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3-BROMOPHENETHYL ALCOHOL

Product Name
3-BROMOPHENETHYL ALCOHOL
CAS No.
28229-69-8
Chemical Name
3-BROMOPHENETHYL ALCOHOL
Synonyms
m-Bromophenylethanol;3-Bromophenethylacohol;Benzeneethanol, 3-broMo-;3-BROMOPHENETHYL ALCOHOL;2-(3-BROMOPHENYL)ETHANOL;3-BROMOPHENYLETHYL ALCOHOL;2-(3-Bromophenyl)ethan-1-ol;3-Bromophenethylalcohol,97%;3-Bromophenethyl alcohol 97%;2-(3-Bromophenyl)ethyl Alcohol
CBNumber
CB6707761
Molecular Formula
C8H9BrO
Formula Weight
201.06
MOL File
28229-69-8.mol
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3-BROMOPHENETHYL ALCOHOL Property

Boiling point:
107-110 °C/1 mmHg (lit.)
Density 
1.478 g/mL at 25 °C (lit.)
refractive index 
n20/D 1.5732(lit.)
Flash point:
>230 °F
storage temp. 
Sealed in dry,Room Temperature
form 
Liquid
pka
14.83±0.10(Predicted)
color 
Clear colorless
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Safety

Hazard Codes 
Xi
Safety Statements 
24/25
WGK Germany 
3
Hazard Note 
Harmful/Irritant/Keep Cold
HS Code 
29062990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
394521
Product name
3-Bromophenethyl alcohol
Purity
99%
Packaging
5g
Price
$67.2
Updated
2025/07/31
Sigma-Aldrich
Product number
394521
Product name
3-Bromophenethyl alcohol
Purity
99%
Packaging
1g
Price
$25
Updated
2023/06/20
TCI Chemical
Product number
B3517
Product name
2-(3-Bromophenyl)ethyl Alcohol
Purity
>98.0%(GC)
Packaging
5g
Price
$68
Updated
2025/07/31
TCI Chemical
Product number
B3517
Product name
2-(3-Bromophenyl)ethyl Alcohol
Purity
>98.0%(GC)
Packaging
25g
Price
$334
Updated
2025/07/31
TRC
Product number
B698238
Product name
2-(3-Bromophenyl)ethanol
Packaging
500mg
Price
$65
Updated
2021/12/16
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3-BROMOPHENETHYL ALCOHOL Chemical Properties,Usage,Production

Chemical Properties

clear colorless liquid

Uses

3-Bromophenethyl alcohol may be used as a starting material in the synthesis of its mesylate derivative (m-Br-C6H4CH2CH2OMs) by treatment with mesyl chloride.

General Description

3-Bromophenethyl alcohol is a phenethyl alcohol derivative. Its enthalpy of vaporization at boiling point has been determined.

Synthesis

1878-67-7

28229-69-8

The general procedure for the synthesis of 3-bromophenylethanol using 3-bromophenylacetic acid as starting material was as follows: to a solution of 3-bromophenylacetic acid (2.00 g, 9.3 mmol) was slowly added BH3-Me2S (7 mL of a 2M THF solution, 14.0 mmol) at 0 °C. The reaction mixture was gradually warmed up to room temperature with continuous stirring for 20 hours. Upon completion of the reaction, the mixture was again cooled to 0 °C and water (10 mL) was added dropwise to quench the reaction. Subsequently, the organic layer was separated, washed with brine (20 mL), dried over anhydrous MgSO4, filtered and concentrated under reduced pressure to give a colorless oily crude product. Purification by column chromatography (eluent: 50% EtOAc in heptane solution) resulted in 3-bromophenethyl alcohol as a colorless oil (1.47 g, 79% yield). The product was detected by mass spectrometry showing m/z 224/226 [M + H]+, and the 1H NMR (300 MHz, CDCl3) data were as follows: δ 7.41-7.35 (2H, m), 7.23-7.16 (2H, m), 3.87 (2H, t, J = 6.5 Hz), 2.86 (2H, t, J = 6.5 Hz).

References

[1] Bioorganic and Medicinal Chemistry Letters, 2007, vol. 17, # 11, p. 3018 - 3022
[2] Journal of Labelled Compounds and Radiopharmaceuticals, 2007, vol. 50, # 3, p. 183 - 188
[3] Patent: WO2008/53136, 2008, A1. Location in patent: Page/Page column 38
[4] Journal of Medicinal Chemistry, 1991, vol. 34, # 9, p. 2882 - 2891
[5] Journal of Medicinal Chemistry, 1998, vol. 41, # 3, p. 358 - 378

3-BROMOPHENETHYL ALCOHOL Preparation Products And Raw materials

Raw materials

Preparation Products

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3-BROMOPHENETHYL ALCOHOL Suppliers

Americas 1 Belgium 2 China 176 Europe 1 Germany 1 India 9 Japan 1 Switzerland 2 United Kingdom 4 United States 23 Global 220
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View Lastest Price from 3-BROMOPHENETHYL ALCOHOL manufacturers

Zhuozhou Wenxi import and Export Co., Ltd
Product
3-BROMOPHENETHYL ALCOHOL 28229-69-8
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-06-27
Career Henan Chemical Co
Product
3-BROMOPHENETHYL ALCOHOL 28229-69-8
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
100KG
Release date
2019-12-25

28229-69-8, 3-BROMOPHENETHYL ALCOHOLRelated Search:

3-BROMOPHENETHYLAMINE 3-BROMOPHENETHYL ALCOHOL 3-Bromophenylacetic acid m-Bromostyrene 7,8-oxide 3-BROMO-4-METHOXYPHENYLACETIC ACID 5-BROMO-2,3-DIHYDROBENZOFURAN-7-CARBOXYLIC ACID 3-BROMO-4-HYDROXYPHENYLACETIC ACID 4-BROMOPHENETHYL ALCOHOL,p-Bromophenethyl alcohol 2-BROMOPHENETHYLALCOHOL 5-Bromo-2-nitrophenylacetic acid 5-BROMO-2-METHOXYPHENYLACETIC ACID AMINO(3-BROMOPHENYL)ACETIC ACID AMINO-(3-BROMO-4,5-DIMETHOXY-PHENYL)-ACETIC ACID 1-(3-BROMOPHENYL)CYCLOPENTANECARBOXYLIC ACID 5,7-DIBROMO-2,3-DIHYDROBENZOFURAN AMINO(3-BROMO-4-FLUOROPHENYL)ACETIC ACID 3-BROMO-4-HYDROXY-5-METHOXYPHENYLACETIC ACID AMINO(5-BROMO-2-METHOXYPHENYL)ACETIC ACID

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