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Methyl p-nitrophenylacetate

Appearance
Product Name
Methyl p-nitrophenylacetate
CAS No.
2945-08-6
Chemical Name
Methyl p-nitrophenylacetate
Synonyms
Methyl 2-(4-nitrophenyl);Methyl p-nitrophenylacetate;Methyl 2-(4-nitrophenyl)acetate;4-Nitrophenylacetic acid methyl ester;4-Nitrobenzeneacetic acid methyl ester;(4-Nitrophenyl)acetic acid methyl ester;2-(p-Nitrophenyl)acetic acid methyl ester;Benzeneacetic acid, 4-nitro-, methyl ester
CBNumber
CB71180214
Molecular Formula
C9H9NO4
Formula Weight
195.17
MOL File
2945-08-6.mol
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Methyl p-nitrophenylacetate Property

Melting point:
52.4-53.3 °C
Boiling point:
308.6±17.0 °C(Predicted)
Density 
1.266±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
form 
solid
color 
Off-white
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Safety

HS Code 
2915390090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific
Product number
2998AB
Product name
Methyl2-(4-nitrophenyl)acetate
Packaging
5g
Price
$171
Updated
2021/12/16
Matrix Scientific
Product number
113919
Product name
Methyl (4-nitrophenyl)acetate
Purity
97%
Packaging
1g
Price
$354
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0392884
Product name
METHYL-2-(4-NITROPHENYL)ACETATE
Purity
95.00%
Packaging
5MG
Price
$504.09
Updated
2021/12/16
AK Scientific
Product number
4995AQ
Product name
methyl2-(4-nitrophenyl)acetate
Packaging
25g
Price
$590
Updated
2021/12/16
Alichem
Product number
2945086
Product name
Methyl2-(4-nitrophenyl)acetate
Packaging
25g
Price
$366.12
Updated
2021/12/16
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Methyl p-nitrophenylacetate Chemical Properties,Usage,Production

Appearance

a pale orange oil

Synthesis

4-nitrophenylacetic acid(2.00 g, 11 mmol) was added to a clean carousel tube. Dimethyl carbonate (3 mL, 3.21 g, 35.6 mmol) was added, and the reaction was heated at reflux overnight. The brown solution was allowed to cool, and poured in to aqueous sodium bicarbonate (10%, 10 mL) while stirring. The resulting mixture was extracted with ethyl acetate (3 x 10 mL). The combined organic layers were washed with water and brine (10 mL each), and dried over anhydrous magnesium sulphate. After filtration and evaporation of the solvents, proton NMR analysis showed the product had formed, and none of the precursor acid remained. No further purification was performed. This gave methyl p-nitrophenylacetate as a pale orange oil (1.929 g, 9.89 mmol, 90%)): 1H NMR (400 MHz, CDCl 3 ) |? 8.20 (d, J = 8.6 Hz, 2H), 7.46 (d, J = 8.6 Hz, 2H, 3.74 (s, 2H), 3.73 (s, 3H).

Methyl p-nitrophenylacetate Preparation Products And Raw materials

Raw materials

Preparation Products

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Methyl p-nitrophenylacetate Suppliers

Accela ChemBio Inc.
Tel
+1-858-6993322
Fax
(+1)-858-876-1948
Email
info@accelachem.com
Country
United States
ProdList
19039
Advantage
58
Alchem Pharmtech,Inc.
Tel
8485655694
Email
sales@alchempharmtech.com
Country
United States
ProdList
63687
Advantage
58
Aladdin Scientific
Tel
Email
tp@aladdinsci.com
Country
United States
ProdList
57505
Advantage
58
Aceschem Inc.
Tel
+1-817863-6948 +1-(817)863-6948
Email
sales@aceschem.com
Country
United States
ProdList
19632
Advantage
58
Synthonix Inc
Tel
--
Fax
--
Email
info@synthonix.com
Country
United States
ProdList
6872
Advantage
58
SynQuest Laboratories, Inc.
Tel
--
Fax
--
Email
info@synquestlabs.com
Country
United States
ProdList
6871
Advantage
62
Matrix Scientific
Tel
--
Fax
--
Email
sales@matrixscientific.com
Country
United States
ProdList
6632
Advantage
80