ChemicalBook > CAS DataBase List > 5-PHENYL-PYRIDIN-3-YLAMINE

5-PHENYL-PYRIDIN-3-YLAMINE

Product Name: 5-PHENYL-PYRIDIN-3-YLAMINE
CAS No.: 31676-54-7
Chemical Name: 5-PHENYL-PYRIDIN-3-YLAMINE
Synonyms: 5-phenyl-3-pyridinamine;5-phenylpyridin-3-aMine;3-AMINO-5-PHENYLPYRIDINE;3-Pyridinamine, 5-phenyl-;5-PHENYL-PYRIDIN-3-YLAMINE
CBNumber: CB6428712
Molecular Formula: C11H10N2
Formula Weight: 170.21
MOL File: 31676-54-7.mol

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5-PHENYL-PYRIDIN-3-YLAMINE Property

Boiling point:: 389.4±30.0 °C(Predicted)
Density: 1.133±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
form: solid
pka: 5.78±0.20(Predicted)
Appearance: Off-white to light brown Solid

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Safety

Risk Statements: 41
Safety Statements: 26-39

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H317May cause an allergic skin reaction

H319Causes serious eye irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B522335
Product name: 5-Phenylpyridin-3-amine
Packaging: 50mg
Price: $45
Updated: 2021/12/16

TRC

Product number: B522335
Product name: 5-Phenylpyridin-3-amine
Packaging: 100mg
Price: $60
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0010268
Product name: 3-AMINO-5-PHENYL PYRIDINE
Purity: 95.00%
Packaging: 5MG
Price: $498.18
Updated: 2021/12/16

Matrix Scientific

Product number: 132529
Product name: 5-Phenyl-pyridin-3-ylamine
Purity: 97%
Packaging: 5g
Price: $1440
Updated: 2021/12/16

AK Scientific

Product number: Z0503
Product name: 3-Amino-5-phenylpyridine
Packaging: 25g
Price: $1740
Updated: 2021/12/16

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5-PHENYL-PYRIDIN-3-YLAMINE Chemical Properties,Usage,Production

Synthesis

13535-01-8

98-80-6

31676-54-7

Step A: Synthesis of 5-phenylpyridin-3-amine 5-Bromopyridin-3-amine (248 mg, 1.43 mmol), tetrakis(triphenylphosphine)palladium (Pd(PPh3)4, 50.4 mg, 0.04 mmol), toluene (3 mL), sodium carbonate (2 M, 3 mL, 6 mmol, dissolved in ethanol), and phenylboronic acid (195 mg, 1.60 mmol) were mixed and heated in an oil bath at 90 °C for 4 hour. Upon completion of the reaction, it was cooled to room temperature and allowed to stand for 16 hours. The reaction mixture was transferred to a partition funnel and extracted with ethyl acetate and water by partition. The aqueous phase was washed again with ethyl acetate and the combined organic phases were washed with brine, dried over magnesium sulfate, filtered and concentrated in vacuum. The residue was purified by column chromatography (80% ethyl acetate/hexane) to afford 5-phenylpyridin-3-amine (31.9 mg, 0.19 mmol, 13% yield) as a white solid. 1H NMR (500 MHz, CDCl3) δ ppm: 8.17-8.42 (m, 1H), 8.02-8.20 (m, 1H), 7.32-7.62 (m, 4H), 7.25 (s, 1H), 7.06-7.20 (m, 1H). MS (LC/MS) retention time (R.T.) = 0.91 min; [M + H]+ = 171.09.

References

[1] Journal of Medicinal Chemistry, 2017, vol. 60, # 2, p. 695 - 709
[2] Patent: US2009/270405, 2009, A1. Location in patent: Page/Page column 84
[3] Patent: WO2011/53292, 2011, A1. Location in patent: Page/Page column 136
[4] Patent: JP5714745, 2015, B2. Location in patent: Paragraph 0271; 0272
[5] New Journal of Chemistry, 2017, vol. 41, # 24, p. 15420 - 15432

5-PHENYL-PYRIDIN-3-YLAMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 5-PHENYL-PYRIDIN-3-YLAMINE manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 5-PHENYL-PYRIDIN-3-YLAMINE 31676-54-7
Price: US $1.00/Kg
Min. Order: 1Kg
Purity: 98%
Supply Ability: 20T
Release date: 2024-07-21

31676-54-7, 5-PHENYL-PYRIDIN-3-YLAMINERelated Search:

2-PHENYL-PYRIDIN-3-YLAMINE 6-PHENYL-PYRIDIN-2-YLAMINE 5-PHENYL-PYRIDIN-2-YLAMINE 2-(4-METHOXY-PHENYL)-PYRIDIN-3-YLAMINE 3-PHENYL-PYRIDIN-2-YLAMINE 4-PHENYL-PYRIDIN-3-YLAMINE 4-PHENYL-PYRIDIN-2-YLAMINE 2-PHENYL-PYRIDIN-3-YLAMINE HYDROCHLORIDE 5-PHENYL-PYRIDIN-3-YLAMINE 2-AMINO-3-TRIDEUTEROMETHYLAMINO-5-PHENYLPYRIDINE 6-METHOXY-3-NITRO-5-PHENYL-PYRIDIN-2-YLAMINE 2-AMINO-3-METHYLAMINO-5-PHENYLPYRIDINE 6-PHENYL-PYRIDIN-3-YLAMINE 3-BROMO-5-PHENYL-PYRIDIN-2-YLAMINE 3-NITRO-5-PHENYLPYRIDINE 6-CHLORO-3-NITRO-5-PHENYL-PYRIDIN-2-YLAMINE 2-PHENYL-PYRIDIN-4-YLAMINE 2-(3-TRIFLUOROMETHYL-PHENYL)-PYRIDIN-3-YLAMINE

3-Pyridinamine, 5-phenyl-

5-phenylpyridin-3-aMine

3-AMINO-5-PHENYLPYRIDINE

5-PHENYL-PYRIDIN-3-YLAMINE

5-phenyl-3-pyridinamine

31676-54-7