ChemicalBook > CAS DataBase List > 6-BROMO-2-PHENYL-IMIDAZO[1,2-A]PYRIDINE

6-BROMO-2-PHENYL-IMIDAZO[1,2-A]PYRIDINE

Product Name
6-BROMO-2-PHENYL-IMIDAZO[1,2-A]PYRIDINE
CAS No.
4044-98-8
Chemical Name
6-BROMO-2-PHENYL-IMIDAZO[1,2-A]PYRIDINE
Synonyms
6-BROMO-2-PHENYL-IMIDAZO[1,2-A]PYRIDINE;Imidazo[1,2-a]pyridine, 6-bromo-2-phenyl-
CBNumber
CB6680378
Molecular Formula
C13H9BrN2
Formula Weight
273.13
MOL File
4044-98-8.mol
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6-BROMO-2-PHENYL-IMIDAZO[1,2-A]PYRIDINE Property

Melting point:
201-202 °C
Density 
1.48±0.1 g/cm3(Predicted)
storage temp. 
Inert atmosphere,Room Temperature
pka
4.98±0.50(Predicted)
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Safety

Hazard Codes 
Xn
Risk Statements 
22
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific
Product number
5450AB
Product name
6-Bromo-2-phenylimidazo[1,2-a]pyridine
Packaging
10g
Price
$90
Updated
2021/12/16
AK Scientific
Product number
5450AB
Product name
6-Bromo-2-phenylimidazo[1,2-a]pyridine
Packaging
1g
Price
$20
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0105319
Product name
6-BROMO-2-PHENYLIMIDAZO(1,2-A)PYRIDINE
Purity
95.00%
Packaging
1G
Price
$691.95
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0105319
Product name
6-BROMO-2-PHENYLIMIDAZO(1,2-A)PYRIDINE
Purity
95.00%
Packaging
5G
Price
$2656.5
Updated
2021/12/16
AstaTech
Product number
52709
Product name
6-BROMO-2-PHENYLIMIDAZO[1,2-A]PYRIDINE
Purity
97%
Packaging
1/ G
Price
$47
Updated
2021/12/16
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6-BROMO-2-PHENYL-IMIDAZO[1,2-A]PYRIDINE Chemical Properties,Usage,Production

Synthesis

1072-97-5

98-86-2

4044-98-8

First, 2-amino-5-bromopyridine (0.25 mmol), acetophenone (0.25 mmol), iodine (20 mol%, 13 mg), and cyclohexane (2 mL) were added to a 25 mL round-bottomed flask, and the reaction was stirred at 60 °C. Stirring was continued under these conditions for 15 min. Subsequently, the reaction mixture was diluted with 30 mL of water and the organic layer was extracted with ethyl acetate. The organic layer was dried with anhydrous sodium sulfate and concentrated under reduced pressure to remove the solvent. The crude product was purified by column chromatography and the eluent was a solvent mixture of petroleum ether and ethyl acetate.

References

[1] Journal of Organic Chemistry, 2013, vol. 78, # 24, p. 12494 - 12504
[2] Advanced Synthesis and Catalysis, 2013, vol. 355, # 9, p. 1741 - 1747
[3] Synthetic Communications, 2018, vol. 48, # 9, p. 1076 - 1084
[4] Advanced Synthesis and Catalysis, 2013, vol. 355, # 11-12, p. 2217 - 2221
[5] European Journal of Organic Chemistry, 2015, vol. 2015, # 29, p. 6526 - 6533

6-BROMO-2-PHENYL-IMIDAZO[1,2-A]PYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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6-BROMO-2-PHENYL-IMIDAZO[1,2-A]PYRIDINE Suppliers

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View Lastest Price from 6-BROMO-2-PHENYL-IMIDAZO[1,2-A]PYRIDINE manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
6-BROMO-2-PHENYL-IMIDAZO[1,2-A]PYRIDINE 4044-98-8
Price
US $3.00-2.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
200000KG
Release date
2024-07-29
Career Henan Chemical Co
Product
6-Bromo-2-phenylimidazo[1,2-a]pyridine 4044-98-8
Price
US $0.01/KG
Min. Order
1KG
Purity
98%; 99%
Supply Ability
500g;1kg; 25kg
Release date
2020-01-09