concentrated under reduced pressure and the residue was purified by silica gel column chromatography to afford the target product 6-chloro-2,2'-bipyridine (12) (3.9 g, quantitative yield). The structure of the product was confirmed by 1H-NMR (DMSO-d6): δ 7.50-7.53 (m, 1H), 7.59 (d, 1H, J = 8.0 Hz), 7.93-8.05 (m, 2H), 8.30 (d, 1H, J = 8.0 Hz), 8.38 (d, 1H, J = 8.0 Hz), 8.72 (d, 1H, J = 4.4 Hz ).
References
[1] Patent: EP2280000, 2011, A1. Location in patent: Page/Page column 34-35
[2] Patent: US2011/28468, 2011, A1. Location in patent: Page/Page column 22
[3] Organic and Biomolecular Chemistry, 2007, vol. 5, # 9, p. 1397 - 1404
6-CHLORO-2,2'-BIPYRIDINE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 6-CHLORO-2,2'-BIPYRIDINE manufacturers
Shanghai UCHEM Inc.
- Product
- 2-Chloro-2,2'-bipyridine 13040-77-2
- Price
- US $55.00-189.00/g
- Min. Order
- 1g
- Purity
- 0.98
- Supply Ability
- 25kg
- Release date
- 2024-04-12
Career Henan Chemical Co
- Product
- 6-CHLORO-2,2'-BIPYRIDINE 13040-77-2
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 200kg
- Release date
- 2020-01-09
13040-77-2, 6-CHLORO-2,2'-BIPYRIDINERelated Search:
3,5,6-Trichloropyrid
4,6'-DICHLORO-2,2'-BIPYRIDINE
6,6'-Dichloro-2,2'-bipyridine
6-CHLORO-2,2'-BIPYRIDINE
6-CHLORO-[2,2']BIPYRIDINYL-5-CARBONITRILE
6-CHLORO-2,2'-BIPYRIDINE N'-OXIDE