Methyl 5-(3-Bromophenyl)isoxazole-3-carboxylate

Product Name: Methyl 5-(3-Bromophenyl)isoxazole-3-carboxylate
CAS No.: 745078-74-4
Chemical Name: Methyl 5-(3-Bromophenyl)isoxazole-3-carboxylate
Synonyms: Methyl 5-(3-Bromophenyl)isoxazole-3-;Methyl 5-(3-Bromophenyl)isoxazole-3-carboxylate;5-(3-Bromophenyl)-3-isoxazolecarboxylic acid methyl ester;5-(3-Bromophenyl)isoxazole-3-carboxylic acid methyl ester;5-(3-bromophenyl)-3-Isoxazole carbocylic acid methyl ester;3-Isoxazolecarboxylic acid, 5-(3-bromophenyl)-, methyl ester
CBNumber: CB62535713
Molecular Formula: C11H8BrNO3
Formula Weight: 282.09
MOL File: 745078-74-4.mol

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Methyl 5-(3-Bromophenyl)isoxazole-3-carboxylate Property

Boiling point:: 405.4±35.0 °C(Predicted)
Density: 1.526±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: -6.52±0.38(Predicted)
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: M295978
Product name: Methyl5-(3-Bromophenyl)isoxazole-3-carboxylate
Packaging: 250mg
Price: $140
Updated: 2021/12/16

AK Scientific

Product number: 7092AJ
Product name: Methyl5-(3-bromophenyl)isoxazole-3-carboxylate
Packaging: 1g
Price: $263
Updated: 2021/12/16

Matrix Scientific

Product number: 181020
Product name: 5-(3-Bromophenyl)-isoxazole-3-carboxylic acid methyl ester
Purity: 95%+
Packaging: 1g
Price: $580
Updated: 2021/12/16

AK Scientific

Product number: 7092AJ
Product name: Methyl5-(3-bromophenyl)isoxazole-3-carboxylate
Packaging: 5g
Price: $771
Updated: 2021/12/16

Advanced Chemicals Intermediatesced Chemicals Intermediates

Product number: ACI-04874
Product name: 5-(3-Bromo-phenyl)-isoxazole-3-carboxylicacidmethylester
Purity: 95%+
Packaging: 5g
Price: $978.75
Updated: 2021/12/16

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Methyl 5-(3-Bromophenyl)isoxazole-3-carboxylate Chemical Properties,Usage,Production

Synthesis

93618-22-5

745078-74-4

Methyl 2,4-dioxo-4-(3-bromophenyl)butyrate (10.3 g, 36.1 mmol) was used as a raw material and suspended in anhydrous methanol (100 mL). To this suspension was added hydroxylamine hydrochloride (3.8 g, 54.2 mmol). The reaction mixture was heated to reflux for 90 minutes. Upon completion of the reaction, the mixture was cooled to room temperature and an ice/water mixture (200 mL) was added. After continued stirring for 20 minutes, the mixture was filtered through a Brinell funnel and washed with cold water. The resulting light yellow solid was dried in a vacuum oven to give methyl 5-(3-bromophenyl)isoxazole-3-carboxylate (8.9 g, 87% yield).

References

[1] Patent: US2004/167188, 2004, A1
[2] Patent: US2004/214870, 2004, A1. Location in patent: Page 18

Methyl 5-(3-Bromophenyl)isoxazole-3-carboxylate Preparation Products And Raw materials

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View Lastest Price from Methyl 5-(3-Bromophenyl)isoxazole-3-carboxylate manufacturers

Career Henan Chemical Co

Product: Methyl 5-(3-Bromophenyl)isoxazole-3-carboxylate 745078-74-4
Price: US $0.01/KG
Min. Order: 500g
Purity: 98%; 99%
Supply Ability: 500g；1kg； 10kg; 25kg
Release date: 2020-01-08

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745078-74-4