ChemicalBook > CAS DataBase List > 1-Methylpiperidine-4-carboxylic acid hydrochloride
1-Methylpiperidine-4-carboxylic acid hydrochloride
- Product Name
- 1-Methylpiperidine-4-carboxylic acid hydrochloride
- CAS No.
- 71985-80-3
- Chemical Name
- 1-Methylpiperidine-4-carboxylic acid hydrochloride
- Synonyms
- BIO-FARMA BF002150;RARECHEM AH CK 0139;TIMTEC-BB SBB003751;Lasmiditan Impurity 45;N-MethylisonipecoticacidHCl;4-CARBOXY-1-METHYL-PIPERIDINE HCL;1-Methyl-piperidine-4-carboxylic a;Methylpiperidincarbonsurehydrochlorid;1-Methyl-4-piperidinecarboxylic acid HCl;1-METHYL-PIPERIDINE-4-CARBOXYLIC ACID HCL
- CBNumber
- CB6341912
- Molecular Formula
- C7H14ClNO2
- Formula Weight
- 179.64
- MOL File
- 71985-80-3.mol
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1-Methylpiperidine-4-carboxylic acid hydrochloride Property
- Melting point:
- 226-228°C (dec.)
- storage temp.
- Inert atmosphere,Room Temperature
- form
- solid
- color
- Off-white
- InChI
- InChI=1S/C7H13NO2.ClH/c1-8-4-2-6(3-5-8)7(9)10;/h6H,2-5H2,1H3,(H,9,10);1H
- InChIKey
- NLUDEWJJEMHIIL-UHFFFAOYSA-N
- SMILES
- N1(C)CCC(C(O)=O)CC1.[H]Cl
- CAS DataBase Reference
- 71985-80-3(CAS DataBase Reference)
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Safety
- Hazard Codes
- Xi
- Risk Statements
- 36/37/38-20/21/22
- Safety Statements
- 26-36-24/25-36/37
- HazardClass
- IRRITANT
- HS Code
- 29339900
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
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N-Bromosuccinimide Price
TRC
- Product number
- M320978
- Product name
- 1-Methylpiperidine-4-carboxylic acid hydrochloride
- Packaging
- 500mg
- Price
- $75
- Updated
- 2021/12/16
AK Scientific
- Product number
- Y9343
- Product name
- 1-Methylpiperidine-4-carboxylic acid hydrochloride
- Packaging
- 25g
- Price
- $82
- Updated
- 2021/12/16
Frontier Specialty Chemicals
- Product number
- JK118455
- Product name
- 1-Methylpiperidine-4-carboxylic acid hydrochloride
- Purity
- 98%
- Packaging
- 5g
- Price
- $100
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 016314
- Product name
- 1-Methylpiperidine-4-carboxylic acidhydrochloride
- Packaging
- 1g
- Price
- $10
- Updated
- 2021/12/16
SynQuest Laboratories
- Product number
- 4H21-5-Z0
- Product name
- 1-Methylpiperidine-4-carboxylic acid hydrochloride
- Purity
- 98%
- Packaging
- 1g
- Price
- $21
- Updated
- 2021/12/16
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1-Methylpiperidine-4-carboxylic acid hydrochloride Chemical Properties,Usage,Production
Chemical Properties
Off-white solid
Synthesis
The synthesis method of 1-Methylpiperidine-4-carboxylic acid Hydrochloride is shown below: Charge isonipecotic acid, palladium, and purified water into a reaction vessel. Heat the resulting mixture to 90 to 95° C. Charge formic acid and formaldehyde to the vessel. Cool the resulting mixture to 20 to 30° C. Filter the reaction mixture through GF/F. Wash the filter cake with purified water. Concentrate the combined filtrates to ca 2 vol at atmospheric pressure. Adjust the temperature 65 to 75° C. Charge conc—hydrochloric acid to the vessel. Charge acetonitrile to the vessel at ≧70° C. and concentrate the solution to ca 2 vol at atmospheric pressure. Charge acetonitrile to the vessel. Moreover, concentrate the solution at atmospheric pressure to ca 2 vol. Charge acetonitrile to the vessel. Moreover, concentrate the solution at atmospheric pressure to ca 3 vol. Check the water content by KF analysis of the supernatant liquors using AX reagent. Cool the reaction mixture to 20 to 25° C. Stir the reaction mixture for 1 to 2 hours. Filter the reaction mixture. Wash the filter cake with acetonitrile. Dry the product up to 50° C. until ≦0.5% w/w by LOD and ≦0.2% w/w water.
1-Methylpiperidine-4-carboxylic acid hydrochloride Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 1-Methylpiperidine-4-carboxylic acid hydrochloride manufacturers
Hangzhou ICH Biofarm Co., Ltd
- Product
- 1-METHYLPIPERIDINE-4-CARBOXYLIC ACID HYDROCHLORIDE 71985-80-3
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 99.0%min
- Supply Ability
- 10000kg
- Release date
- 2023-06-09
Career Henan Chemical Co
- Product
- 1-METHYLPIPERIDINE-4-CARBOXYLIC ACID HYDROCHLORIDE 71985-80-3
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- ≥98%
- Supply Ability
- 20 tons
- Release date
- 2020-01-09
71985-80-3, 1-Methylpiperidine-4-carboxylic acid hydrochlorideRelated Search:
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(S)-1-Methylpiperidine-2-carboxylic acid hydrochloride
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