METHYL 2-METHOXY-6-METHYLBENZOATE
- Product Name
- METHYL 2-METHOXY-6-METHYLBENZOATE
- CAS No.
- 79383-44-1
- Chemical Name
- METHYL 2-METHOXY-6-METHYLBENZOATE
- Synonyms
- METHYL 2-METHOXY-6-METHYLBENZOATE;2-Methoxy-6-Methyl-benzoic acid Methyl ester;Benzoic acid, 2-Methoxy-6-Methyl-, Methyl ester
- CBNumber
- CB6751007
- Molecular Formula
- C10H12O3
- Formula Weight
- 180.2
- MOL File
- 79383-44-1.mol
METHYL 2-METHOXY-6-METHYLBENZOATE Property
- Boiling point:
- 95-96 °C(Press: 0.5 Torr)
- Density
- 1.075±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- Light yellow to yellow Liquid
Safety
- HS Code
- 2918999090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M356755
- Product name
- methyl2-methoxy-6-methylbenzoate
- Packaging
- 500mg
- Price
- $200
- Updated
- 2021/12/16
- Product number
- J57236
- Product name
- Methyl2-methoxy-6-methylbenzoate
- Packaging
- 1g
- Price
- $80
- Updated
- 2021/12/16
- Product number
- 077350
- Product name
- Methyl 2-methoxy-6-methylbenzoate
- Packaging
- 500mg
- Price
- $252
- Updated
- 2021/12/16
- Product number
- 077350
- Product name
- Methyl 2-methoxy-6-methylbenzoate
- Packaging
- 1g
- Price
- $315
- Updated
- 2021/12/16
- Product number
- J57236
- Product name
- Methyl2-methoxy-6-methylbenzoate
- Packaging
- 10g
- Price
- $420
- Updated
- 2021/12/16
METHYL 2-METHOXY-6-METHYLBENZOATE Chemical Properties,Usage,Production
Synthesis
6161-65-5
74-88-4
79383-44-1
General procedure for the synthesis of methyl 2-methoxy-6-methylbenzoate from 2-methoxy-6-methylbenzoic acid and iodomethane: To a solution of 2-methoxy-6-methylbenzoic acid (1.0 eq.) in N,N-dimethylformamide (DMF, 3.8 mL/mmol 2-methoxy-6-methylbenzoic acid) was added iodomethane (3.0-6.0 eq.) and potassium carbonate ( K2CO3, 2.5-5.0 eq.). The reaction mixture was heated to 70 °C and stirred for 17-18 hours. Upon completion of the reaction, the mixture was cooled to room temperature and the reaction was quenched by addition of water (H2O). The organic phase was extracted with ethyl acetate (EtOAc), the organic layers were combined, dried over anhydrous magnesium sulfate (MgSO4) and concentrated under reduced pressure in a fume hood to give the target product methyl 2-methoxy-6-methylbenzoate. Precautions: Iodomethane is toxic and carcinogenic, the operation should wear gloves and be carried out in a well-ventilated fume hood.
References
[1] Tetrahedron, 2018, vol. 74, # 2, p. 224 - 239
[2] Bioorganic and Medicinal Chemistry Letters, 2013, vol. 23, # 1, p. 360 - 365
METHYL 2-METHOXY-6-METHYLBENZOATE Preparation Products And Raw materials
Raw materials
Preparation Products
METHYL 2-METHOXY-6-METHYLBENZOATE Suppliers
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