ChemicalBook > CAS DataBase List > 6-Fluoro-2-aminophenol

6-Fluoro-2-aminophenol

Product Name
6-Fluoro-2-aminophenol
CAS No.
53981-25-2
Chemical Name
6-Fluoro-2-aminophenol
Synonyms
6-Fluoro-2-aminophen;6-Fluoro-2-Aminophenol;2-Amino-6-fluorophenol97%;Phenol, 2-amino-6-fluoro-;2-Amino-6-fluorophenol 97%;3-Fluoro-2-hydroxyaniline 97%
CBNumber
CB71459457
Molecular Formula
C6H6FNO
Formula Weight
127.12
MOL File
53981-25-2.mol
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6-Fluoro-2-aminophenol Property

Boiling point:
215.7±25.0 °C(Predicted)
Density 
1.347±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
solubility 
DMSO (Slightly), Methanol (Slightly)
pka
8.50±0.10(Predicted)
form 
Solid
Appearance
Brown to black Solid
InChI
InChI=1S/C6H6FNO/c7-4-2-1-3-5(8)6(4)9/h1-3,9H,8H2
InChIKey
MDIAVSZFIQWYST-UHFFFAOYSA-N
SMILES
C1(O)=C(F)C=CC=C1N
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Safety

RIDADR 
2811
HazardClass 
6.1
PackingGroup 
Ⅲ
HS Code 
2921420090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H312Harmful in contact with skin

H315Causes skin irritation

H319Causes serious eye irritation

H331Toxic if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC
Product number
A609590
Product name
2-Amino-6-fluorophenol
Packaging
5g
Price
$290
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA17661
Product name
2-Amino-6-fluorophenol
Packaging
1g
Price
$40
Updated
2021/12/16
Matrix Scientific
Product number
073498
Product name
6-Fluoro-2-aminophenol
Purity
95+%
Packaging
1g
Price
$43
Updated
2021/12/16
SynQuest Laboratories
Product number
4656-3-08
Product name
2-Amino-6-fluorophenol
Purity
97%
Packaging
1g
Price
$52
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA17661
Product name
2-Amino-6-fluorophenol
Packaging
2g
Price
$70
Updated
2021/12/16
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6-Fluoro-2-aminophenol Chemical Properties,Usage,Production

Chemical Properties

Purple crystals

Uses

A metabolite of halogenated aniline.

Synthesis

1526-17-6

53981-25-2

The general procedure for the synthesis of 6-fluoro-2-aminophenol from 2-fluoro-6-nitrophenol was as follows: 2-fluoro-6-nitrophenol (6.37 mmol, 1.00 g) was dissolved in methanol (100 mL), and 10% activated charcoal-loaded palladium catalyst (10% by weight of 2-fluoro-6-nitrophenol, 0.10 g) was added. The reaction system was displaced first with argon and then with hydrogen, each displacement lasting 15 min, during which magnetic stirring was maintained. Subsequently, the reaction was carried out at atmospheric pressure (using a hydrogen balloon) and under hydrogen atmosphere for 1 hour. Upon completion of the reaction, the gas in the reaction vessel was again replaced with argon for 15 minutes. The reaction mixture was filtered through a diatomaceous earth pad and washed with methanol (50 mL). The filtrate was concentrated under vacuum to give a red solid product. Purification by silica gel column chromatography (eluent ratio 1:1 hexane/chloroform) gave a white crystalline solid in 87% yield.

References

[1] Bioorganic and Medicinal Chemistry Letters, 2014, vol. 24, # 15, p. 3521 - 3525
[2] Patent: JP2016/124812, 2016, A. Location in patent: Paragraph 0115
[3] Patent: US2010/298334, 2010, A1. Location in patent: Page/Page column 46
[4] Patent: WO2005/118561, 2005, A1. Location in patent: Page/Page column 25
[5] Patent: US2005/124667, 2005, A1. Location in patent: Page/Page column 17

6-Fluoro-2-aminophenol Preparation Products And Raw materials

Raw materials

Preparation Products

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6-Fluoro-2-aminophenol Suppliers

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View Lastest Price from 6-Fluoro-2-aminophenol manufacturers

Career Henan Chemical Co
Product
6-Fluoro-2-aminophenol 53981-25-2
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
200kg
Release date
2020-01-02

53981-25-2, 6-Fluoro-2-aminophenolRelated Search:

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  • 6-Fluoro-2-Aminophenol
  • 6-Fluoro-2-aminophen
  • 3-Fluoro-2-hydroxyaniline 97%
  • 2-Amino-6-fluorophenol97%
  • 2-Amino-6-fluorophenol 97%
  • Phenol, 2-amino-6-fluoro-
  • 53981-25-2
  • Aromatics
  • Metabolites & Impurities