4-Pyrimidinamine, 6-chloro-5-methyl- (9CI)

Product Name: 4-Pyrimidinamine, 6-chloro-5-methyl- (9CI)
CAS No.: 14394-56-0
Chemical Name: 4-Pyrimidinamine, 6-chloro-5-methyl- (9CI)
Synonyms: 6-Chloro-5-methyl-4-pyrimidinamine;6-chloro-5-methylpyrimidin-4-amine;4-Amino-6-chloro-5-methylpyrimidine;6-AMINO-4-CHLORO-5-METHYLPYRIMIDINE;4-Pyrimidinamine, 6-Chloro-5-Methyl;6-Chloro-5-methyl-pyrimidin-4-ylamine;4-Pyrimidinamine, 6-chloro-5-methyl- (9CI);4-Pyrimidinamine, 6-chloro-5-methyl- (9CI) ISO 9001：2015 REACH
CBNumber: CB71081878
Molecular Formula: C5H6ClN3
Formula Weight: 143.57
MOL File: 14394-56-0.mol

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4-Pyrimidinamine, 6-chloro-5-methyl- (9CI) Property

Melting point:: 237-238℃
Boiling point:: 292.4±35.0 °C(Predicted)
Density: 1.349±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 2.41±0.10(Predicted)
Appearance: White to off-white Solid

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Safety

HS Code: 2933599590

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H227Combustible liquid

H411Toxic to aquatic life with long lasting effects

Precautionary statements

P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.

P273Avoid release to the environment.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P370+P378In case of fire: Use … for extinction.

P391Collect spillage. Hazardous to the aquatic environment

P403+P235Store in a well-ventilated place. Keep cool.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: A617408
Product name: 6-Amino-4-chloro-5-methylpyrimidine
Packaging: 100mg
Price: $60
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC142695
Product name: 6-Chloro-5-methylpyrimidin-4-amine
Packaging: 2g
Price: $154
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: NUC0000951
Product name: 6-AMINO-4-CHLORO-5-METHYLPYRIMIDINE
Purity: 95.00%
Packaging: 250MG
Price: $163.8
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC142695
Product name: 6-Chloro-5-methylpyrimidin-4-amine
Packaging: 5G
Price: $307
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC142695
Product name: 6-Chloro-5-methylpyrimidin-4-amine
Packaging: 10g
Price: $534
Updated: 2021/12/16

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4-Pyrimidinamine, 6-chloro-5-methyl- (9CI) Chemical Properties,Usage,Production

Synthesis

4316-97-6

14394-56-0

4,6-Dichloro-5-methylpyrimidine (Sigma-Aldrich No. 595446, 5 g, 30.70 mmol) was used as starting material and dissolved in a methanol solution of 7 M ammonia (15 ml, 105 mmol). The reaction mixture was placed in a sealed vial and the reaction was stirred at 140 °C for 40 min. After completion of the reaction, the resulting white suspension was poured into a mixture of water (300 ml) and ethyl acetate (600 ml), shaken well and left to stratify. The aqueous phase was separated and extracted with ethyl acetate (3 x 600 ml). The organic phases were combined, dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure to afford the target compound 6-chloro-5-methyl-4-pyrimidinamine (3.10 g, 20.73 mmol, 68% yield) as a white solid. The product was analyzed by UPLC (retention time: 0.41 min) and the mass spectrum showed major peaks at m/z 144 ([M+H]+, 100%) and m/z 146 ([M+H]+, 33%), which was in accordance with the theoretical molecular weight of 143 (C5H6ClN3).1H NMR (400 MHz, DMSO-d6) δ (ppm): 8.06 (s, 1H) , 7.09 (bs, 2H), 2.07 (s, 3H).

References

[1] Patent: WO2009/3997, 2009, A1. Location in patent: Page/Page column 18
[2] Journal of the Chemical Society, 1947, p. 41,45

4-Pyrimidinamine, 6-chloro-5-methyl- (9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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4-Pyrimidinamine, 6-chloro-5-methyl- (9CI) Suppliers

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Shanghai ZaiQi Bio-Tech Co., Ltd.

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Chemfun Medical Technology(Shanghai) Co., Ltd.

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View Lastest Price from 4-Pyrimidinamine, 6-chloro-5-methyl- (9CI) manufacturers

Dideu Industries Group Limited

Product: 4-Pyrimidinamine, 6-chloro-5-methyl- (9CI) 14394-56-0
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons Min
Release date: 2021-12-07

Wuhan Monad Medicine Tech Co.,LTD

Product: 4-Amino-6-chloro-5-methylpyrimidine 14394-56-0
Price: US $10.00/KG
Min. Order: 1KG
Purity: 99%min
Supply Ability: 20000
Release date: 2020-12-17

Shijiazhuang tongyang Import and Export Co., LTD

Product: 4-Pyrimidinamine, 6-chloro-5-methyl- (9CI) 14394-56-0
Price: US $48.00/KG
Min. Order: 1g
Purity: 99.9%
Supply Ability: 500000kgs
Release date: 2021-08-11

14394-56-0, 4-Pyrimidinamine, 6-chloro-5-methyl- (9CI)Related Search:

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4-Pyrimidinamine, 6-Chloro-5-Methyl

6-AMINO-4-CHLORO-5-METHYLPYRIMIDINE

4-Amino-6-chloro-5-methylpyrimidine

6-Chloro-5-methyl-pyrimidin-4-ylamine

4-Pyrimidinamine, 6-chloro-5-methyl- (9CI)

6-chloro-5-methylpyrimidin-4-amine

6-Chloro-5-methyl-4-pyrimidinamine

4-Pyrimidinamine, 6-chloro-5-methyl- (9CI) ISO 9001：2015 REACH

14394-56-0

18620-69-0

Heterocycle-Pyrimidine series

PYRIMIDINE