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4-Ethylphenylhydrazine hydrochloride

Product Name
4-Ethylphenylhydrazine hydrochloride
CAS No.
53661-18-0
Chemical Name
4-Ethylphenylhydrazine hydrochloride
Synonyms
BIO-FARMA BF001075;TIMTEC-BB SBB005537;IFLAB-BB F1371-0140;3-BROMOPYRIDIN-4-AMINE;3-BROMO-4-PYRIDINEAMINE;3-BROMO-4-PYRIDINYLAMINE;3-BROMO-PYRIDIN-4-YLAMINE;4-ETHYLPHENYLHYDRAZINE HCL;4-ETHYLPHENYLHYDRAZINE HYDROCHLORIDE;1-(4-ETHYLPHENYL)HYDRAZINE HYDROCHLORIDE
CBNumber
CB6314585
Molecular Formula
C8H13ClN2
Formula Weight
172.66
MOL File
53661-18-0.mol
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4-Ethylphenylhydrazine hydrochloride Property

Melting point:
67-71 °C
storage temp. 
Sealed in dry,Room Temperature
Appearance
White to off-white Solid
CAS DataBase Reference
53661-18-0(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
37/39-26-24/25
Hazard Note 
Irritant
HazardClass 
IRRITANT, IRRITANT-HARMFUL
HS Code 
29280000
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TRC
Product number
E926058
Product name
4-Ethylphenylhydrazinehydrochloride
Packaging
100mg
Price
$45
Updated
2021/12/16
TRC
Product number
E926058
Product name
4-Ethylphenylhydrazinehydrochloride
Packaging
500mg
Price
$65
Updated
2021/12/16
Usbiological
Product number
275692
Product name
4-Ethylphenylhydrazine Hydrochloride
Packaging
1g
Price
$363
Updated
2021/12/16
Oakwood
Product number
023498
Product name
4-Ethylphenylhydrazinehydrochloride
Purity
95%
Packaging
250mg
Price
$10
Updated
2021/12/16
Oakwood
Product number
023498
Product name
4-Ethylphenylhydrazinehydrochloride
Purity
95%
Packaging
1g
Price
$14
Updated
2021/12/16
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4-Ethylphenylhydrazine hydrochloride Chemical Properties,Usage,Production

Uses

4-Ethylphenylhydrazine, HCl

Synthesis

589-16-2

53661-18-0

The general procedure for the synthesis of 4-ethylphenylhydrazine hydrochloride from 4-ethylaniline is as follows: 150 mL of deionized water and 160 mL of 12 N hydrochloric acid were added to a reaction flask containing 24.2 g (0.2 mol) of 4-ethylaniline. After cooling the reaction mixture to 0°C, 14 g (0.2 mol) of sodium nitrite solution dissolved in 140 mL of water was added slowly and dropwise. The reaction temperature was maintained at 0 °C and after 1 h, 112 g (0.496 mol) of stannous chloride dihydrate solution pre-dissolved in 90 mL of 12 N hydrochloric acid was added to the reaction mixture, controlling the temperature of the reaction not to exceed 10 °C during the addition process. After the addition, the reaction was continued with stirring at 10 °C for 1.5 h. The reaction mixture was cooled to 0 °C and then filtered. Upon completion of the reaction, the reaction mixture was filtered and the brown solid product was collected with a measured melting point of 198°C and 95% yield.

References

[1] Patent: US2004/43995, 2004, A1. Location in patent: Page 13
[2] Journal of Medicinal Chemistry, 1999, vol. 42, # 3, p. 526 - 531
[3] Journal of the Chinese Chemical Society, 2018, vol. 65, # 5, p. 538 - 547
[4] European Journal of Medicinal Chemistry, 2018, vol. 156, p. 137 - 147

4-Ethylphenylhydrazine hydrochloride Preparation Products And Raw materials

Raw materials

Preparation Products

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4-Ethylphenylhydrazine hydrochloride Suppliers

Specs
Tel
--
Fax
--
Email
info@specs.net
Country
The Netherlands
ProdList
6833
Advantage
70
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View Lastest Price from 4-Ethylphenylhydrazine hydrochloride manufacturers

Career Henan Chemical Co
Product
4-Ethylphenylhydrazine hydrochloride 53661-18-0
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
1kg-1000kg
Release date
2020-01-02

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