ChemicalBook > CAS DataBase List > 5-Nitro-2-furaldehyde diacetate

5-Nitro-2-furaldehyde diacetate

Product Name: 5-Nitro-2-furaldehyde diacetate
CAS No.: 92-55-7
Chemical Name: 5-Nitro-2-furaldehyde diacetate
Synonyms: 5-NITROFURFURAL DIACETATE;5-Nitro-2-furaL;5-NITROFURFURYLIDENE DIACETATE;5-NITRO-2-FURFURALDEHYDE DIACETATE;IITR01324;Nifuratel-1;dehyde diacetate;Nifuratel impurity C;Nifuratel impuritiesA;Nifuroxazide Impurity C
CBNumber: CB6328551
Molecular Formula: C9H9NO7
Formula Weight: 243.17
MOL File: 92-55-7.mol

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5-Nitro-2-furaldehyde diacetate Property

Melting point:: 89-93 °C
Boiling point:: 386.04°C (rough estimate)
Density: 1.5301 (rough estimate)
refractive index: 1.5800 (estimate)
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
solubility: Chloroform (Slightly), Methanol (Very Slightly)
form: Fine Crystalline Powder
color: Yellow
Sensitive: Light Sensitive
BRN: 255089
InChI: InChI=1S/C9H9NO7/c1-5(11)15-9(16-6(2)12)7-3-4-8(17-7)10(13)14/h3-4,9H,1-2H3
InChIKey: HSXKWKJCZNRMJO-UHFFFAOYSA-N
SMILES: C(OC(=O)C)(OC(=O)C)C1=CC=C([N+]([O-])=O)O1
LogP: 1.06 at 20℃
CAS DataBase Reference: 92-55-7(CAS DataBase Reference)
NIST Chemistry Reference: 2-(Diacetoxymethyl)-5-nitrofuran(92-55-7)
EPA Substance Registry System: Methanediol, (5-nitro-2-furanyl)-, diacetate (ester) (92-55-7)

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Safety

Hazard Codes: Xn
Risk Statements: 68-40-20/21/22
Safety Statements: 24/25-36-22-45-36/37/39-7
RTECS: LU1940000
TSCA: Yes
HS Code: 29321900

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H341Suspected of causing genetic defects

Precautionary statements

P201Obtain special instructions before use.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P308+P313IF exposed or concerned: Get medical advice/attention.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: Y0001570
Product name: Nitrofural impurity B
Purity: European Pharmacopoeia (EP) Reference Standard
Packaging: 30 mg
Price: $156
Updated: 2025/07/31

Sigma-Aldrich

Product number: R427055
Product name: 5-NITRO-2-FURALDEHYDE DIACETATE
Purity: Aldrich<sup>CPR</sup>
Packaging: 1 unit
Price: $185
Updated: 2025/07/31

Sigma-Aldrich

Product number: PHR2456
Product name: Nitrofurfural diacetate
Purity: Pharmaceutical Secondary Standard; Certified Reference Material
Packaging: 200MG
Price: $502
Updated: 2025/07/31

Sigma-Aldrich

Product number: 1465503
Product name: Nitrofurfural diacetate
Purity: United States Pharmacopeia (USP) Reference Standard
Packaging: 100mg
Price: $1300
Updated: 2025/07/31

Sigma-Aldrich

Product number: Y0001570
Product name: Nitrofural impurity B
Purity: European Pharmacopoeia (EP) Reference Standard
Packaging: y0001570
Price: $153
Updated: 2024/03/01

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5-Nitro-2-furaldehyde diacetate Chemical Properties,Usage,Production

Chemical Properties

yellow fine crystalline powder

Uses

5-Nitrofuraldehyde Diacetate (cas# 92-55-7) is a compound useful in organic synthesis.

Synthesis

98-01-1

108-24-7

92-55-7

GENERAL STEPS: A premixed solution of concentrated nitric acid (8.6 mL, 12.2 g, 193.62 mmol) and concentrated sulfuric acid (0.06 mL, 1.1 g, 11.2 mmol) was slowly added dropwise under stirring conditions to acetic anhydride (90 mL) at 0 °C. Subsequently, freshly distilled 2-furancarboxaldehyde (10.4 mL, 12.06 g, 125.5 mmol) was added dropwise to the above reaction mixture over 45 minutes and stirring was continued at 0 °C for 1 hour. Upon completion of the reaction, water (100 mL) was added to the mixture and stirred at room temperature for 30 min to promote the formation of a white precipitate. Next, the pH of the reaction mixture was adjusted to about 2.5 with 10% NaOH solution, followed by heating the mixture at 50 °C for 1 hour. After the reaction solution was cooled to room temperature, the white precipitate formed was collected by filtration, washed with water, and finally recrystallized by anhydrous ethanol and dried to afford 5-nitrofurfural diacetate (Product 2) in a yield of 24.84 g in 82% yield.

References

[1] Asian Journal of Chemistry, 2018, vol. 30, # 2, p. 312 - 316
[2] Journal of Organic Chemistry, 2018, vol. 83, # 8, p. 4427 - 4440
[3] Industrial and Engineering Chemistry, 1955, vol. 47, p. 358,359
[4] Kagaku Kenkyusho Hokoku, 1955, vol. 31, p. 430,434
[5] Chem.Abstr., 1956, p. 15504

5-Nitro-2-furaldehyde diacetate Preparation Products And Raw materials

Raw materials

p-Toluenesulfonic acid Acetic anhydride Sodium sulfate Diethyl ether Ethyl acetate Sodium bicarbonate Nitric acid Sodium hydroxide Pyridine Furfural PETROLEUM ETHER Sulfuric acid

Preparation Products

Nitrofurantoin

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View Lastest Price from 5-Nitro-2-furaldehyde diacetate manufacturers

WUHAN FORTUNA CHEMICAL CO., LTD

Product: 5-Nitro-2-furaldehyde diacetate 92-55-7
Price: US $0.00-0.00/Kg/Drum
Min. Order: 1KG
Purity: 98%min
Supply Ability: 1000kg
Release date: 2021-11-18

Hangzhou Verychem Science And Technology Co.Ltd

Product: 5-Nitro-2-furaldehyde diacetate 92-55-7
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 99%min
Supply Ability: 20 TONS
Release date: 2025-02-06

Shaanxi Dideu Medichem Co. Ltd

Product: 5-Nitro-2-furaldehyde diacetate 92-55-7
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 99.0%
Supply Ability: 1000KG
Release date: 2024-08-08

92-55-7, 5-Nitro-2-furaldehyde diacetateRelated Search:

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(ACETYLOXY)(5-NITRO-2-FURYL)METHYL ACETATE

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Nifuratel Impurity A (Nitrofurfural Diacetate)

Furazolidone Impurit :5-Nitro-2-furaldehyde diacetate

Nifuratel-1

5-nitro-2-furanmethandioldiacetate

5-Nitro-2-furaldehyde diacetate, 98+%

Methanediol, 1-(5-nitro-2-furanyl)-, 1,1-diacetate

(5-nitrofuran-2-yl)Methylene diacetate

Nitrofurfural diacetate

Nitrofural impurity B

5-nitro-furfural diethyl

5-NITROFURFURAL DIACETATEFURAZOLIDONE

5-Nitro-2-pyrpryoldiacetate

2-Nitro-5-(diacetoxymethyl)furan

5-Nitrofuran-2-methanediol diacetate

Diacetic acid (5-nitro-2-furyl)methylene

Diacetic acid (5-nitro-2-furyl)methylene ester

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5-Nitro-2-furfurylidene Diacetate

2-(Diacetoxymethyl)-5-nitrofuran 5-Nitrofurfural Diacetyl Acetal 5-Nitrofurfurylidene Diacetate

Acetic acid coMpound with 5-nitrofuran-2-carbaldehyde (2:1)

5-NITROFURFURAL DIACETYL ACETAL

5-NITRO-2-FURANMETHANEDIOL DIACETATE

5-NITRO-2-FURFURALDEHYDE DIACETATE

5-NITRO-2-FURFURAL DIACETATE

5-NITRO-2-FURFURAL DIACETYL ACETAL

5-NITRO-2-FURALDEHYDE DIACETATE

2-(DIACETOXYMETHYL)-5-NITROFURAN

5-NITROFURAN-2-ALDEHYDE DIACETATE

Nifuratel impurity C

5-Nitro-2-furaL

dehyde diacetate

2-(5-nitro-2-furanyl)acetaldehyde diacetate

Nitrofural impurity B CRS

Nitrofurfural Diacetate (5-Nitro-2-furaldehyde Diacetate)

(5-Nitrofuran-2-yl)methylene Diacet

5-Nitro-2-furaldehydeDiacetate&gt

Nitrofurazone EP Impurity B

Nifuratel Impurity A (Nitrofurazone EP Impurity B)

Nifuratel impuritiesA

Nitrofurfural Diacetate (5-Nitro-2-furaldehyde Diacetate)Q: What is Nitrofurfural Diacetate (5-Nitro-2-furaldehyde Diacetate) Q: What is the CAS Number of Nitrofurfural Diacetate (5-Nitro-2-furaldehyde Diacetate) Q: What is the storage condition of Nitrofurfural Diacetate (5-Nitro-2-furaldehyde Diacetate)

TIANFU-CHEM - 5-Nitro-2-furaldehyde diacetate

Nitrofurfural Diacetate (1465503)