2-Chloro-1,10-phenanthroline
- Product Name
- 2-Chloro-1,10-phenanthroline
- CAS No.
- 7089-68-1
- Chemical Name
- 2-Chloro-1,10-phenanthroline
- Synonyms
- VUF 7730;chlorophenanthroline;2-Chloro-1,10-phenan;2-Chloro-1,10-phenthroline;2-CHLORO-1,10-PHENANTHROLINE;1,10-Phenanthroline, 2-chloro-;2-Chloro-1,10-diazaphenanthrene;2-Chloro-1,10-phenanthroline >2-Chloro-1,10-phenanthroline Cas: 7089-68-1
- CBNumber
- CB6483144
- Molecular Formula
- C12H7ClN2
- Formula Weight
- 214.65
- MOL File
- 7089-68-1.mol
2-Chloro-1,10-phenanthroline Property
- Melting point:
- 130 °C
- Boiling point:
- 391.8±22.0 °C(Predicted)
- Density
- 1.375
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- solubility
- soluble in Methanol
- form
- powder to crystal
- pka
- 4.22±0.10(Predicted)
- color
- White to Yellow to Orange
- InChI
- InChI=1S/C12H7ClN2/c13-10-6-5-9-4-3-8-2-1-7-14-11(8)12(9)15-10/h1-7H
- InChIKey
- JHRMQHFRVPVGHL-UHFFFAOYSA-N
- SMILES
- N1C2C(=CC=C3C=2N=CC=C3)C=CC=1Cl
Safety
- Safety Statements
- 24/25
- HS Code
- 29339900
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- C1560
- Product name
- 2-Chloro-1,10-phenanthroline
- Purity
- >98.0%(HPLC)(T)
- Packaging
- 1g
- Price
- $666
- Updated
- 2025/07/31
- Product number
- C1560
- Product name
- 2-Chloro-1,10-phenanthroline
- Purity
- >98.0%(HPLC)(T)
- Packaging
- 100mg
- Price
- $171
- Updated
- 2025/07/31
- Product number
- B419493
- Product name
- 2-Chloro-1,10-phenanthroline
- Packaging
- 50mg
- Price
- $200
- Updated
- 2021/12/16
- Product number
- B419493
- Product name
- 2-Chloro-1,10-phenanthroline
- Packaging
- 100mg
- Price
- $310
- Updated
- 2021/12/16
- Product number
- FC60892
- Product name
- 2-Chloro-1,10-phenanthroline
- Packaging
- 25mg
- Price
- $50
- Updated
- 2021/12/16
2-Chloro-1,10-phenanthroline Chemical Properties,Usage,Production
Chemical Properties
Light yellow solid
Synthesis
1891-19-6
7089-68-1
General procedure for the synthesis of 2-chloro-1,10-phenanthroline from 1,10-phenanthroline 1-oxide: the procedure was similar to General Procedure I, with the difference that the reaction conditions were adjusted to be carried out at room temperature using 1,10-phenanthroline 1-oxide (1.00 eq.), POBr3 (3.00 eq.), and DMF (1.50 eq.) at a concentration of 0.2M. General procedure I (0013) for the bromination of acridazine N-oxide was carried out as follows: an appropriate amount of acridazine N-oxide was dissolved in anhydrous CH2Cl2 (0.1 M) at 0 °C, POBr3 (1.2 eq.) was added with stirring, followed by a slow, dropwise addition of DMF (0.5 eq.) under argon gas protection. The reaction mixture was gradually warmed to 25 °C with continuous stirring until TLC showed completion of the reaction. Upon completion of the reaction, the pH was adjusted to 7-8 by slow addition of saturated aqueous sodium carbonate solution. the mixture was separated and the aqueous phase was fully extracted with CH2Cl2. All organic phases were combined, washed with brine, dried over anhydrous Na2SO4, filtered and concentrated under reduced pressure to obtain the crude product. The crude product was purified by fast column chromatography with PE/EA (100:1) as eluent.
References
[1] Tetrahedron, 2016, vol. 72, # 38, p. 5762 - 5768
[2] Journal of Organic Chemistry, 2007, vol. 72, # 7, p. 2318 - 2328
[3] Chemistry - A European Journal, 2017, vol. 23, # 27, p. 6499 - 6503
[4] Journal of Organic Chemistry, 2017, vol. 82, # 8, p. 4203 - 4215
2-Chloro-1,10-phenanthroline Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-Chloro-1,10-phenanthroline manufacturers
- Product
- 2-Chloro[1,10]phenanthroline 7089-68-1
- Price
- US $1.10-9.90/KG
- Min. Order
- 1KG
- Purity
- 99%min
- Supply Ability
- 100KG
- Release date
- 2025-08-20
- Product
- 2-Chloro-1,10-phenanthroline 7089-68-1
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1ton
- Release date
- 2022-10-14
- Product
- 2-chloro-1,10-phenanthroline 7089-68-1
- Price
- US $15.00-65.00/g
- Min. Order
- 5g
- Purity
- 0.98
- Supply Ability
- 25kg
- Release date
- 2024-10-25