1,3,5-Tris(4-bromophenyl)benzene
- Product Name
- 1,3,5-Tris(4-bromophenyl)benzene
- CAS No.
- 7511-49-1
- Chemical Name
- 1,3,5-Tris(4-bromophenyl)benzene
- Synonyms
- Nsc30660;1,3,5-tri(4-bromophenyl)benzene;1,3,5-Tris(4-broMophenyl)benzen;1,3,5-Tris(4-bromophenyl)benzene;1,3,5-Tris(4-bromophenyc)-benzene;1,3,5-Tris(4'-bromophenyl)benzene;1,3,5-tri(4-broMobenzeneyl)benzene;4,4''-dibroMo-5'-(4-broMophenyl)-1,1':3',1''-terphenyl;1,1':3',1''-Terphenyl, 4,4''-dibromo-5'-(4-bromophenyl)-
- CBNumber
- CB5498862
- Molecular Formula
- C24H15Br3
- Formula Weight
- 543.09
- MOL File
- 7511-49-1.mol
1,3,5-Tris(4-bromophenyl)benzene Property
- Melting point:
- 261-265 °C
- Boiling point:
- 574.9±45.0 °C(Predicted)
- Density
- 1.626±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- form
- Crystalline Powder
- color
- Yellow to pale brown
- λmax
- 288nm(CHCl3)(lit.)
- InChI
- InChI=1S/C24H15Br3/c25-22-7-1-16(2-8-22)19-13-20(17-3-9-23(26)10-4-17)15-21(14-19)18-5-11-24(27)12-6-18/h1-15H
- InChIKey
- HJQRITCAXSBOPC-UHFFFAOYSA-N
- SMILES
- C1(C2=CC(C3=CC=C(Br)C=C3)=CC(C3=CC=C(Br)C=C3)=C2)=CC=C(Br)C=C1
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H318Causes serious eye damage
H413May cause long lasting harmful effects to aquatic life
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 648906
- Product name
- 1,3,5-Tris(4-bromophenyl)benzene
- Purity
- 97%
- Packaging
- 5g
- Price
- $243
- Updated
- 2025/07/31
- Product number
- 648906
- Product name
- 1,3,5-Tris(4-bromophenyl)benzene
- Purity
- 97%
- Packaging
- 1g
- Price
- $70
- Updated
- 2023/06/20
- Product number
- T2644
- Product name
- 1,3,5-Tris(4-bromophenyl)benzene
- Purity
- >98.0%(HPLC)
- Packaging
- 1g
- Price
- $51
- Updated
- 2025/07/31
- Product number
- T2644
- Product name
- 1,3,5-Tris(4-bromophenyl)benzene
- Purity
- >98.0%(HPLC)
- Packaging
- 5g
- Price
- $173
- Updated
- 2025/07/31
- Product number
- T895748
- Product name
- 1,3,5-tris(4-Bromophenyl)benzene
- Packaging
- 500mg
- Price
- $90
- Updated
- 2021/12/16
1,3,5-Tris(4-bromophenyl)benzene Chemical Properties,Usage,Production
Chemical Properties
White to tan solid
Uses
TBB can be used to synthesize porous aromatic frameworks for the development of adsorption membranes to treat organic pollutants. It can also be used in the fabrication of pyridine based high efficiency organic light emitting diodes(OLEDs).
General Description
1,3,5-Tris(4-bromophenyl)benzene (TBB) is a halogenated aromatic monomer that can be used in the formation of covalent aromatic frameworks(COF).
Synthesis
99-90-1
7511-49-1
General method: p-Bromoacetophenone (3 mmol) was mixed with sulfated tungstate (20 wt%) in a round-bottomed flask fitted with a condenser tube and the reaction was carried out with stirring at 130°C. The reaction was monitored by thin film chromatography (TLC). The reaction progress was monitored by thin layer chromatography (TLC). After complete consumption of p-bromoacetophenone, the reaction was continued for 2 hours. After the reaction mixture was cooled, it was diluted with 30 mL of ethyl acetate and filtered to recover the catalyst. The filtrate was sequentially washed with 10 mL of water, dried over anhydrous sodium sulfate and subsequently concentrated under reduced pressure. The residue was purified by column chromatography on silica gel (60-120 mesh) using petroleum ether: ethyl acetate (9:1, v/v) as eluent to give pure 1,3,5-tris(4-bromophenyl)benzene.
References
[1] Synthetic Communications, 2013, vol. 43, # 16, p. 2178 - 2190
[2] RSC Advances, 2015, vol. 5, # 27, p. 21206 - 21214
[3] Journal of the Iranian Chemical Society, 2012, vol. 9, # 5, p. 791 - 798
[4] European Journal of Organic Chemistry, 2014, vol. 2014, # 14, p. 2907 - 2916
[5] Synthetic Communications, 2005, vol. 35, # 24, p. 3167 - 3171
1,3,5-Tris(4-bromophenyl)benzene Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 1,3,5-Tris(4-bromophenyl)benzene manufacturers
- Product
- 1,3,5-Tris(4-bromophenyl)benzene 7511-49-1
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 1Ton
- Release date
- 2022-09-27
- Product
- 1,3,5-Tris(4-bromophenyl)benzene 7511-49-1
- Price
- US $7.00-97.00/g
- Min. Order
- 1g
- Purity
- 0.98
- Supply Ability
- 25kg
- Release date
- 2024-10-25
- Product
- 1,3,5-Tris(4-bromophenyl)benzene 7511-49-1
- Price
- US $0.10/KG
- Min. Order
- 1KG
- Purity
- 99.0%
- Supply Ability
- 1000 tons
- Release date
- 2024-08-15