1,3,5-Tris(3-bromophenyl)benzene
- Product Name
- 1,3,5-Tris(3-bromophenyl)benzene
- CAS No.
- 96761-85-2
- Chemical Name
- 1,3,5-Tris(3-bromophenyl)benzene
- Synonyms
- cas 96761-85-2;96761-85-2 cas;cas no 96761-85-2;5-Tris(3-bromophenyl)benzene;1,3,5-tri-(3-bromophenyl)benzene;1,3,5-TRIS(3-BROMOPHENYL)BENZENE;3,3''-Dibromo-5'-(3-bromophenyl)-1,1':3',1''-terphenyl;1,1':3',1''-Terphenyl, 3,3''-dibromo-5'-(3-bromophenyl)-
- CBNumber
- CB9511538
- Molecular Formula
- C24H15Br3
- Formula Weight
- 543.09
- MOL File
- 96761-85-2.mol
1,3,5-Tris(3-bromophenyl)benzene Property
- Melting point:
- 170.0 to 174.0 °C
- Boiling point:
- 553.9±45.0 °C(Predicted)
- Density
- 1.626±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- solubility
- soluble in Toluene
- form
- powder to crystal
- color
- White to Almost white
- InChI
- InChI=1S/C24H15Br3/c25-22-7-1-4-16(13-22)19-10-20(17-5-2-8-23(26)14-17)12-21(11-19)18-6-3-9-24(27)15-18/h1-15H
- InChIKey
- JKCQADHKVQXKFF-UHFFFAOYSA-N
- SMILES
- C1(C2=CC(C3=CC=CC(Br)=C3)=CC(C3=CC=CC(Br)=C3)=C2)=CC=CC(Br)=C1
Safety
- HS Code
- 2903.99.8001
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H302Harmful if swallowed
H312Harmful in contact with skin
H314Causes severe skin burns and eye damage
H332Harmful if inhaled
- Precautionary statements
-
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P321Specific treatment (see … on this label).
P322Specific measures (see …on this label).
P330Rinse mouth.
P363Wash contaminated clothing before reuse.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- T3073
- Product name
- 1,3,5-Tris(3-bromophenyl)benzene
- Purity
- >96.0%(HPLC)
- Packaging
- 1g
- Price
- $61
- Updated
- 2025/07/31
- Product number
- T3073
- Product name
- 1,3,5-Tris(3-bromophenyl)benzene
- Purity
- >96.0%(HPLC)
- Packaging
- 5g
- Price
- $241
- Updated
- 2025/07/31
- Product number
- 095526
- Product name
- 3,3''-Dibromo-5'-(3-bromophenyl)-1,1':3',1''-terphenyl
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $243
- Updated
- 2021/12/16
- Product number
- 095526
- Product name
- 3,3''-Dibromo-5'-(3-bromophenyl)-1,1':3',1''-terphenyl
- Purity
- 95+%
- Packaging
- 1g
- Price
- $538
- Updated
- 2021/12/16
- Product number
- HCH0037635
- Product name
- 1,3,5-TRIS(3-BROMOPHENYL)BENZENE
- Purity
- 95.00%
- Packaging
- 5G
- Price
- $909.56
- Updated
- 2021/12/16
1,3,5-Tris(3-bromophenyl)benzene Chemical Properties,Usage,Production
Synthesis
2142-63-4
96761-85-2
GENERAL METHODS: Trifluoroacetic acid (0.045 mL, 0.6 mmol) and ethylenediamine (0.020 mL, 0.3 mmol) were sequentially added to an anhydrous nitromethane (1.5 mL) solution of 3'-bromoacetophenone (1.5 mmol). The reaction mixture was stirred under reflux conditions and the progress of the reaction was monitored by thin layer chromatography (TLC). Upon completion of the reaction, the mixture was cooled to room temperature and the reaction was quenched with saturated ammonium chloride (NH4Cl) solution followed by extraction with ethyl acetate. The organic phases were combined, washed with saturated saline, dried over anhydrous sodium sulfate (Na2SO4) and concentrated under reduced pressure. Finally, the crude product was purified by silica gel column chromatography to give 1,3,5-tris(3-bromophenyl)benzene.
References
[1] Tetrahedron Letters, 2012, vol. 53, # 19, p. 2436 - 2439
[2] Comptes Rendus Chimie, 2013, vol. 16, # 3, p. 252 - 256
[3] Journal of Chemical Research, 2007, # 12, p. 720 - 721
[4] Synthetic Communications, 2012, vol. 42, # 24, p. 3579 - 3588
[5] Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988, p. 1251 - 1258
1,3,5-Tris(3-bromophenyl)benzene Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 1,3,5-Tris(3-bromophenyl)benzene manufacturers
- Product
- 1,3,5-Tris(3-bromophenyl)benzene 96761-85-2
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1ton
- Release date
- 2022-10-08
- Product
- 1,3,5-Tris(3-bromophenyl)benzene 96761-85-2
- Price
- US $9.00-181.00/g
- Min. Order
- 5g
- Purity
- 0.98
- Supply Ability
- 25kg
- Release date
- 2024-10-25
- Product
- 1,3,5-Tris(3-bromophenyl)benzene 96761-85-2
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- Customized
- Release date
- 2019-07-02