ChemicalBook > CAS DataBase List > 5-BROMOSALICYLAMIDE

5-BROMOSALICYLAMIDE

Application

Product Name: 5-BROMOSALICYLAMIDE
CAS No.: 6329-74-4
Chemical Name: 5-BROMOSALICYLAMIDE
Synonyms: Nsc 14278;Brn 3530373;Einecs 228-704-5;bromo-salicylamid;BROMOSALICYLAMIDE;5-BROMOSALICYLAMIDE;Salicylamide, bromo-;bromo-2-hydroxybenzamide;5-BROMO-2-HYDROXYBENZAMIDE;5-broMo-2-hydeoxybenzaMide
CBNumber: CB6345495
Molecular Formula: C7H6BrNO2
Formula Weight: 216.03
MOL File: 6329-74-4.mol

Less

5-BROMOSALICYLAMIDE Property

Melting point:: 241-245 °C(lit.)
Boiling point:: 316.6±32.0 °C(Predicted)
Density: 1.759±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 7.79±0.18(Predicted)
Appearance: White to off-white Solid

Less

Safety

Hazard Codes: Xn
Risk Statements: 22-43
Safety Statements: 28-36/37
WGK Germany: 3
RTECS: VN7000000

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H317May cause an allergic skin reaction

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

Less

N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 631205
Product name: 5-Bromosalicylamide
Purity: 97%
Packaging: 5g
Price: $104
Updated: 2023/06/20

Sigma-Aldrich

Product number: 631205
Product name: 5-Bromosalicylamide
Purity: 97%
Packaging: 25g
Price: $331
Updated: 2023/06/20

TRC

Product number: B688788
Product name: 5-Bromosalicylamide
Packaging: 250mg
Price: $55
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB36899
Product name: 5-Bromosalicylamide
Packaging: 5G
Price: $60
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB36899
Product name: 5-Bromosalicylamide
Packaging: 25g
Price: $200
Updated: 2021/12/16

Less

5-BROMOSALICYLAMIDE Chemical Properties,Usage,Production

Application

5-Bromosalicylate is an amide organic compound that can be used as a pharmaceutical synthesis intermediate.

Synthesis

89-55-4

6329-74-4

A. Procedure for the synthesis of 5-bromo-2-hydroxybenzamide: 1. In a 100 mL round-bottom flask, 5-bromosalicylic acid (30 g, 135.5 mmol) was dissolved in n-butanol (60 mL) and concentrated sulfuric acid (95.6%, 289 μL, 5.42 mmol) was added. The unit was equipped with a Dean-Stark manifold and reflux condenser and 12 mL of n-butanol was added. 2. Reflow the reaction mixture under heat for 2 days. Upon completion of the reaction, it was cooled to room temperature and concentrated to give a light yellow oil. 3. Methanol (50 mL) was added to the above oil, followed by the slow addition of a methanol solution of ammonia (7 N, 116 mL). 4. The reaction mixture was stirred at room temperature for 2 days and the progress of the reaction was monitored by HPLC. 5. 5. After completion of the reaction, the reaction mixture was concentrated to give a white solid. 6. The crude product was washed with a small amount of ethyl acetate and hexane to give 24 g of white crystalline solid in 82% yield.

References

[1] Patent: WO2005/95326, 2005, A2. Location in patent: Page/Page column 253
[2] Patent: US2018/64726, 2018, A1. Location in patent: Paragraph 0360; 0361
[3] Chemical and Pharmaceutical Bulletin, 1996, vol. 44, # 4, p. 734 - 745
[4] Patent: US2006/14737, 2006, A1. Location in patent: Page/Page column 25

5-BROMOSALICYLAMIDE Preparation Products And Raw materials

Raw materials

Acetic anhydride N,N-Dimethylformamide Tetrahydrofuran Oxalyl chloride 5-Bromosalicylic acid Ammonia

Preparation Products

Less

5-BROMOSALICYLAMIDE Suppliers

China 71 Germany 2 India 1 Switzerland 1 United Kingdom 6 United States 13 Global 94

Meryer (Shanghai) Chemical Technology Co., Ltd.

Tel: 4006356688 18621169109
Fax: 86-21-61259102
Email: market03@meryer.com
Country: China
ProdList: 40228
Advantage: 62

Energy Chemical

Tel: 021-021-58432009 400-005-6266
Fax: 021-58436166
Email: sales8178@energy-chemical.com
Country: China
ProdList: 44801
Advantage: 61

Shanghai Hanhong Scientific Co.,Ltd.

Tel: 021-54306202 13764082696
Email: info@hanhongsci.com
Country: China
ProdList: 42934
Advantage: 64

Syntechem Co.,Ltd

Tel
Fax: E-Mail Inquiry
Email: info@syntechem.com
Country: China
ProdList: 12984
Advantage: 57

Shanghai Sunway Pharmaceutical Technology Co., Ltd

Tel: 18270980682
Fax: 021 51613951
Email: mlcheng@sunwaypharm.cn
Country: China
ProdList: 8669
Advantage: 57

Shanghai Topbiochem Technology Co., Ltd

Tel: +86-21-60341587
Fax: +86-21-61294319
Email: sales@topbiochem.com
Country: China
ProdList: 6175
Advantage: 58

Shanghai Raise Chemical Technology Co.,Ltd

Tel: +86-021-50935922
Fax: +86-021-33847795
Country: China
ProdList: 7865
Advantage: 55

Bide Pharmatech Ltd.

Tel: 400-164-7117 13681763483
Fax: +86-21-61629029
Email: product02@bidepharm.com
Country: China
ProdList: 39966
Advantage: 60

Modachem Shanghai Co., Ltd

Tel: +86 (0)21 51320687 51371369 1744605818
Fax: +86 (0)21 51371369
Country: China
ProdList: 1578
Advantage: 58

Shanghai ACT chemical Limited

Tel: 021-59904146 18001826933
Fax: +86-21-59904146
Email: sales@actchemical.com
Country: China
ProdList: 476
Advantage: 56

Shanghai Xingui Biotechnology Co., Ltd.

Tel: 15121041756
Email: xingui2022@126.com
Country: China
ProdList: 9979
Advantage: 58

Shanghai HuanChuan Industry Co.,Ltd.

Tel: 021-61478794
Fax: 021-61478794
Email: sales@hcshhai.com
Country: China
ProdList: 9793
Advantage: 50

Nanjing Chalf-Pharm Technology Co., Ltd.

Tel: 025-57018978 18251899859
Fax: 025-57018008
Email: sales@chalf-pharm.com
Country: China
ProdList: 5674
Advantage: 50

Shanghai Send Pharmaceutical Technology Co., Ltd.

Tel: 021-58088081 Q2635253576
Fax: QQ3382968513
Email: hailey@shsendpharm.com
Country: China
ProdList: 2081
Advantage: 55

Zhengzhou Alfachem Co.,Ltd.

Tel: 0371-53778726 18003825608
Fax: QQ：2885354392
Email: liuxiaoyan@alfachem.cn
Country: China
ProdList: 1986
Advantage: 58

Shanghai YuanYe Biotechnology Co., Ltd.

Tel: 021-61312847; 18021002903
Fax: QQ:3008007432
Email: 3008007409@qq.com
Country: China
ProdList: 71826
Advantage: 60

parabiochem

Tel: 025-83453382-8005
Fax: 025-83453382
Email: sale@parabiochem.com
Country: China
ProdList: 9595
Advantage: 55

Amadis Chemical Company Limited

Tel: 571-89925085
Fax: 0086-571-89925065
Email: sales@amadischem.com
Country: China
ProdList: 131957
Advantage: 58

Dalian lichuang Chemical Co., Ltd

Tel: 0411-0411-00000000 13644282108
Fax: -
Email: 3500508746@qq.com
Country: China
ProdList: 2896
Advantage: 55

Aikon International Limited

Tel: 025-66061636 18013972705
Fax: (3)02557626880
Email: qqyang@aikonchem.com
Country: China
ProdList: 15814
Advantage: 58

Shanghai Jizhi Biochemical Technology Co. Ltd.

Tel: 4009004166/18616739031 18616739031
Email: 3007523370@qq.com
Country: China
ProdList: 52687
Advantage: 58

Cool Pharm, Ltd

Tel: 021-58581007 18019463053
Fax: 021-50966098
Email: sales@coolpharm.com
Country: China
ProdList: 12878
Advantage: 58

Shanghai FWD Chemicals Limited

Tel: 021-54450827 021-54450828
Email: sales@fwdchem.com
Country: China
ProdList: 997
Advantage: 58

Xinyi Kaiwu Chemical Technology Co., Ltd.

Tel: 0516-0516-88997009 18651776937
Email: 4164357@qq.com
Country: China
ProdList: 3204
Advantage: 58

Hefei TNJ Chemical Industry Co.,Ltd.

Tel: +86-0551-65418671 +8618949823763
Fax: 0551-65418697
Email: sales@tnjchem.com
Country: China
ProdList: 34563
Advantage: 58

Dayang Chem (Hangzhou) Co.,Ltd.

Tel: +86-0571-88938639 +8617705817739
Fax: +86-571-88938652，+86-571- 88492614
Email: info@dycnchem.com
Country: China
ProdList: 52846
Advantage: 58

Dideu Industries Group Limited

Tel: +86-29-89586680 +86-15129568250
Email: 1026@dideu.com
Country: China
ProdList: 20284
Advantage: 58

Win-Win chemical CO., Limited

Tel: +86-0086-577-64498589 +86-15355981851
Fax: 0086-577-56994596
Email: sales@win-winchemical.com
Country: China
ProdList: 14359
Advantage: 58

career henan chemical co

Tel: +86-0371-86658258 +8613203830695
Fax: 0086-371-86658258
Email: factory@coreychem.com
Country: China
ProdList: 29798
Advantage: 58

Ningbo jinuo chemical co., LTD

Tel: 0574-87314919 057487319282
Email: info@nbinno.com
Country: China
ProdList: 7047
Advantage: 58

Shanghai Haohong Pharmaceutical Co., Ltd.

Tel: 400-8210725 4008210725
Email: malulu@leyan.com
Country: China
ProdList: 40000
Advantage: 58

Molcoo Chemicals Inc.

Tel: 18576690171
Email: 3001025734@qq.com
Country: China
ProdList: 8880
Advantage: 58

Bide Pharmatech Ltd.

Tel: 400-6005915
Email: sales@picasso-e.com
Country: China
ProdList: 39665
Advantage: 58

Shaanxi Dideu Newmaterial Co., Ltd.

Tel: 029-63373950 17392213970
Email: 1052@dideu.com
Country: China
ProdList: 9998
Advantage: 58

Hangzhou Yaoruiyicheng Biological Medicine Co., Ltd

Tel: 18072846723 18072846723
Email: 2493446488@qq.com
Country: China
ProdList: 568
Advantage: 58

Shaanxi PharmaGHS Science Co., LTD

Tel: 13279368192
Email: pharmaghs@126.com
Country: China
ProdList: 2935
Advantage: 58

Beijing Solarbio Science & Tecnology Co., Ltd.

Tel: 010-50973130 17801761073
Email: Gsiyu@solarbio.com
Country: China
ProdList: 50464
Advantage: 58

Hangzhou Bingochem Co., Ltd.

Tel: 0571-8512-5372
Email: sales@bingochem.com
Country: China
ProdList: 21669
Advantage: 58

Shanghai Aladdin Biochemical Technology Co.,Ltd.

Tel: 400-6206333 13167063860
Email: anhua.mao@aladdin-e.com
Country: China
ProdList: 48457
Advantage: 58

Shanghai Zunlijia Life Technology Co., Ltd

Tel: 021-34045219 13062664914
Email: huji@zunlijia.com
Country: China
ProdList: 10027
Advantage: 58

Hubei Moco Chemical Co., Ltd.

Tel: 18627753421; 18627756402
Fax: QQ：3001051413
Email: 3001051413@qq.com
Country: China
ProdList: 20319
Advantage: 58

Santa Cruz Biotechnology Inc

Tel: 021-60936350
Email: scbt@scbt.com
Country: China
ProdList: 6594
Advantage: 58

Heze Shuying Biotechnology Co., Ltd.

Tel: 18553078733
Email: 1779923533@qq.com
Country: China
ProdList: 1070
Advantage: 58

Guangdong Yuanfeng Chemical Reagent Co., Ltd

Tel: 13318584237
Email: 3930831290@qq.com
Country: China
ProdList: 3843
Advantage: 58

Moxin Chemicals

Tel: +86-17320513646 +8617320513646
Email: anna@molcoo.com
Country: China
ProdList: 10000
Advantage: 58

SHANGHAI KEAN TECHNOLOGY CO., LTD.

Tel: +8613817748580
Fax: 021-50175322
Email: cooperation@kean-chem.com
Country: China
ProdList: 40066
Advantage: 58

Shanghai Acmec Biochemical Technology Co., Ltd.

Tel: +86-18621343501; +undefined18621343501
Email: product@acmec-e.com
Country: China
ProdList: 33338
Advantage: 58

Hebei Chuanghai Biotechnology Co., Ltd

Tel: +8615531151365
Email: mina@chuanghaibio.com
Country: China
ProdList: 18126
Advantage: 58

GIHI CHEMICALS CO.,LIMITED

Tel: +8618058761490
Email: info@gihichemicals.com
Country: China
ProdList: 49941
Advantage: 58

PT CHEM GROUP LIMITED

Tel: +86-85511178;
Email: peter68@ptchemgroup.com
Country: China
ProdList: 35425
Advantage: 58

Less

View Lastest Price from 5-BROMOSALICYLAMIDE manufacturers

Career Henan Chemical Co

Product: 5-BROMOSALICYLAMIDE 6329-74-4
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200kg
Release date: 2020-01-03

6329-74-4, 5-BROMOSALICYLAMIDERelated Search:

5-BROMOSALICYLAMIDE dibromsalan BROMOPRIDE 3,5,4'-TRIBROMOSALICYLANILIDE 3-BROMO-5-CHLORO-2,6-DIMETHOXYBENZAMIDE 5-BROMO-4'-CHLOROSALICYLANILIDE 3,5-DIBROMO SALICYL HYDRAZIDE 3,5-DIBROMOSALICYLAMIDE 4-BROMO-N-DODECYL-1-HYDROXY-2-NAPHTHALENECARBOXAMIDE Flusalan 5-BROMO-2-HYDROXYBENZOHYDRAZIDE 3-BROMO-2,6-DIMETHOXYBENZAMIDE Fursalan 6,8-Dibromo-2-thio-2H-1,3-benzoxazine-2,4(3H)-dione SALOR-INT L365017-1EA N-(3-BROMO-2,6-DIMETHOXY-5-NITROBENZOYL)-N'-(2,3,4,5,6-PENTAFLUOROPHENYL)UREA 3-BROMO-2,6-DIMETHOXY-5-NITROBENZAMIDE N-(3-BROMO-2,6-DIMETHOXYBENZOYL)-N'-(2,3,4,5,6-PENTAFLUOROPHENYL)UREA

5-BROMO-2-HYDROXYBENZAMIDE

BROMOSALICYLAMIDE

Benzamide, 5-bromo-2-hydroxy- (9ci)

Brn 3530373

Einecs 228-704-5

Nsc 14278

Salicylamide, 5-bromo- (8ci)

Salicylamide, bromo-

5-broMo-2-hydeoxybenzaMide

BenzaMide,5-broMo-2-hydroxy-

bromo-salicylamid

5-BROMOSALICYLAMIDE

5-BROMOSALICYLAMIDE ISO 9001：2015 REACH

bromo-2-hydroxybenzamide

6329-74-4

Carbonyl Compounds

Amides

Building Blocks

Organic Building Blocks

Aromatic Carboxylic Acids, Amides, Anilides, Anhydrides & Salts

Amides

Carbonyl Compounds

Organic Building Blocks