ChemicalBook > CAS DataBase List > 2-CHLORO-3-CYANOQUINOLINE

2-CHLORO-3-CYANOQUINOLINE

Product Name: 2-CHLORO-3-CYANOQUINOLINE
CAS No.: 95104-21-5
Chemical Name: 2-CHLORO-3-CYANOQUINOLINE
Synonyms: AKOS BB-7566;2-CHLORO-3-CYANOQUINOLINE;2-Chloro-3-quinolinecarbonitrile;2-CHLOROQUINOLINE-3-CARBONITRILE;3-Quinolinecarbonitrile,2-chloro-;2-CHLORO-3-CYANOQUINOLINE ISO 9001：2015 REACH
CBNumber: CB6324593
Molecular Formula: C10H5ClN2
Formula Weight: 188.61
MOL File: 95104-21-5.mol

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2-CHLORO-3-CYANOQUINOLINE Property

Melting point:: 164-168 °C
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
form: solid
Appearance: White to off-white Solid
InChI: InChI=1S/C10H5ClN2/c11-10-8(6-12)5-7-3-1-2-4-9(7)13-10/h1-5H
InChIKey: UGTRDMPALMEDBU-UHFFFAOYSA-N
SMILES: C1C=C2C(N=C(Cl)C(C#N)=C2)=CC=1

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Safety

Hazard Codes: Xn
Risk Statements: 22-41
Safety Statements: 26
RIDADR: UN 2811 6.1/PG 3
WGK Germany: 3
HS Code: 2933499090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H301Toxic if swalloed

H318Causes serious eye damage

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 687790
Product name: 2-Chloroquinoline-3-carbonitrile
Purity: 97%
Packaging: 250mg
Price: $101
Updated: 2023/01/07

Sigma-Aldrich

Product number: 687790
Product name: 2-Chloroquinoline-3-carbonitrile
Purity: 97%
Packaging: 1g
Price: $196
Updated: 2023/01/07

TRC

Product number: C385125
Product name: 2-Chloroquinoline-3-carbonitrile
Packaging: 500mg
Price: $265
Updated: 2021/12/16

TRC

Product number: C385125
Product name: 2-Chloroquinoline-3-carbonitrile
Packaging: 50mg
Price: $45
Updated: 2021/12/16

Apolloscientific

Product number: OR307835
Product name: 2-Chloroquinoline-3-carbonitrile
Packaging: 1g
Price: $269
Updated: 2021/12/16

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2-CHLORO-3-CYANOQUINOLINE Chemical Properties,Usage,Production

Synthesis

73568-25-9

95104-21-5

General procedure for the synthesis of 2-chloro-3-cyanoquinoline from 2-chloro-3-quinolinecarboxaldehyde: 2-chloroquinoline-3-carboxaldehyde (0.01 mol) was suspended in 30% ammonia (30 mL) and stirred at room temperature for 5 min to form a turbid solution. Stirring was continued at 0 °C and ceric ammonium nitrate (0.01 mol) was slowly added. The reaction process was monitored by thin layer chromatography (TLC) and the reaction time was about 10-15 minutes. After completion of the reaction, the reaction mixture was extracted with a solvent mixture of chloroform-ethyl acetate (5:3 v/v). The organic phase was dried with anhydrous sodium sulfate and concentrated under reduced pressure to give the crude product. The crude product was recrystallized by ethanol to give pure 2-chloro-3-cyanoquinoline as light yellow crystals in 82% yield.

References

[1] Synlett, 2009, # 20, p. 3378 - 3382
[2] Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005, vol. 44, # 9, p. 1868 - 1875
[3] Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006, vol. 45, # 1, p. 292 - 296
[4] Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2009, vol. 48, # 1, p. 152 - 154
[5] Bioorganic and Medicinal Chemistry, 2015, vol. 23, # 3, p. 602 - 611

2-CHLORO-3-CYANOQUINOLINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-CHLORO-3-CYANOQUINOLINE manufacturers

Career Henan Chemical Co

Product: 2-CHLORO-3-CYANOQUINOLINE 95104-21-5
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: KG/T
Release date: 2019-12-20

95104-21-5, 2-CHLORO-3-CYANOQUINOLINERelated Search:

AKOS BB-7566

2-CHLOROQUINOLINE-3-CARBONITRILE

2-CHLORO-3-CYANOQUINOLINE

3-Quinolinecarbonitrile,2-chloro-

2-CHLORO-3-CYANOQUINOLINE ISO 9001：2015 REACH

2-Chloro-3-quinolinecarbonitrile

95104-21-5

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