ChemicalBook > CAS DataBase List > 2-BROMO-4-METHOXYPHENOL

2-BROMO-4-METHOXYPHENOL

Product Name
2-BROMO-4-METHOXYPHENOL
CAS No.
17332-12-6
Chemical Name
2-BROMO-4-METHOXYPHENOL
Synonyms
2-BROMO-4-METHOXYPHENOL;Phenol, 3-bromo-4-methoxy-;3-Bromo-4-methoxyphenol 98%
CBNumber
CB6717618
Molecular Formula
C7H7BrO2
Formula Weight
203.03
MOL File
17332-12-6.mol
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2-BROMO-4-METHOXYPHENOL Property

Melting point:
47°
Boiling point:
281.1±20.0 °C(Predicted)
Density 
1.585±0.06 g/cm3(Predicted)
storage temp. 
Inert atmosphere,Room Temperature
pka
9.49±0.18(Predicted)
Appearance
Light brown to black Solid
InChI
InChI=1S/C7H7BrO2/c1-10-7-3-2-5(9)4-6(7)8/h2-4,9H,1H3
InChIKey
NOJOUQQJSGRBMN-UHFFFAOYSA-N
SMILES
C1(O)=CC=C(OC)C(Br)=C1
CAS DataBase Reference
17332-12-6(CAS DataBase Reference)
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Safety

HazardClass 
IRRITANT
HS Code 
2909500090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
B683810
Product name
3-Bromo-4-Methoxyphenol
Packaging
1g
Price
$60
Updated
2021/12/16
TRC
Product number
B683810
Product name
3-Bromo-4-Methoxyphenol
Packaging
2.5g
Price
$85
Updated
2021/12/16
TRC
Product number
B683810
Product name
3-Bromo-4-Methoxyphenol
Packaging
5g
Price
$140
Updated
2021/12/16
Matrix Scientific
Product number
072744
Product name
3-Bromo-4-methoxyphenol
Purity
95+%
Packaging
1g
Price
$51
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB139866
Product name
3-Bromo-4-methoxyphenol
Packaging
1g
Price
$100
Updated
2021/12/16
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2-BROMO-4-METHOXYPHENOL Chemical Properties,Usage,Production

Uses

3-Bromo-4-methoxyphenol is a malate dehyrogenase inhibitor.

Synthesis

124764-37-0

17332-12-6

General procedure for the synthesis of 3-bromo-4-methoxyphenol from 3-bromo-4-methoxyphenyl acetate: a solution of potassium hydroxide (290 mg, 5.19 mmol) in water (2.5 mL) was added to a solution of 3-bromo-4-methoxyphenyl acetate (1.2 g, 4.9 mmol) in methanol (18.5 mL). The reaction mixture was stirred at room temperature for 30 min, followed by removal of the solvent under reduced pressure. Water (40 mL) was added to the residue and 1.2 M aqueous hydrochloric acid (4.3 mL) was added dropwise until the mixture was acidic. The mixture was extracted with dichloromethane (2 x 40 mL), the organic phases were combined and dried over anhydrous sodium sulfate. After filtration, the filtrate was evaporated under reduced pressure to give 3-bromo-4-methoxyphenol (976 mg, 98% yield) as a light yellow solid.LCMS analysis (Method A): retention time (RT) = 2.11 min; no ionization was observed.TLC analysis: Rf = 0.28 (unfolding reagent ratio 1:4 ethyl acetate:hexane).

References

[1] Patent: WO2009/109743, 2009, A1. Location in patent: Page/Page column 37; 38
[2] Patent: CN105001107, 2016, B. Location in patent: Paragraph 0045; 0047
[3] Patent: WO2004/16621, 2004, A1. Location in patent: Page 31

2-BROMO-4-METHOXYPHENOL Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-BROMO-4-METHOXYPHENOL manufacturers

Hebei Chuanghai Biotechnology Co., Ltd
Product
2-BROMO-4-METHOXYPHENOL 17332-12-6
Price
US $10.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10 mt
Release date
2024-11-05
Henan Bao Enluo International TradeCo.，LTD
Product
2-BROMO-4-METHOXYPHENOL 17332-12-6
Price
US $50.00/kg
Min. Order
1kg
Purity
99.9%
Supply Ability
10000MT
Release date
2023-08-02
Honest Joy Holdings Limited
Product
3-Bromo-4-methoxyphenol 17332-12-6
Price
US $0.00/KG
Min. Order
1KG
Purity
98.5%
Supply Ability
100 tons
Release date
2022-01-17

17332-12-6, 2-BROMO-4-METHOXYPHENOLRelated Search:

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  • 2-BROMO-4-METHOXYPHENOL
  • 3-Bromo-4-methoxyphenol 98%
  • Phenol, 3-bromo-4-methoxy-
  • 17332-12-6
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