ChemicalBook > CAS DataBase List > Methyl 5-bromo-2-chloroisonicotinate
Methyl 5-bromo-2-chloroisonicotinate
- Product Name
- Methyl 5-bromo-2-chloroisonicotinate
- CAS No.
- 886365-28-2
- Chemical Name
- Methyl 5-bromo-2-chloroisonicotinate
- Synonyms
- Methyl 5-bromo-2-chloroisonicotite;Methyl 5-bromo-2-chloroisonicotinate;Methyl 5-bromo-2-chloroisonicotinate 98%;Methyl 5-bromo-2-chloropyridine-4-carboxylate;methyl 5-bromo-2-chloro-4-pyridinecarboxylate;5-bromo-2-chloro-3-methyl-4-pyridinecarboxylate;5-bromo-2-chloro-pyridin-4-carboxylic acid methyl ester;5-Bromo-2-chloro-4-pyridinecarboxylic acid methyl ester;4-Pyridinecarboxylic acid, 5-broMo-2-chloro-, Methyl ester;Methyl 5-bromo-2-chloropyridine-4-carboxylate, 5-Bromo-2-chloro-4-(methoxycarbonyl)pyridine
- CBNumber
- CB9956465
- Molecular Formula
- C7H5BrClNO2
- Formula Weight
- 250.48
- MOL File
- 886365-28-2.mol
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Methyl 5-bromo-2-chloroisonicotinate Property
- Boiling point:
- 286.5±35.0℃ (760 Torr)
- Density
- 1.684±0.06 g/cm3 (20 ºC 760 Torr)
- Flash point:
- 127.1±25.9℃
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- -3.54±0.10(Predicted)
- Appearance
- Off-white to light yellow Solid-liquid mixture
- InChI
- InChI=1S/C7H5BrClNO2/c1-12-7(11)4-2-6(9)10-3-5(4)8/h2-3H,1H3
- InChIKey
- ZGVAWYBJGMOKBV-UHFFFAOYSA-N
- SMILES
- C1(Cl)=NC=C(Br)C(C(OC)=O)=C1
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Safety
- Hazard Codes
- Xi
- HazardClass
- IRRITANT
- HS Code
- 2933399990
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N-Bromosuccinimide Price
TRC
- Product number
- M295880
- Product name
- Methyl5-bromo-2-chloroisonicotinate
- Packaging
- 250mg
- Price
- $55
- Updated
- 2021/12/16
SynQuest Laboratories
- Product number
- 4H23-D-X5
- Product name
- Methyl 5-bromo-2-chloroisonicotinate
- Packaging
- 250mg
- Price
- $38
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 056425
- Product name
- Methyl 5-bromo-2-chloropyridine-4-carboxylate
- Purity
- >95%
- Packaging
- 500mg
- Price
- $80
- Updated
- 2021/12/16
SynQuest Laboratories
- Product number
- 4H23-D-X5
- Product name
- Methyl 5-bromo-2-chloroisonicotinate
- Packaging
- 1g
- Price
- $110
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 056425
- Product name
- Methyl 5-bromo-2-chloropyridine-4-carboxylate
- Purity
- >95%
- Packaging
- 1g
- Price
- $160
- Updated
- 2021/12/16
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Methyl 5-bromo-2-chloroisonicotinate Chemical Properties,Usage,Production
Synthesis
To a 5000 mL three-necked flask, add 3500 mL of the above already prepared methanol solution of hydrogen chloride, 350 g of 5-bromo-2-chloroisonicotinic acid, raise the temperature to 40??C and stir the reaction, track the reaction by liquid chromatography, and stop the reaction when the product, methyl 5-bromo-2-chloroisonicotinate, is greater than 85% by liquid chromatography, and the content of the methyl 5-bromo-2-methoxyisonicotinate by-product (3) is less than 1%. Reaction. Neutralize the system with solid sodium bicarbonate to neutral under stirring, filter, drain, rinse the filter cake with methanol, combine the filtrates and concentrate to obtain a brownish-red liquid 320 g, high vacuum distillation, collect 40-60 Pa, 70-75 ?? fractions, obtain a colorless liquid 5-bromo-2-chloroisonicotinic acid methyl ester (296 g), content of 98.9%.
Methyl 5-bromo-2-chloroisonicotinate Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from Methyl 5-bromo-2-chloroisonicotinate manufacturers
Career Henan Chemical Co
- Product
- Methyl 5-bromo-2-chloroisonicotinate 886365-28-2
- Price
- US $2.00/KG
- Min. Order
- 1g
- Purity
- 98%min
- Supply Ability
- ask
- Release date
- 2020-01-08
886365-28-2, Methyl 5-bromo-2-chloroisonicotinateRelated Search:
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3-BROMOISONICOTINIC ACID METHYL ESTER
SPECS AO-801/41077570