ChemicalBook > CAS DataBase List > 6-Iodo-1H-quinolin-2-one

6-Iodo-1H-quinolin-2-one

Product Name: 6-Iodo-1H-quinolin-2-one
CAS No.: 99455-01-3
Chemical Name: 6-Iodo-1H-quinolin-2-one
Synonyms: 6-Iodoquinolin-2-o;6-Iodoquinolin-2-ol;6-Iodo-2(1H)- quinolone;6-iodo-2(1H)-Quinolinone;6-Iodo-1H-quinolin-2-one;2(1H)-Quinolinone, 6-iodo-
CBNumber: CB62484767
Molecular Formula: C9H6INO
Formula Weight: 271.05
MOL File: 99455-01-3.mol

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6-Iodo-1H-quinolin-2-one Property

Melting point:: 260-263 °C
Boiling point:: 413.1±45.0 °C(Predicted)
Density: 1.880
storage temp.: 2-8°C(protect from light)
pka: 10.92±0.70(Predicted)
Appearance: Yellow to brown Solid

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Safety

HS Code: 2933499090

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

AK Scientific

Product number: W9873
Product name: 6-Iodoquinolin-2-ol
Packaging: 250mg
Price: $100
Updated: 2021/12/16

Matrix Scientific

Product number: 146508
Product name: 6-Iodo-1H-quinolin-2-one
Purity: 95%
Packaging: 1g
Price: $225
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0368143
Product name: 6-IODOQUINOLIN-2-OL
Purity: 95.00%
Packaging: 1G
Price: $484.05
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H56-H-61
Product name: 6-Iodoquinolin-2(1H)-one
Packaging: 1g
Price: $661
Updated: 2021/12/16

Matrix Scientific

Product number: 146508
Product name: 6-Iodo-1H-quinolin-2-one
Purity: 95%
Packaging: 5g
Price: $665
Updated: 2021/12/16

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6-Iodo-1H-quinolin-2-one Chemical Properties,Usage,Production

Synthesis

99465-20-0

99455-01-3

(2E)-3-(ethoxy)-N-(4-iodophenyl)-2-acrylamide (33 g, 104 mmol) was added batchwise to stirred concentrated sulfuric acid (300 mL) at 0 °C. The reaction mixture was stirred continuously for 2 hours at room temperature. Subsequently, the reaction mixture was quenched by slowly pouring it into about 1 kg of ice. The resulting solid product was collected by filtration and washed sequentially with water (3 times) and acetonitrile (2 times). Finally, the solid was dried under vacuum to afford 6-iodo-2-hydroxyquinoline as an off-white solid (27.1 g, yield: 96%). The structure of the product was confirmed by 1H NMR (400 MHz, chloroform-d) and ES-LCMS: 1H NMR δ= 6.73 (d, J = 9.6Hz, 1H), 7.17 (d, J = 8.8Hz, 1H), 7.74 (d, J = 9.6Hz, 1H), 7.77 (dd, J = 8.8,1.4Hz, 1H), 7.93 ( d, J = 1.4 Hz, 1H); ES-LCMS: m/z 272 (M + 1).

References

[1] Patent: WO2012/37108, 2012, A1. Location in patent: Page/Page column 134
[2] Patent: US2006/63804, 2006, A1. Location in patent: Page/Page column 9
[3] Journal of Medicinal Chemistry, 1988, vol. 31, # 10, p. 2048 - 2056
[4] Patent: US4728654, 1988, A

6-Iodo-1H-quinolin-2-one Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 6-Iodo-1H-quinolin-2-one manufacturers

Career Henan Chemical Co

Product: 6-Iodo-1H-quinolin-2-one 99455-01-3
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100kg
Release date: 2019-07-05

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