N-BOC-3-AZA-HEPTAN-1-ONE
- Product Name
- N-BOC-3-AZA-HEPTAN-1-ONE
- CAS No.
- 870842-23-2
- Chemical Name
- N-BOC-3-AZA-HEPTAN-1-ONE
- Synonyms
- 1-BOC-3-OXOAZEPANE;N-Boc-3-oxoazepane;1-Boc-azepan-3-one;N-BOC-3-AZA-HEPTAN-1-ON;N-BOC-3-AZA-HEPTAN-1-ONE;N-Boc-3-azacycloheptan-1-one;Azepan-3-one, N-BOC protected;1H-Azepine-1-carboxylic acid, hexahydro-3-oxo-, 1,1-dimethylethyl ester;tert-Butyl 3-oxoazepane-1-carboxylate, 1-(tert-Butoxycarbonyl)-3-oxoazepane, 1-(tert-Butoxycarbonyl)-3-oxohomopiperidine
- CBNumber
- CB6388478
- Molecular Formula
- C11H19NO3
- Formula Weight
- 213.27
- MOL File
- 870842-23-2.mol
N-BOC-3-AZA-HEPTAN-1-ONE Property
- Boiling point:
- 308.2±35.0 °C(Predicted)
- Density
- 1.072±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C
- pka
- -1.63±0.20(Predicted)
- Appearance
- White to yellow Solid
- InChI
- InChI=1S/C11H19NO3/c1-11(2,3)15-10(14)12-7-5-4-6-9(13)8-12/h4-8H2,1-3H3
- InChIKey
- HMWANNJNYUPZPN-UHFFFAOYSA-N
- SMILES
- N1(C(OC(C)(C)C)=O)CCCCC(=O)C1
Safety
- HS Code
- 2914290090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H302Harmful if swallowed
H304May be fatal if swallowed and enters airways
H315Causes skin irritation
H318Causes serious eye damage
H336May cause drowsiness or dizziness
H373May cause damage to organs through prolonged or repeated exposure
H410Very toxic to aquatic life with long lasting effects
- Precautionary statements
-
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P273Avoid release to the environment.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P314Get medical advice/attention if you feel unwell.
P331Do NOT induce vomiting.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P391Collect spillage. Hazardous to the aquatic environment
P403+P233Store in a well-ventilated place. Keep container tightly closed.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- B872290
- Product name
- tert-Butyl3-oxoazepane-1-carboxylate
- Packaging
- 50mg
- Price
- $110
- Updated
- 2021/12/16
- Product number
- 072957
- Product name
- tert-Butyl 3-oxoazepane-1-carboxylate
- Purity
- 95+%
- Packaging
- 500mg
- Price
- $175
- Updated
- 2021/12/16
- Product number
- W8936
- Product name
- tert-Butyl3-oxoazepane-1-carboxylate
- Packaging
- 1g
- Price
- $267
- Updated
- 2021/12/16
- Product number
- 072957
- Product name
- tert-Butyl 3-oxoazepane-1-carboxylate
- Purity
- 95+%
- Packaging
- 1g
- Price
- $340
- Updated
- 2021/12/16
- Product number
- 4H56-1-8H
- Product name
- tert-Butyl 3-oxoazepane-1-carboxylate
- Purity
- 95%
- Packaging
- 1g
- Price
- $352
- Updated
- 2021/12/16
N-BOC-3-AZA-HEPTAN-1-ONE Chemical Properties,Usage,Production
Synthesis
146407-32-1
24424-99-5
870842-23-2
GENERAL STEPS: To a solution of 1-benzyl-azepan-3-one (5.4 g, 26.6 mmol) in methanol (1000 mL) was added wet Pd/C (3 g, 50% water content) and di-tert-butyl dicarbonate (6.4 g, 29.3 mmol). The mixture was transferred to a hydrogenation flask and the reaction solution was stirred under hydrogenation conditions (H2, 50 psi) for 12 h at room temperature. The progress of the reaction was monitored by TLC and after confirming the completion of the reaction, the reaction solution was filtered to remove the catalyst and the filtrate was subsequently evaporated to afford N-Boc-3-azepinone (oil, 5.6 g, 100% yield).1H NMR (400 MHz, d6-DMSO): δppm 4.04-3.96 (m, 2H), 3.45-3.36 (m, 2H) , 2.55-2.52 (m, 2H), 1.85-1.72 (m, 4H), 1.53-1.48 (m, 9H).
References
[1] Patent: US2017/313683, 2017, A1. Location in patent: Paragraph 1043-1044
N-BOC-3-AZA-HEPTAN-1-ONE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from N-BOC-3-AZA-HEPTAN-1-ONE manufacturers
- Product
- N-Boc-3-azacycloheptan-1-one 870842-23-2
- Price
- US $2.20-8.80/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 100kg
- Release date
- 2025-06-17
- Product
- N-BOC-3-AZA-HEPTAN-1-ONE 870842-23-2
- Price
- US $200.00-1300.00/g
- Min. Order
- 5g
- Purity
- 99%
- Supply Ability
- 50
- Release date
- 2024-07-12
- Product
- N-BOC-3-AZA-HEPTAN-1-ONE 870842-23-2
- Price
- US $0.01/KG
- Min. Order
- 1KG
- Purity
- 98%;99%
- Supply Ability
- 1kg； 5kg；10kg；25kg
- Release date
- 2020-01-07