1,3,5-Tris(4-iodophenyl)benzene
- Product Name
- 1,3,5-Tris(4-iodophenyl)benzene
- CAS No.
- 151417-38-8
- Chemical Name
- 1,3,5-Tris(4-iodophenyl)benzene
- Synonyms
- CAS:151417-38-8;1,3,5-Tri(4-iodophenyl)benzene;1,3,5-TRIS(4-IODOPHENYL)BENZENE;1,3,5-Tris(4-iodophenyl)benzene 97%;1 3 5-TRIS(4-IODOPHENYL)BENZENE) 90;tert-butyl 3-iodoindazole-1-carboxylate;4,4''-Diiodo-5'-(4-iodophenyl)-1,1':3',1''-terphenyl;1,1':3',1''-Terphenyl, 4,4''-diiodo-5'-(4-iodophenyl)-;1 3 5-TRIS(4-IODOPHENYL)BENZENE) 90 ISO 9001:2015 REACH
- CBNumber
- CB6500168
- Molecular Formula
- C24H15I3
- Formula Weight
- 684.09
- MOL File
- 151417-38-8.mol
1,3,5-Tris(4-iodophenyl)benzene Property
- Melting point:
- 254-260 °C (lit.)
- Boiling point:
- 600.3±55.0 °C(Predicted)
- Density
- 1.946±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- form
- powder to crystal
- color
- White to Light yellow
- InChI
- InChI=1S/C24H15I3/c25-22-7-1-16(2-8-22)19-13-20(17-3-9-23(26)10-4-17)15-21(14-19)18-5-11-24(27)12-6-18/h1-15H
- InChIKey
- KGLWDSJGGFTHHD-UHFFFAOYSA-N
- SMILES
- C1(C2=CC(C3=CC=C(I)C=C3)=CC(C3=CC=C(I)C=C3)=C2)=CC=C(I)C=C1
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H318Causes serious eye damage
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 656453
- Product name
- 1,3,5-Tris(4-iodophenyl)benzene
- Purity
- 90%
- Packaging
- 1g
- Price
- $164
- Updated
- 2023/06/20
- Product number
- 656453
- Product name
- 1,3,5-Tris(4-iodophenyl)benzene
- Purity
- 90%
- Packaging
- 5g
- Price
- $546
- Updated
- 2023/01/07
- Product number
- T3084
- Product name
- 1,3,5-Tris(4-iodophenyl)benzene
- Purity
- >98.0%(HPLC)
- Packaging
- 1g
- Price
- $133
- Updated
- 2025/07/31
- Product number
- T3084
- Product name
- 1,3,5-Tris(4-iodophenyl)benzene
- Purity
- >98.0%(HPLC)
- Packaging
- 5g
- Price
- $461
- Updated
- 2025/07/31
- Product number
- X7248
- Product name
- 1,3,5-Tris(4-iodophenyl)benzene
- Packaging
- 1g
- Price
- $150
- Updated
- 2021/12/16
1,3,5-Tris(4-iodophenyl)benzene Chemical Properties,Usage,Production
Uses
Building block in a synthesis of C3-symmetric nano-sized polyaromatics and molecular propellers.
Synthesis
612-71-5
10450-60-9
151417-38-8
Example 1 (Preparation of 1,3,5-tris(4-iodophenyl)benzene): 116 g of 1,3,5-triphenylbenzene, 19 mL of concentrated sulfuric acid (as a catalyst), and 1520 mL of 80% acetic acid (as a reaction solvent) were sequentially added to a 2L three-necked flask. The reaction mixture was heated to 70 °C under stirring conditions. Subsequently, 143 g of iodine and 69.3 g of periodate were added in batches over a period of about 2.5 hours (Note: in the original text, "n-stereo acid" should be "periodate"). After the addition, the reaction was continued with stirring for 6 hours, during which a white precipitate was generated. At the end of the reaction, toluene was added to the reaction mixture to dissolve the precipitate and separate the toluene layer from the water layer. The toluene layer was washed with aqueous sodium bicarbonate and aqueous sodium thiosulfate in turn. The washed organic layer was concentrated and purified by silica gel column chromatography, and finally recrystallized with ethanol/toluene mixed solvent to obtain 34.6 g of the target product 1,3,5-tris(4-iodophenyl)benzene as white needle-like crystals in 13.3% yield.
References
[1] Patent: EP1826837, 2007, A1
1,3,5-Tris(4-iodophenyl)benzene Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 1,3,5-Tris(4-iodophenyl)benzene manufacturers
- Product
- 1,3,5-Tris(4-iodophenyl)benzene 151417-38-8
- Price
- US $667.00-184.00/g
- Min. Order
- 1g
- Purity
- 0.98
- Supply Ability
- 25kg
- Release date
- 2023-10-12