3-((2,2,2- trifluoroethyl)thio)aniline

ChemicalBook > CAS DataBase List > 3-((2,2,2- trifluoroethyl)thio)aniline

3-((2,2,2- trifluoroethyl)thio)aniline

Product Name: 3-((2,2,2- trifluoroethyl)thio)aniline
CAS No.: 1445684-99-0
Chemical Name: 3-((2,2,2- trifluoroethyl)thio)aniline
Synonyms: NA12878;CarolGold;WKPep Erasin;Palm-Glu-OtBu;Fmoc-D-Ala-Ala-OH;CarolGold (Lutein);Magnolol & Honokiol;BOC-(D)-HIS(TRT)-AIB;Octa(OtBu)-D-Glu-OtBu;Boc-D-His(Trt)-Aib-OH
CBNumber: CB71459710
Molecular Formula: C8H8F3NS
Formula Weight: 207.22
MOL File: 1445684-99-0.mol

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3-((2,2,2- trifluoroethyl)thio)aniline Property

InChI: InChI=1S/C8H8F3NS/c9-8(10,11)5-13-7-3-1-2-6(12)4-7/h1-4H,5,12H2
InChIKey: KMYQCBMXXMOPSD-UHFFFAOYSA-N
SMILES: C1(N)=CC=CC(SCC(F)(F)F)=C1

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

chempep

Product number: 181931
Product name: Boc-His(Trt)-Aib-Glu(OtBu)-Gly-OH
Packaging: 1g
Price: $300
Updated: 2021/12/16

Iris Biotech GmbH

Product number: FAA7750
Product name: Fmoc-D-Lys(Palm-D-Glu-OtBu)-OH
Packaging: 1g
Price: $607.5
Updated: 2021/12/16

chempep

Product number: 181931
Product name: Boc-His(Trt)-Aib-Glu(OtBu)-Gly-OH
Packaging: 5g
Price: $900
Updated: 2021/12/16

chempep

Product number: 181931
Product name: Boc-His(Trt)-Aib-Glu(OtBu)-Gly-OH
Packaging: 25g
Price: $2000
Updated: 2021/12/16

Iris Biotech GmbH

Product number: FAA7750
Product name: Fmoc-D-Lys(Palm-D-Glu-OtBu)-OH
Packaging: 5G
Price: $2160
Updated: 2021/12/16

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3-((2,2,2- trifluoroethyl)thio)aniline Chemical Properties,Usage,Production

Uses

3-((2,2,2-trifluoroethyl)thio)aniline can be used as an intermediate in pharmaceutical research.

Synthesis

To a solution of 3-aminobenzenethiol (4.43 g, 35.4 mmol) in THF (225 mL) was added sodium hydride (1.77 g, 44.3 mmol) at 0 °C and stirred for 30 min. Then, 2,2,2-trifluoroethyl 4- methylbenzenesulfonate (9.0 g, 35.4 mmol) was added and the reaction mixture was stirred for 18 h. The reaction mixture was quenched with water (20 mL) and extracted with EtOAc (2x50 mL). The combined organic extracts were washed with water, dried over Na2SO4, fdtered, and concentrated under reduced pressure. The crude residue was purified by flash chromatography through a Redi-Sep pre-packed silica gel column, eluting with a gradient of 5 % to 10 % EtOAc in hexanes, to give 3-((2,2,2- trifluoroethyl)thio)aniline (5 g, 68 % yield) as a pale brown oil.

3-((2,2,2- trifluoroethyl)thio)aniline Preparation Products And Raw materials

Raw materials

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View Lastest Price from 3-((2,2,2- trifluoroethyl)thio)aniline manufacturers

Career Henan Chemical Co

Product: 4-Chluoro-2-bromotoluene 1445684-99-0
Price: US $1.00/ASSAYS
Min. Order: 1ASSAYS
Purity: 98%
Supply Ability: 1kg,2kg,100kg
Release date: 2019-07-09

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