3-AMINO-N,N-DIMETHYL-BENZENESULFONAMIDE

Product Name: 3-AMINO-N,N-DIMETHYL-BENZENESULFONAMIDE
CAS No.: 6274-18-6
Chemical Name: 3-AMINO-N,N-DIMETHYL-BENZENESULFONAMIDE
Synonyms: AKOS BBS-00004621;3-AMINO-N,N-DIMETHYL-BENZENESULFONAMIDE;Benzenesulfonamide, 3-amino-N,N-dimethyl-;3-amino-N,N-dimethylbenzene-1-sulfonamide
CBNumber: CB6417631
Molecular Formula: C8H12N2O2S
Formula Weight: 200.26
MOL File: 6274-18-6.mol

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3-AMINO-N,N-DIMETHYL-BENZENESULFONAMIDE Property

Melting point:: 156-158 °C
Boiling point:: 367.4±44.0 °C(Predicted)
Density: 1.273±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: 3.12±0.10(Predicted)
Appearance: Off-white to light yellow Solid

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Safety

Hazard Codes: Xi
HazardClass: IRRITANT

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: A605188
Product name: 3-Amino-N,N-dimethylbenzenesulfonamide
Packaging: 100mg
Price: $75
Updated: 2021/12/16

Matrix Scientific

Product number: 016779
Product name: 3-Amino-N,N-dimethyl-benzenesulfonamide
Packaging: 1g
Price: $79
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0023299
Product name: 3-AMINO-N,N-DIMETHYL-BENZENESULFONAMIDE
Purity: 95.00%
Packaging: 1G
Price: $721.57
Updated: 2021/12/16

AK Scientific

Product number: V6969
Product name: 3-Amino-N,N-dimethylbenzenesulfonamide
Packaging: 25g
Price: $784
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0023299
Product name: 3-AMINO-N,N-DIMETHYL-BENZENESULFONAMIDE
Purity: 95.00%
Packaging: 2.5G
Price: $983.88
Updated: 2021/12/16

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3-AMINO-N,N-DIMETHYL-BENZENESULFONAMIDE Chemical Properties,Usage,Production

Synthesis

26199-83-7

6274-18-6

Step 2: N,N-dimethyl-3-nitrobenzenesulfonamide (850 mg, 3.7 mmol) was dissolved in methanol (20 mL). Wet Pd/C catalyst (85 mg) was added to the solution. The reaction mixture was stirred overnight under hydrogen atmosphere. Upon completion of the reaction, the catalyst was removed by filtration and the solvent was evaporated under reduced pressure to afford 3-amino-N,N-dimethylbenzenesulfonamide (600 mg, 80% yield) as a white solid.LCMS (Method B): 0.48 [M + H]+ = 201.1.

References

[1] Patent: WO2015/172203, 2015, A1. Location in patent: Page/Page column 84
[2] Patent: US6503949, 2003, B1
[3] Patent: WO2009/66084, 2009, A1. Location in patent: Page/Page column 107-108
[4] Patent: EP1183229, 2005, B1. Location in patent: Page/Page column 153
[5] Bioorganic and Medicinal Chemistry Letters, 2017, vol. 27, # 1, p. 94 - 97

3-AMINO-N,N-DIMETHYL-BENZENESULFONAMIDE Preparation Products And Raw materials

Raw materials

Stannous chloride dihydrate 3-Nitrobenzenesulfonyl chloride Dimethylamine hydrochloride Tetrahydrofuran Sodium bicarbonate Magnesium sulfate

Preparation Products

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3-AMINO-N,N-DIMETHYL-BENZENESULFONAMIDE Suppliers

China 46 Germany 1 India 1 Russia 1 Ukraine 3 United States 9 Global 61

J & K SCIENTIFIC LTD.

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Jiangsu Aikon Biopharmaceutical R&D co.,Ltd.

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Accela ChemBio Inc.

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Changzhou Hopschain Chemical Co.,Ltd.

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Amadis Chemical Company Limited

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Amatek Scientific Co. Ltd.

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6274-18-6, 3-AMINO-N,N-DIMETHYL-BENZENESULFONAMIDERelated Search:

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3-AMINO-N,N-DIMETHYL-BENZENESULFONAMIDE

AKOS BBS-00004621

3-amino-N,N-dimethylbenzene-1-sulfonamide

Benzenesulfonamide, 3-amino-N,N-dimethyl-

6274-18-6