TERT-BUTYL 4-BROMOBENZYLCARBAMATE
- Product Name
- TERT-BUTYL 4-BROMOBENZYLCARBAMATE
- CAS No.
- 68819-84-1
- Chemical Name
- TERT-BUTYL 4-BROMOBENZYLCARBAMATE
- Synonyms
- N-BOC-4-broMobenzylaMine;4-Bromo-N-BOC-benzylamine;TERT-BUTYL 4-BROMOBENZYLCARBAMATE;tert-Butyl 4-bromobenzylcarbamate 98%;tert-Butyl N-(4-bromobenzyl)carbamate;tert-butyl N-[(4-bromophenyl)methyl]carbamate;N-(4-Bromobenzyl)carbamic acid tert-butyl ester;(4-BROMO-BENZYL)-CARBAMIC ACID TERT-BUTYL ESTER;Carbamic acid, (4-bromophenyl)methyl-, 1,1-dimethylethyl ester;N-[(4-Bromophenyl)methyl]-carbamic acid 1,1-dimethylethyl ester
- CBNumber
- CB6838195
- Molecular Formula
- C12H16BrNO2
- Formula Weight
- 286.16
- MOL File
- 68819-84-1.mol
TERT-BUTYL 4-BROMOBENZYLCARBAMATE Property
- Melting point:
- 86-88℃
- Boiling point:
- 374.3±25.0 °C(Predicted)
- Density
- 1.319±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- form
- solid
- pka
- 12.05±0.46(Predicted)
- color
- Off-white
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
N-Bromosuccinimide Price
- Product number
- B694555
- Product name
- tert-Butyl4-Bromobenzylcarbamate
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- FB155794
- Product name
- tert-Butyl 4-bromobenzylcarbamate
- Packaging
- 1g
- Price
- $80
- Updated
- 2021/12/16
- Product number
- CS-W005364
- Product name
- tert-Butyl4-bromobenzylcarbamate
- Purity
- 99.98%
- Packaging
- 10g
- Price
- $110
- Updated
- 2021/12/16
- Product number
- FB155794
- Product name
- tert-Butyl 4-bromobenzylcarbamate
- Packaging
- 2g
- Price
- $130
- Updated
- 2021/12/16
- Product number
- OR315540
- Product name
- tert-Butyl4-bromobenzylcarbamate
- Purity
- 98%
- Packaging
- 5g
- Price
- $166
- Updated
- 2021/12/16
TERT-BUTYL 4-BROMOBENZYLCARBAMATE Chemical Properties,Usage,Production
Synthesis
Tert-Butyl 4-bromobenzylcarbamate is prepared by the reaction of di-tert-butyl dicarbonate and 4-bromobenzylamine hydrochloride. The specific synthesis steps are as follows:
To a stirred suspension of 4-bromo-benzylamine hydrochloride (968mg, 4.35mmol) and triethylamine (0.666ml, 4.79mmol) in chloroform (15ml) was added di-tert-butyldicarbonate (949mg, 4.35mmol). The resulting solution was stirred at ambient temperature for 2h and then diluted with DCM (40ml). The organic solution was washed sequentially with 10% aqueous citric acid (40ml) and brine (40ml). The organic phase was dried over anhydrous magnesium sulfate and the filtrate evaporated at reduced pressure to afford Tert-Butyl 4-bromobenzylcarbamate (1.23g, 99%). 1H NMR 7.48-7.43 (2H, m), 7.18 (2H, d, 8.4), 4.84 (1H, br s), 4.27 (2H, d, 5.7), 1.46 (9H, s).
TERT-BUTYL 4-BROMOBENZYLCARBAMATE Preparation Products And Raw materials
Raw materials
Preparation Products
TERT-BUTYL 4-BROMOBENZYLCARBAMATE Suppliers
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View Lastest Price from TERT-BUTYL 4-BROMOBENZYLCARBAMATE manufacturers
- Product
- TERT-BUTYL 4-BROMOBENZYLCARBAMATE 68819-84-1
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100KG
- Release date
- 2020-01-02