ChemicalBook > CAS DataBase List > P-(4-PROPYLCYCLOHEXYL)PHENYLBORONIC ACID
P-(4-PROPYLCYCLOHEXYL)PHENYLBORONIC ACID
- Product Name
- P-(4-PROPYLCYCLOHEXYL)PHENYLBORONIC ACID
- CAS No.
- 156837-90-0
- Chemical Name
- P-(4-PROPYLCYCLOHEXYL)PHENYLBORONIC ACID
- Synonyms
- P-(4-PROPYLCYCLOHEXYL)PHENYLBORONIC ACID;[4-(4-Propylcyclohexyl)phenyl]boric acid;4-trans-Propylcyclohexylphenylboronic acid;Boronic acid,B-[4-(4-propylcyclohexyl)phenyl]-;trans-[4-(4-propylcyclohexyl)phenyl]boronic acid
- CBNumber
- CB71013189
- Molecular Formula
- C15H23BO2
- Formula Weight
- 246.15
- MOL File
- 156837-90-0.mol
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P-(4-PROPYLCYCLOHEXYL)PHENYLBORONIC ACID Property
- Boiling point:
- 394.9±35.0 °C(Predicted)
- Density
- 1.03±0.1 g/cm3 (20 ºC 760 Torr)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- 8.70±0.17(Predicted)
- Appearance
- White to off-white Solid
- InChI
- InChI=1S/C15H23BO2/c1-2-3-12-4-6-13(7-5-12)14-8-10-15(11-9-14)16(17)18/h8-13,17-18H,2-7H2,1H3
- InChIKey
- QTBUVZSHCNAPRT-UHFFFAOYSA-N
- SMILES
- B(C1=CC=C(C2CCC(CCC)CC2)C=C1)(O)O
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
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N-Bromosuccinimide Price
TRC
- Product number
- P835173
- Product name
- (4-(4-Propylcyclohexyl)phenyl)boronicAcid
- Packaging
- 250mg
- Price
- $45
- Updated
- 2021/12/16
AK Scientific
- Product number
- 9353AF
- Product name
- p-(4-propylcyclohexyl)thenylboronicacid
- Packaging
- 25g
- Price
- $217
- Updated
- 2021/12/16
American Custom Chemicals Corporation
- Product number
- BOR0000332
- Product name
- 4-(4-PROPYLCYCLOHEXYL)PHENYLBORONIC ACID
- Purity
- 95.00%
- Packaging
- 5G
- Price
- $909.56
- Updated
- 2021/12/16
Crysdot
- Product number
- CD41001916
- Product name
- (4-(4-Propylcyclohexyl)phenyl)boronicacid
- Purity
- 97%
- Packaging
- 100g
- Price
- $446
- Updated
- 2021/12/16
Alichem
- Product number
- 156837900
- Product name
- (4-(4-Propylcyclohexyl)phenyl)boronicacid
- Packaging
- 100g
- Price
- $463.5
- Updated
- 2021/12/16
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P-(4-PROPYLCYCLOHEXYL)PHENYLBORONIC ACID Chemical Properties,Usage,Production
Chemical Properties
White powder
Synthesis
860639-66-3
156837-90-0
Under nitrogen protection, 4-(4-propylcyclohexyl)iodobenzene (50.0 g) was added to a reaction vial with anhydrous ether (800 mL) and cooled to -70 °C. Slowly n-butyllithium (1.63 M, n-hexane solution, 112 mL) was added dropwise, and after completion of the dropwise addition, the reaction was stirred at -70 °C for 2 hours. Subsequently, a solution of diethyl ether (50.0 mL) of trimethyl borate (22.8 g) was slowly added, gradually warmed to room temperature and continued stirring for 12 hours. Upon completion of the reaction, the reaction solution was cooled to -30°C, 6N hydrochloric acid (150 mL) was slowly added, gradually warmed to room temperature and stirred for 3 hours. The reaction mixture was poured into water and the aqueous layer was extracted with ethyl acetate. The organic layers were combined, washed with saturated brine and dried over anhydrous magnesium sulfate. The organic phase was concentrated under reduced pressure and the residue was purified by recrystallization from heptane to give (4-(4-propylcyclohexyl)phenyl)boronic acid (29.2 g, 78% yield).
References
[1] Patent: EP2957554, 2015, A1. Location in patent: Paragraph 0132
P-(4-PROPYLCYCLOHEXYL)PHENYLBORONIC ACID Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from P-(4-PROPYLCYCLOHEXYL)PHENYLBORONIC ACID manufacturers
Henan Aochuang Chemical Co.,Ltd.
- Product
- P-(4-PROPYLCYCLOHEXYL)PHENYLBORONIC ACID 156837-90-0
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1ton
- Release date
- 2022-09-28
Henan Fengda Chemical Co., Ltd
- Product
- [4-(trans-4-Propylcyclohexyl)phenyl]boronic acid 156837-90-0
- Price
- US $6.00-0.60/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2024-01-18
Career Henan Chemical Co
- Product
- P-(4-PROPYLCYCLOHEXYL)PHENYLBORONIC ACID 156837-90-0
- Price
- US $7.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100KG
- Release date
- 2018-08-20
156837-90-0, P-(4-PROPYLCYCLOHEXYL)PHENYLBORONIC ACIDRelated Search:
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