2-BROMO-3-CHLOROANILINE

Product Name: 2-BROMO-3-CHLOROANILINE
CAS No.: 96558-73-5
Chemical Name: 2-BROMO-3-CHLOROANILINE
Synonyms: 2-BROMO-3-CHLOROANILINE;2-broMo-3-chlorobenzenaMine;Benzenamine, 2-bromo-3-chloro;(2-Bromo-3-chlorophenyl)amine;BENZENAMINE,2-BROMO-3-CHLORO,2-Bromo-3-chloro-phenylamine,2-BROMO-3-CHLOROBENZENAMINE
CBNumber: CB71092742
Molecular Formula: C6H5BrClN
Formula Weight: 206.47
MOL File: 96558-73-5.mol

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2-BROMO-3-CHLOROANILINE Property

Melting point:: 41-43℃
Boiling point:: 277℃
Density: 1.722
Flash point:: 122℃
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
form: crystalline solid
pka: 1.48±0.10(Predicted)
color: Light to dark brown
InChI: InChI=1S/C6H5BrClN/c7-6-4(8)2-1-3-5(6)9/h1-3H,9H2
InChIKey: JHHMLFBYFNAPDZ-UHFFFAOYSA-N
SMILES: C1(N)=CC=CC(Cl)=C1Br

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Safety

RIDADR: 2811
HazardClass: 6.1
PackingGroup: Ⅲ
HS Code: 2921420090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P403+P233Store in a well-ventilated place. Keep container tightly closed.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: B415965
Product name: 2-Bromo-3-chloroaniline
Packaging: 500mg
Price: $60
Updated: 2021/12/16

TRC

Product number: B415965
Product name: 2-Bromo-3-chloroaniline
Packaging: 1g
Price: $75
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB33044
Product name: 2-Bromo-3-chloroaniline
Packaging: 5G
Price: $94
Updated: 2021/12/16

Apolloscientific

Product number: OR51860
Product name: 2-Bromo-3-chloroaniline
Purity: 98%
Packaging: 5g
Price: $63
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3630-D-00
Product name: 2-Bromo-3-chloroaniline
Purity: 98%
Packaging: 5G
Price: $69
Updated: 2021/12/16

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2-BROMO-3-CHLOROANILINE Chemical Properties,Usage,Production

Chemical Properties

2-Bromo-3-chloroaniline exhibits nonpolar properties, which allows it to bind to the stationary phase of the column and act as an electron scavenger. It reacts with the electrons released by the sample components, resulting in a measurable current.

Uses

2-Bromo-3-chloroaniline is a bromoderivative that is used as an electron detector in gas chromatography. It can also be used as an indicator for bromination reactions.

Synthesis

1463053-89-5

96558-73-5

Step B: Synthesis of 2-bromo-3-chloroaniline To a solution of tert-butyl (2-bromo-3-chlorophenyl)carbamate (0.4 g) in dichloromethane (DCM, 20 mL) was added trifluoroacetic acid (TFA, 10 mL). The reaction mixture was stirred at room temperature for 3 h. The reaction solution was subsequently concentrated by rotary evaporator. Water (10 mL) was added to the concentrated residue and the mixture was extracted with dichloromethane (2 x 20 mL). The organic phase was separated and washed sequentially with saturated aqueous sodium bicarbonate (NaHCO3) and saturated aqueous sodium chloride (NaCl), dried over anhydrous sodium sulfate (Na2SO4), and then the organic phase was concentrated to give the title compound 2-bromo-3-chloroaniline as a solid (0.2 g, 77% yield). 1H NMR (400 MHz, CDCl3) δ 7.03-6.99 (1H, m), 6.85-6.83 (1H, d, J = 8.0 Hz), 6.65-6.63 (1H, d, J = 8.0 Hz), 4.25 (2H, s).

References

[1] Patent: WO2013/148603, 2013, A1. Location in patent: Paragraph 0185-0186

2-BROMO-3-CHLOROANILINE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-BROMO-3-CHLOROANILINE Suppliers

China 130 India 2 United Kingdom 3 United States 8 Global 143

Changzhou Anxuan Chemical, Co., Ltd.

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Wuhan ariel chemical Co., LTD.

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View Lastest Price from 2-BROMO-3-CHLOROANILINE manufacturers

Career Henan Chemical Co

Product: 2-BROMO-3-CHLOROANILINE 96558-73-5
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100kg
Release date: 2019-07-11

96558-73-5, 2-BROMO-3-CHLOROANILINERelated Search:

2-BROMO-5-METHOXYPHENOL 2-BROMO-5-IODOPHENOL 2,6-DIBROMO-3-CHLORO-4-[1,3]OXAZOLO[4,5-B]PYRIDIN-2-YLANILINE 3-CHLORO-2,6-DIBROMO-4-FLUOROANILINE 4-(1,3-BENZOTHIAZOL-2-YL)-2,6-DIBROMO-3-CHLOROANILINE 2-Amino-4-chloro-3,5-dibromotoluene 1-(2,6-dibromo-3-chloro-4-fluorophenyl)hydrazine 3-Chloro-2,4-dibromo-6-methylphenylisothiocyanate 2,4-DIBROMO-3,6-DICHLOROANILINE 3-CHLORO-2,6-DIBROMO-4-METHYLANILINE N-(2,6-DIBROMO-3-CHLORO-4-METHYLPHENYL)OXO(DIPHENYL)PHOSPHORANECARBOTHIOAMIDE 3-Chloro-2,6-dibromo-4-methylphenylisothiocyanate 2,6-DIBROMO-3-CHLOROBENZENAMINE

2-BROMO-3-CHLOROANILINE

(2-Bromo-3-chlorophenyl)amine

2-broMo-3-chlorobenzenaMine

Benzenamine, 2-bromo-3-chloro

BENZENAMINE,2-BROMO-3-CHLORO,2-Bromo-3-chloro-phenylamine,2-BROMO-3-CHLOROBENZENAMINE

96558-73-5