Methyl p-nitrophenylacetate
Appearance- Product Name
- Methyl p-nitrophenylacetate
- CAS No.
- 2945-08-6
- Chemical Name
- Methyl p-nitrophenylacetate
- Synonyms
- Methyl 2-(4-nitrophenyl);Methyl p-nitrophenylacetate;Methyl 2-(4-nitrophenyl)acetate;4-Nitrophenylacetic acid methyl ester;4-Nitrobenzeneacetic acid methyl ester;(4-Nitrophenyl)acetic acid methyl ester;2-(p-Nitrophenyl)acetic acid methyl ester;Benzeneacetic acid, 4-nitro-, methyl ester
- CBNumber
- CB71180214
- Molecular Formula
- C9H9NO4
- Formula Weight
- 195.17
- MOL File
- 2945-08-6.mol
Methyl p-nitrophenylacetate Property
- Melting point:
- 52.4-53.3 °C
- Boiling point:
- 308.6±17.0 °C(Predicted)
- Density
- 1.266±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- form
- solid
- color
- Off-white
Safety
- HS Code
- 2915390090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 2998AB
- Product name
- Methyl2-(4-nitrophenyl)acetate
- Packaging
- 5g
- Price
- $171
- Updated
- 2021/12/16
- Product number
- 113919
- Product name
- Methyl (4-nitrophenyl)acetate
- Purity
- 97%
- Packaging
- 1g
- Price
- $354
- Updated
- 2021/12/16
- Product number
- CHM0392884
- Product name
- METHYL-2-(4-NITROPHENYL)ACETATE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $504.09
- Updated
- 2021/12/16
- Product number
- 4995AQ
- Product name
- methyl2-(4-nitrophenyl)acetate
- Packaging
- 25g
- Price
- $590
- Updated
- 2021/12/16
- Product number
- 2945086
- Product name
- Methyl2-(4-nitrophenyl)acetate
- Packaging
- 25g
- Price
- $366.12
- Updated
- 2021/12/16
Methyl p-nitrophenylacetate Chemical Properties,Usage,Production
Appearance
a pale orange oil
Synthesis
4-nitrophenylacetic acid(2.00 g, 11 mmol) was added to a clean
carousel tube. Dimethyl carbonate (3 mL, 3.21 g, 35.6 mmol) was
added, and the reaction was heated at reflux overnight. The brown
solution was allowed to cool, and poured in to aqueous sodium
bicarbonate (10%, 10 mL) while stirring. The resulting mixture was
extracted with ethyl acetate (3 x 10 mL). The combined organic layers
were washed with water and brine (10 mL each), and dried over anhydrous
magnesium sulphate. After filtration and evaporation of the solvents,
proton NMR analysis showed the product had formed, and none of the
precursor acid remained. No further purification was performed. This
gave methyl p-nitrophenylacetate as a pale orange oil (1.929 g, 9.89
mmol, 90%)): 1H NMR (400 MHz, CDCl 3 ) |? 8.20 (d, J = 8.6 Hz, 2H), 7.46 (d,
J = 8.6 Hz, 2H, 3.74 (s, 2H), 3.73 (s, 3H).
Methyl p-nitrophenylacetate Preparation Products And Raw materials
Raw materials
Preparation Products
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