4-HYDROXY-B-NITROSTYRENE
- Product Name
- 4-HYDROXY-B-NITROSTYRENE
- CAS No.
- 3179-08-6
- Chemical Name
- 4-HYDROXY-B-NITROSTYRENE
- Synonyms
- 4-(2-Nitrovinyl)phenol;4-Hydroxy--nitrostyrene;4-HYDROXY-B-NITROSTYRENE;4-Hydroxy-β-Nitrostyrene;Phenol, 4-(2-nitroethenyl)-;4-HYDROXY-BETA-NITROSTYRENE;4'-HYDROXY-BETA-NITROSTYRENE;4-Hydroxy-alpha-nitrostyrene;2-(4-HYDROXYPHENYL)NITROETHENE;TRANS-4-HYDROXY-BETA-NITROSTYRENE
- CBNumber
- CB6324179
- Molecular Formula
- C8H7NO3
- Formula Weight
- 165.15
- MOL File
- 3179-08-6.mol
4-HYDROXY-B-NITROSTYRENE Property
- Melting point:
- 167-171 °C(lit.)
- Boiling point:
- 318.3±17.0 °C(Predicted)
- Density
- 1.320±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- 8.04±0.13(Predicted)
- Appearance
- Yellow to brown Solid
- InChI
- InChI=1S/C8H7NO3/c10-8-3-1-7(2-4-8)5-6-9(11)12/h1-6,10H
- InChIKey
- CTJKRKMPTRJAIT-UHFFFAOYSA-N
- SMILES
- C1(O)=CC=C(C=C[N+]([O-])=O)C=C1
- CAS DataBase Reference
- 3179-08-6(CAS DataBase Reference)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 126612
- Product name
- 4-(2-Nitrovinyl)phenol
- Purity
- >95%
- Packaging
- 1g
- Price
- $28
- Updated
- 2021/12/16
- Product number
- 126612
- Product name
- 4-(2-Nitrovinyl)phenol
- Purity
- >95%
- Packaging
- 5g
- Price
- $82
- Updated
- 2021/12/16
- Product number
- 126612
- Product name
- 4-(2-Nitrovinyl)phenol
- Purity
- >95%
- Packaging
- 10g
- Price
- $144
- Updated
- 2021/12/16
- Product number
- J56748
- Product name
- 4-(2-Nitrovinyl)phenol
- Packaging
- 25g
- Price
- $197
- Updated
- 2021/12/16
- Product number
- J56748
- Product name
- 4-(2-Nitrovinyl)phenol
- Packaging
- 10g
- Price
- $100
- Updated
- 2021/12/16
4-HYDROXY-B-NITROSTYRENE Chemical Properties,Usage,Production
Synthesis
7400-08-0
3179-08-6
General procedure for the synthesis of 4-(2-nitrovinyl)phenol from 4-hydroxycinnamic acid: 0.01 mol of 4-hydroxycinnamic acid, about 0.01 mol of TCICA/DMF reagent, 1 g of sodium nitrite, and 25 mL of CH2Cl2 or acetonitrile were added to a pre-cleaned round-bottomed flask with stirring and the reaction was carried out under refluxing conditions for 8 to 10 hours. The progress of the reaction was monitored by TLC. Upon completion of the reaction, the reaction mixture was washed with NaHCO3 solution and subsequently extracted with ethyl acetate. The organic layer was separated, dried with anhydrous MgSO4 and concentrated in vacuum. Finally, purification by column chromatography using ethyl acetate-hexane as eluent gave the pure product 4-(2-nitrovinyl)phenol as a yellow powder.
References
[1] Synthetic Communications, 2013, vol. 43, # 19, p. 2672 - 2677
[2] Catalysis Science and Technology, 2016, vol. 6, # 5, p. 1430 - 1434
[3] Synthesis and Reactivity in Inorganic, Metal-Organic and Nano-Metal Chemistry, 2013, vol. 43, # 8, p. 977 - 983
[4] Synthetic Communications, 2015, vol. 45, # 19, p. 2251 - 2258
4-HYDROXY-B-NITROSTYRENE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-HYDROXY-B-NITROSTYRENE manufacturers
- Product
- 4-HYDROXY-B-NITROSTYRENE 3179-08-6
- Price
- US $1.00/Kg
- Min. Order
- 1Kg
- Purity
- 98%
- Supply Ability
- 20T
- Release date
- 2024-07-08
- Product
- 4-Hydroxy-β-nitrostyrene 3179-08-6
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- 97%
- Supply Ability
- 100kg
- Release date
- 2020-01-09