TERT-BUTYL N-(4-IODOPHENYL)CARBAMATE
- Product Name
- TERT-BUTYL N-(4-IODOPHENYL)CARBAMATE
- CAS No.
- 159217-89-7
- Chemical Name
- TERT-BUTYL N-(4-IODOPHENYL)CARBAMATE
- Synonyms
- TERT-BUTYL 4-IODOPHENYLCARBAMATE;N-BOC-4-IODOANILIN;N-BOC-4-IODOANILINE;N-Boc-4-iodoaniline;ert-Butyl(4-iodophenyl)carbamate;TERT-BUTYL N-(4-IODOPHENYL)CARBAMATE;N-(tert-Butoxycarbonyl)-4-iodoaniline;(4-Iodophenyl)carbamic acid tert-butyl ester;N-(4-iodophenyl)carbamic acid tert-butyl ester;Carbamic acid, N-(4-iodophenyl)-, 1,1-dimethylethyl ester
- CBNumber
- CB7118623
- Molecular Formula
- C11H14INO2
- Formula Weight
- 319.14
- MOL File
- 159217-89-7.mol
TERT-BUTYL N-(4-IODOPHENYL)CARBAMATE Property
- Melting point:
- 144-148 °C
- Boiling point:
- 299.0±23.0 °C(Predicted)
- Density
- 1.591±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- form
- solid
- pka
- 13.12±0.70(Predicted)
- Appearance
- White to off-white Solid
- Sensitive
- Light Sensitive
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H317May cause an allergic skin reaction
H410Very toxic to aquatic life with long lasting effects
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P273Avoid release to the environment.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
N-Bromosuccinimide Price
- Product number
- 761826
- Product name
- N-Boc-4-iodoaniline
- Purity
- 95%
- Packaging
- 5g
- Price
- $201
- Updated
- 2023/06/20
- Product number
- 761826
- Product name
- N-Boc-4-iodoaniline
- Purity
- 95%
- Packaging
- 1g
- Price
- $41.2
- Updated
- 2022/05/15
- Product number
- 010776
- Product name
- tert-ButylN-(4-iodophenyl)carbamate
- Purity
- 95%
- Packaging
- 1g
- Price
- $12
- Updated
- 2021/12/16
- Product number
- 010776
- Product name
- tert-ButylN-(4-iodophenyl)carbamate
- Purity
- 95%
- Packaging
- 5g
- Price
- $25
- Updated
- 2021/12/16
- Product number
- 5050AD
- Product name
- tert-Butyl4-iodophenylcarbamate
- Packaging
- 1g
- Price
- $66
- Updated
- 2021/12/16
TERT-BUTYL N-(4-IODOPHENYL)CARBAMATE Chemical Properties,Usage,Production
Synthesis
24424-99-5
540-37-4
159217-89-7
GENERAL STEPS: The reaction was carried out in a 50 mL round-bottomed flask at 80°C under reduced pressure for 10 minutes. In a typical experiment, 5 mmol of p-iodoaniline was mixed with 5 mmol of di-tert-butyl dicarbonate and the reaction lasted for 10 minutes. Upon completion of the reaction, the solvent was removed by rotary evaporator under vacuum to give tert-butyl (4-iodophenyl)carbamate.
References
[1] Bioorganic and Medicinal Chemistry Letters, 2006, vol. 16, # 22, p. 5864 - 5869
[2] Research on Chemical Intermediates, 2017, vol. 43, # 3, p. 1355 - 1363
[3] Chemical Communications, 2013, vol. 49, # 61, p. 6909 - 6911
[4] Patent: WO2004/12736, 2004, A1. Location in patent: Page/Page column 24
[5] Organic Letters, 2018, vol. 20, # 7, p. 1693 - 1697
TERT-BUTYL N-(4-IODOPHENYL)CARBAMATE Preparation Products And Raw materials
Raw materials
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