TERT-BUTYL N-(4-IODOPHENYL)CARBAMATE

Product Name: TERT-BUTYL N-(4-IODOPHENYL)CARBAMATE
CAS No.: 159217-89-7
Chemical Name: TERT-BUTYL N-(4-IODOPHENYL)CARBAMATE
Synonyms: TERT-BUTYL 4-IODOPHENYLCARBAMATE;N-BOC-4-IODOANILIN;N-BOC-4-IODOANILINE;N-Boc-4-iodoaniline;ert-Butyl(4-iodophenyl)carbamate;TERT-BUTYL N-(4-IODOPHENYL)CARBAMATE;N-(tert-Butoxycarbonyl)-4-iodoaniline;(4-Iodophenyl)carbamic acid tert-butyl ester;N-(4-iodophenyl)carbamic acid tert-butyl ester;Carbamic acid, N-(4-iodophenyl)-, 1,1-dimethylethyl ester
CBNumber: CB7118623
Molecular Formula: C11H14INO2
Formula Weight: 319.14
MOL File: 159217-89-7.mol

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TERT-BUTYL N-(4-IODOPHENYL)CARBAMATE Property

Melting point:: 144-148 °C
Boiling point:: 299.0±23.0 °C(Predicted)
Density: 1.591±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
form: solid
pka: 13.12±0.70(Predicted)
Appearance: White to off-white Solid
Sensitive: Light Sensitive

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Safety

Hazard Codes: Xn,N
Risk Statements: 22-43-50
Safety Statements: 36/37-61
RIDADR: UN 3077 9 / PGIII
WGK Germany: 3
HS Code: 2924297099

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H317May cause an allergic skin reaction

H410Very toxic to aquatic life with long lasting effects

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P273Avoid release to the environment.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 761826
Product name: N-Boc-4-iodoaniline
Purity: 95%
Packaging: 5g
Price: $201
Updated: 2023/06/20

Sigma-Aldrich

Product number: 761826
Product name: N-Boc-4-iodoaniline
Purity: 95%
Packaging: 1g
Price: $41.2
Updated: 2022/05/15

American Custom Chemicals Corporation

Product number: HCH0027219
Product name: TERT-BUTYL N-(4-IODOPHENYL)CARBAMATE
Purity: 95.00%
Packaging: 5G
Price: $830.74
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0027219
Product name: TERT-BUTYL N-(4-IODOPHENYL)CARBAMATE
Purity: 95.00%
Packaging: 25G
Price: $1257.63
Updated: 2021/12/16

Oakwood

Product number: 010776
Product name: tert-ButylN-(4-iodophenyl)carbamate
Purity: 95%
Packaging: 100g
Price: $345
Updated: 2021/12/16

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TERT-BUTYL N-(4-IODOPHENYL)CARBAMATE Chemical Properties,Usage,Production

Synthesis

24424-99-5

540-37-4

159217-89-7

GENERAL STEPS: The reaction was carried out in a 50 mL round-bottomed flask at 80°C under reduced pressure for 10 minutes. In a typical experiment, 5 mmol of p-iodoaniline was mixed with 5 mmol of di-tert-butyl dicarbonate and the reaction lasted for 10 minutes. Upon completion of the reaction, the solvent was removed by rotary evaporator under vacuum to give tert-butyl (4-iodophenyl)carbamate.

References

[1] Bioorganic and Medicinal Chemistry Letters, 2006, vol. 16, # 22, p. 5864 - 5869
[2] Research on Chemical Intermediates, 2017, vol. 43, # 3, p. 1355 - 1363
[3] Chemical Communications, 2013, vol. 49, # 61, p. 6909 - 6911
[4] Patent: WO2004/12736, 2004, A1. Location in patent: Page/Page column 24
[5] Organic Letters, 2018, vol. 20, # 7, p. 1693 - 1697

TERT-BUTYL N-(4-IODOPHENYL)CARBAMATE Preparation Products And Raw materials

Raw materials

Preparation Products

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TERT-BUTYL N-(4-IODOPHENYL)CARBAMATE Suppliers

China 70 France 2 India 2 Japan 1 United Kingdom 5 United States 10 Global 90

J & K SCIENTIFIC LTD.

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159217-89-7, TERT-BUTYL N-(4-IODOPHENYL)CARBAMATERelated Search:

4-Chlorophenethylamine 5-IODO-2,3-DIHYDRO-INDOLE-1-CARBOXYLIC ACID TERT-BUTYL ESTER TERT-BUTYL N-(4-IODOPHENYL)CARBAMATE TERT-BUTYL 4-IODO-2-METHYLPHENYLCARBAMATE BOC-2-AMINO-5-IODOBENZOIC ACID (2-AMINO-4-IODO-PHENYL)-CARBAMIC ACID TERT-BUTYL ESTER TERT-BUTYL N-(2-FLUORO-4-IODOPHENYL)CARBAMATE TERT-BUTYL 2-CHLORO-4-IODOPHENYLCARBAMATE

N-(tert-Butoxycarbonyl)-4-iodoaniline

N-BOC-4-IODOANILINE

TERT-BUTYL 4-IODOPHENYLCARBAMATE

TERT-BUTYL N-(4-IODOPHENYL)CARBAMATE

(4-Iodophenyl)carbamic acid tert-butyl ester

N-(4-iodophenyl)carbamic acid tert-butyl ester

Carbamic acid, N-(4-iodophenyl)-, 1,1-dimethylethyl ester

ert-Butyl(4-iodophenyl)carbamate

<i>N</i>-Boc-4-iodoaniline

N-BOC-4-IODOANILIN

159217-89-7

C11H14INO2