ChemicalBook > CAS DataBase List > 1-BROMO-2,4-DIMETHYL-5-NITROBENZENE

1-BROMO-2,4-DIMETHYL-5-NITROBENZENE

Product Name
1-BROMO-2,4-DIMETHYL-5-NITROBENZENE
CAS No.
69383-59-1
Chemical Name
1-BROMO-2,4-DIMETHYL-5-NITROBENZENE
Synonyms
4-BROMO-6-NITRO-M-XYLENE;2-NITRO-4-BROMO-M-XYLENE;5-Bromo-2,4-dimethylnitrobenzene;1-BROMO-2,4-DIMETHYL-5-NITROBENZENE;Benzene, 1-bromo-2,4-dimethyl-5-nitro-;1-BROMO-2,4-DIMETHYL-5-NITROBENZENE ISO 9001：2015 REACH;1-Bromo-2,4-dimethyl-5-nitrobenzene, 4-Bromo-6-nitro-m-xylene;5-BroMo-2,4-diMethylnitrobenzene (1-BroMo-2,4-diMethyl-5-nitrobenzene)
CBNumber
CB6721477
Molecular Formula
C8H8BrNO2
Formula Weight
230.06
MOL File
69383-59-1.mol
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1-BROMO-2,4-DIMETHYL-5-NITROBENZENE Property

Melting point:
54-56°C
Boiling point:
293.6±35.0 °C(Predicted)
Density 
1.533±0.06 g/cm3(Predicted)
storage temp. 
2-8°C
form 
Solid
color 
Pale yellow
Water Solubility 
Slightly soluble in water.
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Safety

Risk Statements 
20/21/22
Safety Statements 
24/25-36/37/39
HazardClass 
6.1
HS Code 
2904990090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H312Harmful in contact with skin

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC
Product number
B691658
Product name
1-Bromo-2,4-dimethyl-5-nitrobenzene
Packaging
100mg
Price
$45
Updated
2021/12/16
Apolloscientific
Product number
OR6965
Product name
1-Bromo-2,4-dimethyl-5-nitrobenzene
Packaging
5g
Price
$51
Updated
2021/12/16
SynQuest Laboratories
Product number
4754-9-X2
Product name
5-Bromo-2,4-dimethylnitrobenzene
Packaging
5G
Price
$56
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB70937
Product name
4-Bromo-6-nitro-m-xylene
Packaging
5G
Price
$70
Updated
2021/12/16
AK Scientific
Product number
X8363
Product name
5-Bromo-2,4-dimethylnitrobenzene
Packaging
5g
Price
$97
Updated
2021/12/16
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1-BROMO-2,4-DIMETHYL-5-NITROBENZENE Chemical Properties,Usage,Production

Uses

It is an important organic intermediate. It can be used in agrochemical, pharmaceutical and dyestuff field.

Synthesis

583-70-0

69383-59-1

General procedure for the synthesis of 5-bromo-2,4-dimethylnitrobenzene from 2,4-dimethylbromobenzene: 1-bromo-2,4-dimethylbenzene (9 g, 48.6 mmol) was slowly added to a 60% solution of nitric acid (100 mL) at room temperature. The reaction mixture was stirred continuously at room temperature overnight. Upon completion of the reaction, the mixture was carefully poured into ice water and extracted with ethyl acetate (EtOAc). After separation of the organic phase, it was dried over anhydrous sodium sulfate (Na2SO4) and subsequently concentrated under reduced pressure to afford the crude product 1-bromo-2,4-dimethyl-5-nitrobenzene (6.5 g). The product can be used directly in the subsequent reaction steps without further purification.

References

[1] Journal of the Indian Chemical Society, 1935, vol. 12, p. 540
[2] Patent: WO2013/117522, 2013, A1. Location in patent: Page/Page column 42
[3] Patent: US2015/18367, 2015, A1. Location in patent: Paragraph 0189

1-BROMO-2,4-DIMETHYL-5-NITROBENZENE Preparation Products And Raw materials

Raw materials

Preparation Products

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1-BROMO-2,4-DIMETHYL-5-NITROBENZENE Suppliers

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View Lastest Price from 1-BROMO-2,4-DIMETHYL-5-NITROBENZENE manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
5-Bromo-2,4-dimethylnitrobenzene 69383-59-1
Price
US $0.00-0.00/Kg
Min. Order
1KG
Purity
99.0%
Supply Ability
100 tons
Release date
2020-01-10

69383-59-1, 1-BROMO-2,4-DIMETHYL-5-NITROBENZENERelated Search:

5-BROMO-2,4-DIMETHOXYPYRIMIDINE 1-BROMO-2,4-DIFLUORO-5-NITROBENZENE Nitrobenzene Xylene 3-Bromo-4-methylaniline 2-Bromo-4-nitrotoluene 2-BROMO-4-NITRO-1,3,5-TRIMETHYLBENZENE 4-Bromo-2-nitrotoluene 2,4-Dimethylbromobenzene 5-Bromo-2-methylaniline 1-bromo-2,3-dimethyl-4-nitrobenzene 1-BROMO-2,4-DIMETHYL-5-NITROBENZENE 5-bromo-2,4-dimethylphenylamine 1-bromo-2,5-dimethyl-4-nitrobenzene 2-bromo-1,3-dimethyl-5-nitrobenzene 1-bromo-4,5-dimethyl-2-nitrobenzene 2-bromo-1,5-dimethyl-3-nitrobenzene 2-BROMO-3,4-DIMETHYL-1-NITROBENZENE

  • 2-NITRO-4-BROMO-M-XYLENE
  • 1-BROMO-2,4-DIMETHYL-5-NITROBENZENE
  • 4-BROMO-6-NITRO-M-XYLENE
  • 5-Bromo-2,4-dimethylnitrobenzene
  • 1-Bromo-2,4-dimethyl-5-nitrobenzene, 4-Bromo-6-nitro-m-xylene
  • 5-BroMo-2,4-diMethylnitrobenzene (1-BroMo-2,4-diMethyl-5-nitrobenzene)
  • Benzene, 1-bromo-2,4-dimethyl-5-nitro-
  • 1-BROMO-2,4-DIMETHYL-5-NITROBENZENE ISO 9001：2015 REACH
  • 69383-59-1
  • Aromatic Hydrocarbons (substituted) & Derivatives