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2,4-Dichlorobenzothiazole

Product Name
2,4-Dichlorobenzothiazole
CAS No.
3622-30-8
Chemical Name
2,4-Dichlorobenzothiazole
Synonyms
2,4-Dichlorobenzo[d]thiazole;IFLAB-BB F1910-0008;2,4-Dichlorbenzothiazol;2,4-DICHLOROBENZOTHIAZOLE;Benzothiazole, 2,4-dichloro-;2,4-DICHLORO-1,3-BENZOTHIAZOLE;Benzothiazole, 2,4-dichloro- (7CI,8CI,9CI);sulfuric acid [[3-hydroxy-1-oxo-2-[(2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)-2-mercapto-2-oxanyl]pent-4-enyl]amino] ester
CBNumber
CB6481539
Molecular Formula
C7H3Cl2NS
Formula Weight
204.08
MOL File
3622-30-8.mol
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2,4-Dichlorobenzothiazole Property

Melting point:
96-97 °C
Boiling point:
286.8±13.0 °C(Predicted)
Density 
1.567±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
pka
-2.02±0.10(Predicted)
Appearance
Light yellow to orange Solid
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Safety

HS Code 
29342000
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

Biosynth Carbosynth
Product number
FD140265
Product name
2,4-Dichlorobenzo[d]thiazole
Packaging
1g
Price
$70
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD140265
Product name
2,4-Dichlorobenzo[d]thiazole
Packaging
2g
Price
$121
Updated
2021/12/16
SynQuest Laboratories
Product number
7H70-5-1B
Product name
2,4-Dichloro-1,3-benzothiazole
Purity
95.0%
Packaging
5G
Price
$136
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD140265
Product name
2,4-Dichlorobenzo[d]thiazole
Packaging
5G
Price
$241
Updated
2021/12/16
Matrix Scientific
Product number
072090
Product name
2,4-Dichlorobenzothiazole
Purity
95+%
Packaging
1g
Price
$278
Updated
2021/12/16
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2,4-Dichlorobenzothiazole Chemical Properties,Usage,Production

Chemical Properties

Pale yellow solid

Synthesis

19952-47-7

3622-30-8

Step B: 4-Chlorobenzo[d]thiazol-2-amine (4.78 g, 25.8 mmol) and copper(II) chloride (4.16 g, 31 mmol) were dissolved in acetonitrile (25 mL), followed by tert-butyl nitrite (4.61 mL, 38.8 mmol) at room temperature. The reaction mixture was heated to 60 °C and maintained for 30 min. Upon completion of the reaction, the solvent was removed by rotary evaporation. The residue was suspended in water and the solid product was collected by filtration and dried to give 2,4-dichlorobenzo[d]thiazole (5.3 g, 81% yield). Mass spectrometry analysis showed a m/z of 205.9 [M + H]+.

References

[1] Chemistry - A European Journal, 2018, vol. 24, # 55, p. 14622 - 14626
[2] Patent: WO2013/101974, 2013, A1. Location in patent: Paragraph 00586; 00588
[3] Patent: US9617268, 2017, B2. Location in patent: Page/Page column 321; 322
[4] Gazzetta Chimica Italiana, 1964, vol. 94, p. 372 - 381
[5] Chemistry and Biodiversity, 2011, vol. 8, # 2, p. 253 - 265

2,4-Dichlorobenzothiazole Preparation Products And Raw materials

Raw materials

Preparation Products

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2,4-Dichlorobenzothiazole Suppliers

J & K SCIENTIFIC LTD.
Tel
18210857532; 18210857532
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
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China
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96815
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future industrial shanghai co., ltd
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400-0066400 13621662912
Fax
021-55660885
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sales@jonln.com
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China
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1995
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Shijiazhuang Sdyano Fine Chemical Co., Ltd.
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0311-89250318 031166536426
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4000311741
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master@sjzsdyn.com
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China
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2806
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JinYan Chemicals(ShangHai) Co.,Ltd.
Tel
13817811078
Fax
86-021-50426522,50426273
Email
sales@jingyan-chemical.com
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China
ProdList
9976
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Pure Chemistry Scientific Inc.
Tel
001-857-928-2050 or 1-888-588-9418
Fax
001-617-206-9595
Email
sales@chemreagents.com
Country
United States
ProdList
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Shanghai Longsheng chemical Co.,Ltd.
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021-58099652-8005 13585536065
Fax
021-58099609
Email
bin.wu@shlschem.com
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China
ProdList
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Shanghai Hanhong Scientific Co.,Ltd.
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021-54306202 13764082696
Email
info@hanhongsci.com
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China
ProdList
42934
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China DongFan Chemical Co.,LTD
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86-0571-85151182
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86-0571-85151182
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China
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5691
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China Langchem Inc.
Tel
0086-21-58956006
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0086-21-58956100
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China
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7811
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Shanghai Sunway Pharmaceutical Technology Co., Ltd
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18270980682
Fax
021 51613951
Email
mlcheng@sunwaypharm.cn
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China
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8669
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57
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View Lastest Price from 2,4-Dichlorobenzothiazole manufacturers

Hebei Chuanghai Biotechnology Co., Ltd
Product
2,4-Dichlorobenzothiazole 3622-30-8
Price
US $10.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10 mt
Release date
2024-12-04
Shaanxi Dideu Medichem Co. Ltd
Product
2,4-Dichlorobenzothiazole 3622-30-8
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
20t
Release date
2024-07-15
Honest Joy Holdings Limited
Product
2,4-Dichlorobenzothiazole 3622-30-8
Price
US $0.00/KG
Min. Order
1KG
Purity
97.1%
Supply Ability
100 tons
Release date
2022-01-14