5-CHLORO-2-(TRIFLUOROMETHYL)BENZALDEHYDE
- Product Name
- 5-CHLORO-2-(TRIFLUOROMETHYL)BENZALDEHYDE
- CAS No.
- 90381-07-0
- Chemical Name
- 5-CHLORO-2-(TRIFLUOROMETHYL)BENZALDEHYDE
- Synonyms
- 2-trifluoromethyl-5-chlorobenzaldehyde;Benzaldehyde, 5-chloro-2-(trifluoromethyl)-
- CBNumber
- CB71091013
- Molecular Formula
- C8H4ClF3O
- Formula Weight
- 208.57
- MOL File
- 90381-07-0.mol
5-CHLORO-2-(TRIFLUOROMETHYL)BENZALDEHYDE Property
- Boiling point:
- 82-86℃
- Density
- 1.423±0.06 g/cm3(Predicted)
- refractive index
- 1.4880
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- form
- liquid
- color
- Clear, colourless
- Sensitive
- Air Sensitive
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- C381705
- Product name
- 5-Chloro-2-(trifluoromethyl)benzaldehyde
- Packaging
- 50mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 074464
- Product name
- 5-Chloro-2-(trifluoromethyl)benzaldehyde
- Purity
- 95+%
- Packaging
- 1g
- Price
- $60
- Updated
- 2021/12/16
- Product number
- FC67847
- Product name
- 5-Chloro-2-(trifluoromethyl)benzaldehyde
- Packaging
- 10g
- Price
- $56
- Updated
- 2021/12/16
- Product number
- FC67847
- Product name
- 5-Chloro-2-(trifluoromethyl)benzaldehyde
- Packaging
- 25g
- Price
- $112
- Updated
- 2021/12/16
- Product number
- PC302415
- Product name
- 5-Chloro-2-(trifluoromethyl)benzaldehyde
- Purity
- 98%
- Packaging
- 5g
- Price
- $77
- Updated
- 2021/12/16
5-CHLORO-2-(TRIFLUOROMETHYL)BENZALDEHYDE Chemical Properties,Usage,Production
Synthesis
261763-21-7
90381-07-0
General procedure for the synthesis of 5-chloro-2-trifluoromethylbenzaldehyde from (5-chloro-2-trifluoromethylphenyl)methanol: (5-chloro-2-trifluoromethylphenyl)methanol (347 mg, 1.66 mmol) was dissolved in dichloromethane (10 mL). Pyridinium chlorochromate (717 mg, 3.32 mmol) was added to the solution and the reaction mixture was stirred for 2 hours at room temperature. After the reaction was completed, the reaction solution was diluted with ether and stirring was continued for 1 hour. Subsequently, the reaction mixture was filtered to remove insoluble impurities and the filtrate was concentrated to remove solvent. Finally, the crude product was purified by silica gel column chromatography using a hexane solution of 10% ethyl acetate as eluent to afford 5-chloro-2-trifluoromethylbenzaldehyde as a colorless oil (285 mg, 82% yield).1H NMR (400 MHz, MeOH-d4) δ 10.33 (s, 1H), 7.90 (s, 1H), 7.69 (d, 1H, J = 8.4 Hz), 7.54 (d, 1H, J = 8.4 Hz).
References
[1] Patent: WO2006/44454, 2006, A1. Location in patent: Page/Page column 13-14
5-CHLORO-2-(TRIFLUOROMETHYL)BENZALDEHYDE Preparation Products And Raw materials
Raw materials
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View Lastest Price from 5-CHLORO-2-(TRIFLUOROMETHYL)BENZALDEHYDE manufacturers
- Product
- 5-CHLORO-2-(TRIFLUOROMETHYL)BENZALDEHYDE 90381-07-0
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-10
- Product
- 5-CHLORO-2-(TRIFLUOROMETHYL)BENZALDEHYDE 90381-07-0
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-09
- Product
- 5-CHLORO-2-(TRIFLUOROMETHYL)BENZALDEHYDE 90381-07-0
- Price
- US $1.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 200kg
- Release date
- 2018-12-17