Benzofuro[3,2-d]pyriMidine-2,4(1H,3H)-dione

Product Name: Benzofuro[3,2-d]pyriMidine-2,4(1H,3H)-dione
CAS No.: 62208-68-8
Chemical Name: Benzofuro[3,2-d]pyriMidine-2,4(1H,3H)-dione
Synonyms: BNZOFURO[3,2-D]PYRIMIDINE-2,4(1H,3H)-DIONE;1H-[1]benzofuro[3,2-d]pyrimidine-2,4-dione;Benzofuro[3,2-d]pyriMidine-2,4(1H,3H)-dione;1H-Benzo[4,5]furo[3,2-D]pyrimidine-2,4-dione
CBNumber: CB62723305
Molecular Formula: C10H6N2O3
Formula Weight: 202.17
MOL File: 62208-68-8.mol

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Benzofuro[3,2-d]pyriMidine-2,4(1H,3H)-dione Property

storage temp.: Inert atmosphere,Room Temperature
Appearance: Off-white to light yellow Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

Ambeed

Product number: A103238
Product name: Benzofuro[3,2-d]pyrimidine-2,4(1H,3H)-dione
Purity: 95%
Packaging: 250mg
Price: $15
Updated: 2021/12/16

Ambeed

Product number: A103238
Product name: Benzofuro[3,2-d]pyrimidine-2,4(1H,3H)-dione
Purity: 95%
Packaging: 1g
Price: $35
Updated: 2021/12/16

Ambeed

Product number: A103238
Product name: Benzofuro[3,2-d]pyrimidine-2,4(1H,3H)-dione
Purity: 95%
Packaging: 5g
Price: $107
Updated: 2021/12/16

Alichem

Product number: 62208688
Product name: Benzofuro[3,2-d]pyrimidine-2,4(1H,3H)-dione
Packaging: 1g
Price: $218
Updated: 2021/12/16

Ambeed

Product number: A103238
Product name: Benzofuro[3,2-d]pyrimidine-2,4(1H,3H)-dione
Purity: 95%
Packaging: 25g
Price: $370
Updated: 2021/12/16

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Benzofuro[3,2-d]pyriMidine-2,4(1H,3H)-dione Chemical Properties,Usage,Production

Synthesis

886950-29-4

62208-68-8

Ethyl 2-carbamoylbenzofuran-3-ylcarbamate (114 mg, 0.460 mmol, 1.0 eq.) was heated to reflux for 1 h in 5% NaOH solution (3.7 mL, 4.60 mmol, 10.0 eq.) and EtOH (2.2 mL). Upon completion of the reaction, the mixture was cooled to room temperature and the product was precipitated by addition of 37% HCl solution. The solid was collected by filtration and washed sequentially with water and ether. The resulting benzofuro[3,2-d]pyrimidine-2,4(1H,3H)-dione (40 mg, 43% yield) could be used in the next step of the reaction without further purification. The product was characterized as follows: 1H-NMR (500 MHz, DMSO): δ 12.03 (s, 1H), 11.43 (s, 1H), 8.00 (d, 3JHH = 7.3 Hz, 1H), 7.75 (d, 3JHH = 8.5 Hz, 1H), 7.64 (t, 3JHH = 7.3 Hz, 1H), 7.45 (t, 3JHH = 7.3 Hz, 1H), 7.45 (t, 3JHH = 7.3 Hz). 3JHH = 7.3 Hz, 1H); 13C-NMR (100 MHz, DMSO): δ 155.5, 154.9, 151.3, 133.3, 130.6, 129.8, 123.9, 121.6, 117.6, 112.9.

References

[1] Patent: WO2010/52569, 2010, A2. Location in patent: Page/Page column 242

Benzofuro[3,2-d]pyriMidine-2,4(1H,3H)-dione Preparation Products And Raw materials

Raw materials

Preparation Products

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Benzofuro[3,2-d]pyriMidine-2,4(1H,3H)-dione Suppliers

China 22 India 1 United States 2 Global 25

Bide Pharmatech Ltd.

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Rhawn Reagent

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Suzhou Rovathin Foreign Trade Co.,Ltd

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Taizhou Nanfeng Pharmaceutical Research Institute

Tel: nanfengdrug@163.com; 18616377689
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62208-68-8, Benzofuro[3,2-d]pyriMidine-2,4(1H,3H)-dioneRelated Search:

Sulfadimethoxine sodium salt 1H-BENZOIMIDAZOLE-4-CARBOXYLIC ACID 4-Benzothiazolecarboxaldehyde 7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzo[b]furan Benzothiazole-5-carboxylic acid BENZOFURAN-5-BORONIC ACID BENZOFURAN-3-BORONIC ACID

Benzofuro[3,2-d]pyriMidine-2,4(1H,3H)-dione

1H-Benzo[4,5]furo[3,2-D]pyrimidine-2,4-dione

1H-[1]benzofuro[3,2-d]pyrimidine-2,4-dione

BNZOFURO[3,2-D]PYRIMIDINE-2,4(1H,3H)-DIONE

62208-68-8