ChemicalBook > CAS DataBase List > Methyl 5-(3-Bromophenyl)isoxazole-3-carboxylate
Methyl 5-(3-Bromophenyl)isoxazole-3-carboxylate
- Product Name
- Methyl 5-(3-Bromophenyl)isoxazole-3-carboxylate
- CAS No.
- 745078-74-4
- Chemical Name
- Methyl 5-(3-Bromophenyl)isoxazole-3-carboxylate
- Synonyms
- Methyl 5-(3-Bromophenyl)isoxazole-3-;Methyl 5-(3-Bromophenyl)isoxazole-3-carboxylate;5-(3-Bromophenyl)-3-isoxazolecarboxylic acid methyl ester;5-(3-Bromophenyl)isoxazole-3-carboxylic acid methyl ester;5-(3-bromophenyl)-3-Isoxazole carbocylic acid methyl ester;3-Isoxazolecarboxylic acid, 5-(3-bromophenyl)-, methyl ester
- CBNumber
- CB62535713
- Molecular Formula
- C11H8BrNO3
- Formula Weight
- 282.09
- MOL File
- 745078-74-4.mol
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Methyl 5-(3-Bromophenyl)isoxazole-3-carboxylate Property
- Boiling point:
- 405.4±35.0 °C(Predicted)
- Density
- 1.526±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- -6.52±0.38(Predicted)
- Appearance
- White to off-white Solid
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N-Bromosuccinimide Price
TRC
- Product number
- M295978
- Product name
- Methyl5-(3-Bromophenyl)isoxazole-3-carboxylate
- Packaging
- 250mg
- Price
- $140
- Updated
- 2021/12/16
AK Scientific
- Product number
- 7092AJ
- Product name
- Methyl5-(3-bromophenyl)isoxazole-3-carboxylate
- Packaging
- 1g
- Price
- $263
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 181020
- Product name
- 5-(3-Bromophenyl)-isoxazole-3-carboxylic acid methyl ester
- Purity
- 95%+
- Packaging
- 1g
- Price
- $580
- Updated
- 2021/12/16
AK Scientific
- Product number
- 7092AJ
- Product name
- Methyl5-(3-bromophenyl)isoxazole-3-carboxylate
- Packaging
- 5g
- Price
- $771
- Updated
- 2021/12/16
Ambeed
- Product number
- A128612
- Product name
- Methyl5-(3-bromophenyl)isoxazole-3-carboxylate
- Purity
- 97%
- Packaging
- 250mg
- Price
- $47
- Updated
- 2021/12/16
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Methyl 5-(3-Bromophenyl)isoxazole-3-carboxylate Chemical Properties,Usage,Production
Synthesis
93618-22-5
745078-74-4
Methyl 2,4-dioxo-4-(3-bromophenyl)butyrate (10.3 g, 36.1 mmol) was used as a raw material and suspended in anhydrous methanol (100 mL). To this suspension was added hydroxylamine hydrochloride (3.8 g, 54.2 mmol). The reaction mixture was heated to reflux for 90 minutes. Upon completion of the reaction, the mixture was cooled to room temperature and an ice/water mixture (200 mL) was added. After continued stirring for 20 minutes, the mixture was filtered through a Brinell funnel and washed with cold water. The resulting light yellow solid was dried in a vacuum oven to give methyl 5-(3-bromophenyl)isoxazole-3-carboxylate (8.9 g, 87% yield).
References
[1] Patent: US2004/167188, 2004, A1
[2] Patent: US2004/214870, 2004, A1. Location in patent: Page 18
Methyl 5-(3-Bromophenyl)isoxazole-3-carboxylate Preparation Products And Raw materials
Raw materials
Preparation Products
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Methyl 5-(3-Bromophenyl)isoxazole-3-carboxylate Suppliers
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View Lastest Price from Methyl 5-(3-Bromophenyl)isoxazole-3-carboxylate manufacturers
Career Henan Chemical Co
- Product
- Methyl 5-(3-Bromophenyl)isoxazole-3-carboxylate 745078-74-4
- Price
- US $0.01/KG
- Min. Order
- 500g
- Purity
- 98%; 99%
- Supply Ability
- 500g；1kg； 10kg; 25kg
- Release date
- 2020-01-08
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