ChemicalBook > CAS DataBase List > 2-Amino-3,5-dichloropyridine

2-Amino-3,5-dichloropyridine

Product Name
2-Amino-3,5-dichloropyridine
CAS No.
4214-74-8
Chemical Name
2-Amino-3,5-dichloropyridine
Synonyms
AKOS BBS-00001349;BUTTPARK 153\57-29;TIMTEC-BB SBB003932;Edoxaban Impurity 104;3,5-dichloro-3-pyridylamine;3,5-DICHLORO-2-PYRIDINAMINE;3,5-DICHLOROPYRIDIN-2-AMINE;2-AMINO-3,5-DICHLIROPYRIDINE;3,5-Dichloro-2-AminoPyridine;2-AMINO-3,5-DICHLOROPYRIDINE
CBNumber
CB0356640
Molecular Formula
C5H4Cl2N2
Formula Weight
163
MOL File
4214-74-8.mol
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2-Amino-3,5-dichloropyridine Property

Melting point:
81-83 °C(lit.)
Boiling point:
268.76°C (rough estimate)
Density 
1.5462 (rough estimate)
refractive index 
1.6300 (estimate)
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
form 
Powder or Crystals
pka
2.43±0.10(Predicted)
color 
Off-white to pink to beige
Water Solubility 
insoluble
BRN 
119376
InChI
InChI=1S/C5H4Cl2N2/c6-3-1-4(7)5(8)9-2-3/h1-2H,(H2,8,9)
InChIKey
OCWBGKZFOYMCCN-UHFFFAOYSA-N
SMILES
C1(N)=NC=C(Cl)C=C1Cl
CAS DataBase Reference
4214-74-8(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38-20/21/22
Safety Statements 
26-36-37/39-28A-45-24/25
RIDADR 
UN2811
WGK Germany 
3
HazardClass 
IRRITANT
HS Code 
29333990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H312Harmful in contact with skin

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TCI Chemical
Product number
A1502
Product name
2-Amino-3,5-dichloropyridine
Purity
>98.0%(GC)(T)
Packaging
5g
Price
$25
Updated
2025/07/31
TCI Chemical
Product number
A1502
Product name
2-Amino-3,5-dichloropyridine
Purity
>98.0%(GC)(T)
Packaging
25g
Price
$77
Updated
2025/07/31
TRC
Product number
D438170
Product name
3,5-Dichloropyridin-2-amine
Packaging
100mg
Price
$45
Updated
2021/12/16
Apolloscientific
Product number
OR4268
Product name
2-Amino-3,5-dichloropyridine
Purity
97+%
Packaging
5g
Price
$15
Updated
2021/12/16
SynQuest Laboratories
Product number
3H30-5-X6
Product name
2-Amino-3,5-dichloropyridine
Purity
97.0%
Packaging
5G
Price
$16
Updated
2021/12/16
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2-Amino-3,5-dichloropyridine Chemical Properties,Usage,Production

Chemical Properties

LIGHT BEIGE TO GREY CRYSTALLINE POWDER OR FLAKES

Uses

3,5-Dichloropyridin-2-amine can be used as herbicidal active substances.

Synthesis

1072-98-6

4214-74-8

General procedure for the synthesis of 2-amino-3,5-dichloropyridine from 2-amino-5-chloropyridine: 5500 mL of a solvent mixture of DMF and methanol with a volume ratio of 2.5:1 was added to a 10L three-necked round-bottomed flask, a thermometer was mounted and configured with condensation reflux device, and a magnetic stirrer was started. 2560.8 g of 2-amino-5-chloropyridine and 6118.4 g of N-chlorosuccinimide were added sequentially, and the reaction mixture was stirred at 45 °C for 2.5 hours. The reaction progress was monitored by TLC and GC until the reaction was complete. After completion of the reaction, the solvent was removed by distillation to obtain the crude product, which was purified by recrystallization with ethanol to afford the target compound 2-amino-3,5-dichloropyridine. The product was dried in 70.5% yield and 98.20% purity (GC analysis).

References

[1] European Journal of Organic Chemistry, 2012, # 28, p. 5595 - 5604
[2] Patent: CN104016908, 2016, B. Location in patent: Paragraph 0027; 0028
[3] Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1928, vol. 60, p. 689
[4] Chem. Zentralbl., 1928, vol. 99, # II, p. 1671

2-Amino-3,5-dichloropyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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2-Amino-3,5-dichloropyridine Suppliers

Changzhou Yuxiang Chemical Co., Ltd
Tel
13809076511
Email
344679571@qq.com
Country
China
ProdList
311
Advantage
58
J & K SCIENTIFIC LTD.
Tel
18210857532; 18210857532
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
Country
China
ProdList
96815
Advantage
76
Meryer (Shanghai) Chemical Technology Co., Ltd.
Tel
4006356688 18621169109
Fax
86-21-61259102
Email
market03@meryer.com
Country
China
ProdList
40228
Advantage
62
Liaoning Tianhua Chemical Co., Ltd.
Tel
0418-6530555 2855550
Fax
+86-418-6502885
Country
China
ProdList
338
Advantage
69
Alfa Aesar
Tel
400-6106006
Fax
021-67582001/03/05
Email
saleschina@alfa-asia.com
Country
China
ProdList
30123
Advantage
84
TCI (Shanghai) Development Co., Ltd.
Tel
021-67121386
Fax
021-67121385
Email
Sales-CN@TCIchemicals.com
Country
China
ProdList
24529
Advantage
81
Energy Chemical
Tel
021-021-58432009 400-005-6266
Fax
021-58436166
Email
sales8178@energy-chemical.com
Country
China
ProdList
44801
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61
Shijiazhuang Sdyano Fine Chemical Co., Ltd.
Tel
0311-89250318 031166536426
Fax
4000311741
Email
master@sjzsdyn.com
Country
China
ProdList
2809
Advantage
65
Wuhan Chemwish Technology Co., Ltd
Tel
86-027-67849912
Fax
86-027-87531808
Email
sales@chemwish.com
Country
China
ProdList
35896
Advantage
56
Capot Chemical Co., Ltd
Tel
+86 (0) 571 85 58 67 18
Fax
0086-571-85864795
Country
China
ProdList
18207
Advantage
66
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View Lastest Price from 2-Amino-3,5-dichloropyridine manufacturers

Hebei Chuanghai Biotechnology Co., Ltd
Product
2-Amino-3,5-dichloropyridine 4214-74-8
Price
US $10.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10 mt
Release date
2024-11-28
Henan Aochuang Chemical Co.,Ltd.
Product
2-Amino-3,5-dichloropyridine 4214-74-8
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
1Ton
Release date
2022-10-13
Shaanxi Dideu Medichem Co. Ltd
Product
2-Amino-3,5-dichloropyridine 4214-74-8
Price
US $20.00-100.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
200000KG
Release date
2024-08-09

4214-74-8, 2-Amino-3,5-dichloropyridineRelated Search:


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