3-BROMO-5-PHENYLPYRIDINE
- Product Name
- 3-BROMO-5-PHENYLPYRIDINE
- CAS No.
- 142137-17-5
- Chemical Name
- 3-BROMO-5-PHENYLPYRIDINE
- Synonyms
- 106472;3-BROMO-5-PHENYLPYRIDI;5-Bromo-3-Phenylpyridine;3-BROMO-5-PHENYLPYRIDINE;Pyridine, 3-broMo-5-phenyl-
- CBNumber
- CB6728698
- Molecular Formula
- C11H8BrN
- Formula Weight
- 234.09
- MOL File
- 142137-17-5.mol
3-BROMO-5-PHENYLPYRIDINE Property
- Melting point:
- 46.0 to 50.0 °C
- Boiling point:
- 101°C(lit.)
- storage temp.
- Inert atmosphere,Room Temperature
- form
- powder to crystal
- color
- White to Almost white
Safety
- HS Code
- 2933.39.9200
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- B5151
- Product name
- 3-Bromo-5-phenylpyridine
- Purity
- >98.0%(GC)(T)
- Packaging
- 1g
- Price
- $224
- Updated
- 2025/07/31
- Product number
- B5151
- Product name
- 3-Bromo-5-phenylpyridine
- Purity
- >98.0%(GC)(T)
- Packaging
- 200mg
- Price
- $76
- Updated
- 2025/07/31
- Product number
- B997420
- Product name
- 3-Bromo-5-phenylpyridine
- Packaging
- 5mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- FB145011
- Product name
- 3-Bromo-5-phenylpyridine
- Packaging
- 50mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- FB145011
- Product name
- 3-Bromo-5-phenylpyridine
- Packaging
- 100mg
- Price
- $80
- Updated
- 2021/12/16
3-BROMO-5-PHENYLPYRIDINE Chemical Properties,Usage,Production
Synthesis
625-92-3
98-80-6
142137-17-5
A mixture of tetrakis(triphenylphosphine)palladium(0) (1.45 g, 1.25 mmol) and potassium carbonate (17.5 g, 127 mmol) was added as 3,5-dibromopyridine (10.0 g, 42.2 mmol) and phenylboronic acid (4.6 g, 38.0 mmol). The reaction mixture was dissolved in a solvent mixture of water (63 ml) and 1,2-dimethoxyethane (126 ml) and the reaction was stirred under reflux conditions overnight. Upon completion of the reaction, the reaction was neutralized by addition of aqueous sodium hydroxide (1M, 60 ml), followed by extraction with ether (100 ml) twice and combining the organic phases. Purification was carried out by silica gel column chromatography using dichloromethane as solvent to afford the target product 3-bromo-5-phenylpyridine. The yield was 6.1 g in 68% yield and the melting point was 42-44 °C.
References
[1] Journal of Materials Chemistry C, 2014, vol. 2, # 47, p. 10129 - 10137
[2] Patent: US2004/72823, 2004, A1. Location in patent: Page/Page column 20
[3] Patent: US2004/72823, 2004, A1. Location in patent: Page/Page column 15
[4] Bioorganic and Medicinal Chemistry Letters, 2013, vol. 23, # 14, p. 4145 - 4149
[5] Organic and Biomolecular Chemistry, 2016, vol. 14, # 24, p. 5820 - 5825
3-BROMO-5-PHENYLPYRIDINE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-BROMO-5-PHENYLPYRIDINE manufacturers
- Product
- 3-BROMO-5-PHENYLPYRIDINE 142137-17-5
- Price
- US $35.00-25.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 20 Ton
- Release date
- 2023-11-08
- Product
- [1,1'-Biphenyl]-2,4-diol 142137-17-5
- Price
- US $35.00-25.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 20 Ton
- Release date
- 2023-11-08
- Product
- 3-BROMO-5-PHENYLPYRIDINE 142137-17-5
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 200kg
- Release date
- 2019-12-26